KR20160047368A - High performance Liquid Distributor - Google Patents

High performance Liquid Distributor Download PDF

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Publication number
KR20160047368A
KR20160047368A KR1020140172306A KR20140172306A KR20160047368A KR 20160047368 A KR20160047368 A KR 20160047368A KR 1020140172306 A KR1020140172306 A KR 1020140172306A KR 20140172306 A KR20140172306 A KR 20140172306A KR 20160047368 A KR20160047368 A KR 20160047368A
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KR
South Korea
Prior art keywords
liquid
catch
present
pipe
liquid distributor
Prior art date
Application number
KR1020140172306A
Other languages
Korean (ko)
Inventor
강기준
윤영범
Original Assignee
(주)티피티퍼시픽
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Application filed by (주)티피티퍼시픽 filed Critical (주)티피티퍼시픽
Publication of KR20160047368A publication Critical patent/KR20160047368A/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/32Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77Liquid phase processes
    • B01D53/78Liquid phase processes with gas-liquid contact

Abstract

The present invention relates to a high performance liquid distributor comprising: a feed pipe, which supplies a liquid flowing from the outside of a reactor or a fractionation column, or a collector tray, which collects a liquid flowing from the outside or a liquid falling from an upper part of the column; a catch pan introduced from the feed pipe or the collector tray; and two or more down pipes which are divided into several pipes and supplying the liquid to a liquid distributor connected to the lower side. Therefore, the liquid is equally distributed to the whole area of the distributor if a support ring in the distributor is not installed horizontally, thereby maximizing gas-liquid contact and increasing efficiency and the amount of the liquid distributed to each divided pipe of the liquid distributor is equal in a floating production storage and offloading (FPSO) with the shaking of the distributor, thereby keeping an even distribution of the liquid.

Description

TECHNICAL FIELD [0001] The present invention relates to a high-performance liquid distributor,

The present invention relates to a high-efficiency liquid distributor, and more particularly to a liquid distributor for use in a fractionation column and related apparatus among fluid contact and dispersing apparatuses, As a distributor of a distillation column for separating substances using distillation, absorption and cooling principles in a distillation tower, a washing tower and an absorption tower for removing and separating fine chemicals and noxious gases or organic matters, And more particularly, to a high-efficiency liquid dispensing apparatus for maximizing efficiency of vapor-liquid contact by maximizing the efficiency of vapor-liquid contact.

Currently, there are columns which are used industrially for distillation, absorption and cooling. These columns are devices for separating or absorbing a desired substance through vapor-liquid contact.

Particularly, an apparatus constituting the inside of the column for facilitating gas-liquid contact is referred to as a tower internal, and representative examples thereof include a tray and a packing.

Examples of the packing include random packing, structured packing, and grid packing. In general, the structured packing has a high efficiency and a large processing capacity, and the grid packing is processed Although the capacity is large, the efficiency is low and the use is limited to a specific use.

The packed column includes a packing support for supporting the packing, a bed limiter for preventing flow to the upper part, a liquid distributor for uniformly dispersing the liquid in the packing, (Liquid Distributor).

The liquid distributor is a tower interior that has the greatest influence on the performance of the packing. The liquid distributor has a variety of structures depending on the conditions. Particularly, in the FPSO, the liquid distributor is not flat (Pipe Orifice Type) is widely used because the uneven distribution of the liquid is required to minimize the liquid level difference.

The configuration, function and operation of a conventionally used pipe orifice type liquid dispensing apparatus will be described below.

FIGS. 1A to 1C are views showing a liquid distributor according to a first embodiment of the present invention, and FIGS. 2A to 2C are diagrams showing a liquid distributor according to a second embodiment of the present invention 3A to 3C are views showing a liquid distributor according to a third embodiment of the present invention.

The liquid flowing from the upper or the lower collector tray 500 is discharged through a pipe orifice 100 through a feed pipe 100 or a down pipe 300, Orifice Type) liquid dispenser 400. The liquid dispenser 400 is connected to the liquid dispenser 400 via a liquid supply pipe (not shown).

The liquid 10 transferred to the catch pan is transferred to a main header pipe 410 and is supplied to each of the side pipes connected to the main header pipe 410 And 420 and is distributed to the upper portion of the packing through a nipple pipe 430 formed at the lower end.

When the diameter of the column is large, a distance from the catch pan is increased due to pressure drop in the distributor lateral pipe 420 of the distributor, The amount of the liquid (liquid) 10 to be dispensed may be different.

Therefore, the number of catch pan (Catch Pan) should be more than two.

FIG. 4A is a front view showing a vertical state of a liquid distributor according to a third embodiment of the present invention, and FIG. 4B is a front view showing a state in which the liquid distributor according to the third embodiment of the present invention is tilted Is a front view showing the dispensing state of the liquid.

Referring to FIGS. 4A and 4B, as a distribution apparatus used in the FPSO among liquid distribution apparatuses, a floating production storage and offloading (FPSO) is generally used for a marine plant or a drillship The FPSO is a special ship capable of refining crude oil extracted from a tanker and storing it in a shuttle tanker or other transporting area. The FPSO produces and processes the lower hull structure (Hull) (Topsides) that function as a facility.

In the case of such an FPSO, a liquid level difference occurs between the catch pan and the main header pipe connected to each catch pan when the sea structure or ship is shaken by the wind or wave, The amount of the liquid 10 supplied to the lateral pipe 420 and the amount of the liquid supplied to the lateral pipe 420 may be different from each other and the liquid in the nipple pipe 430 at the lower end of the lateral pipe 420 , 10) is different for each drop point (Drip Points).

In addition, a support ring welded to the inside of the column for installation of a collector tray in the case of an onshore plant or a column installed in an FPSO is tilted due to manufacturing problems, The level of the collector tray installed thereon is also tilted.

That is, since the liquid level of each down pipe is different from that of the collector tray, the amount of the liquid supplied to the liquid distributor mounted on the lower portion of the down pipe varies even if the column is not shaken.

Ultimately, if the amount of liquid to be supplied to the packing under each drip point is changed, the performance of the packing is remarkably deteriorated to deteriorate separation and absorption.

Korean Patent Publication No. 2003-0041510, published on May 27, 2003

Accordingly, a first object of the present invention is to provide a high-efficiency liquid dispensing apparatus capable of increasing the efficiency by maximizing the vapor-liquid contact effect by uniformly distributing the liquid dispensed to the entire column And a second object of the present invention is to provide a method for manufacturing a collector tray in a column installed in an onshore plant or an FPSO even when a support ring welded to the inside of the column is installed in an inclined state, The present invention provides a liquid distribution apparatus capable of evenly distributing the liquid, and a third object of the present invention is to provide a liquid distribution apparatus capable of uniformly distributing the liquids, such as floating production storage and offloading (FPSO) In the case of a land-based plant, the amount of liquid dispensed between each branched pipe of the liquid distributing device is not different, And it is a fourth object of the present invention to provide a highly efficient liquid distributing apparatus applicable to a reaction apparatus or a distillation apparatus.

According to an aspect of the present invention, there is provided a method of controlling a flow rate of a liquid supplied from a feed pipe, the method comprising: A catch pan in which a liquid level is formed and a configuration of two or more down pipes for supplying a liquid to a liquid distributor which is branched from the catch pan into a plurality of pieces and connected to the lower side Lt; / RTI >

According to the structure of the present invention as described above, the distribution of the liquid is uniformly distributed over the entire area of the apparatus, thereby maximizing the gas-liquid contact effect, thereby increasing the liquid distribution efficiency.

In addition, even in offshore plants where float shaking is present in floating plant storage and offloading (FPSO) or tilted support rings, differences in the amount of liquid dispensed between each branch pipe of the liquid distributor So it is a very useful invention that can keep liquid distribution even.

Furthermore, it is also effective in improving the liquid dispensing effect by applying to a distillation apparatus, a reaction apparatus, a drum, or the like.

FIG. 1A is a perspective view showing a liquid distributor according to a first embodiment of the present invention. FIG.
1B is a front view showing a liquid distributor according to the first embodiment of the present invention.
1C is a side view showing a liquid distributor according to the first embodiment of the present invention.
2A is a perspective view showing a liquid distributor according to a second embodiment of the present invention.
2B is a front view showing a liquid distributor according to a second embodiment of the present invention.
2C is a side view showing a liquid distributor according to a second embodiment of the present invention.
3A is a perspective view showing a liquid distributor according to a third embodiment of the present invention.
3B is a front view showing a liquid distributor according to a third embodiment of the present invention.
3C is a side view showing a liquid distributor according to a third embodiment of the present invention.
4A is a front view showing a vertical state of a liquid distributor according to a third embodiment of the present invention.
4B is a front view showing a distribution state of the liquid in a tilted state of the liquid distributor according to the third embodiment of the related art.
5A is a perspective view showing a high-efficiency liquid distributor according to the first embodiment of the present invention.
5B is a front view showing a high-efficiency liquid distributor according to the first embodiment of the present invention.
FIG. 5C is a side view showing a high-efficiency liquid distributor according to the first embodiment of the present invention; FIG.
6A is a perspective view showing a high-efficiency liquid distributor according to a second embodiment of the present invention.
6B is a front view showing a high-efficiency liquid distributor according to the second embodiment of the present invention.
6C is a side view showing a high-efficiency liquid distributor according to a second embodiment of the present invention
7A is a perspective view showing a high-efficiency liquid distributor according to a third embodiment of the present invention.
7B is a front view showing a high-efficiency liquid distributor according to the third embodiment of the present invention.
7C is a side view showing a high-efficiency liquid distributor according to the third embodiment of the present invention
8 is a perspective view showing a high-efficiency liquid dispensing apparatus according to a fourth embodiment of the present invention;
9A is a perspective view showing a high-efficiency liquid distributing apparatus according to a fifth embodiment of the present invention;
FIG. 9B is a perspective view showing a high-efficiency liquid distributing apparatus according to a sixth embodiment of the present invention; FIG.
FIG. 10A is a perspective view showing a catch fan of a high-efficiency liquid distributor according to a seventh embodiment of the present invention; FIG.
FIG. 10B is a front view showing the catch fan of the high-efficiency liquid distributor according to the eighth embodiment of the present invention; FIG.
FIG. 10C is a side view showing a catch fan of a high-efficiency liquid distributor according to a ninth embodiment of the present invention; FIG.
FIG. 10D is a side view showing the catch fan of the high-efficiency liquid distributor according to the tenth embodiment of the present invention
11A is a front view showing a vertical state of a liquid distributor according to a third embodiment of the present invention;
11B is a front view showing a distribution state of the liquid in a tilted state of the liquid distributor according to the third embodiment of the present invention

In order to accomplish the above object, the present invention provides a feed pipe for feeding a liquid introduced from the outside of a fractionation column, and a feed pipe connected to the feed pipe, A catch pan in which a liquid level of the liquid introduced from the inside is formed and a pair of two liquid distributors branched from the catch pan and connected to the lower side, And a down pipe.

Hereinafter, embodiments according to the present invention will be described with reference to the accompanying drawings.

FIG. 5A is a perspective view showing a high-efficiency liquid distributor according to the first embodiment of the present invention, FIG. 5B is a front view showing a high-efficiency liquid distributor according to the first embodiment of the present invention, 5C is a side view showing a high-efficiency liquid distributor according to the first embodiment of the present invention.

5A to 5C, a high-efficiency liquid distributor according to the first embodiment of the present invention includes a feed pipe 100, a catch pan 200, a liquid distributor (not shown) And a down pipe 300 for supplying the liquid to the liquid distributor 400.

The feed pipe 100 is configured to supply the liquid introduced from the outside of the fractionation column.

One of the catch pans 200 is connected to the feed pipe 100 so that the liquid 10 supplied from the feed pipe 100 flows and the liquid level of the liquid 10 Liquid level is formed.

Providing one configuration for the catch fan is to prevent the liquid distribution from becoming uneven due to the tilting of the liquid level or the fluctuation of the liquid level. The liquid is branched at an appropriate position and an appropriate number and distributed to the liquid distributor, It is intended to prevent the uneven distribution due to the shaking of the ship in the plant structure or the FPSO distillation apparatus so as to maintain even distribution to the uniform state.

The down pipe 300 is configured to supply liquid to a liquid distributor 400 branched from the catch fan 200 and connected to the lower side.

FIG. 6A is a perspective view showing a high-efficiency liquid distributor according to a second embodiment of the present invention, FIG. 6B is a front view showing a high-efficiency liquid distributor according to a second embodiment of the present invention, 6C is a side view showing a high-efficiency liquid distributor according to a second embodiment of the present invention.

6A to 6C, a high-efficiency liquid distributor according to a second embodiment of the present invention includes a collector tray 500 and one or a plurality of collectors 500 coupled to the collector tray 500 A down pipe 310, a catch pan 200, and a liquid distributor 400 connected to the lower side of the catch pan. , 300).

The collector tray 500 receives a liquid that flows from the outside of the fractionation column or descends from the top or receives liquid from the outside and a liquid that falls from the top, (Liquid level) is formed.

One or more down pipes 310 coupled to the collector tray 500 and falling down from the collector tray 500 are mounted.

A catch pan connected to the down pipe 310 to receive the liquid 10 supplied from the down pipe 310 and having a liquid level of the liquid 10 introduced therein, 200 and a down pipe 300 for supplying a liquid to a liquid distributor 400 connected to the catch fan 200 on the lower side.

FIG. 7A is a perspective view showing a high-efficiency liquid distributor according to a third embodiment of the present invention, FIG. 7B is a front view showing a high-efficiency liquid distributor according to a third embodiment of the present invention, 7C is a side view showing a highly efficient liquid distributor according to a third embodiment of the present invention.

7A to 7C, a high-efficiency liquid distributor according to a third embodiment of the present invention includes a liquid introduced from the outside of the fractionation column or a liquid falling from the top of the column, A collector tray 500 for collecting the liquid to be dropped from the upper portion of the column and the liquid to be lowered from the upper portion of the column and a collector tray 500 for passing the liquid 10 from the collector tray 500, A plurality of down pipes 310 and a liquid 10 supplied from the down pipe 310 which is connected to the down pipe 310 and flows into the liquid level And two or more down pipes 300 for supplying a liquid to a liquid distributor 400 connected to the lower side of the catch pan 200. [ ) It is configured.

8 is a perspective view illustrating a high-efficiency liquid dispensing apparatus according to a fourth embodiment of the present invention. Referring to FIG. 8, the high-efficiency liquid dispensing apparatus according to the fourth embodiment of the present invention includes:

And a balance control pipe 600 connected to the upper or lower part of the catch pan 200. The balance control pipe 600 is connected to the down pipe having a slanted level And the inclined level is adjusted through the ballast control pipe 600 to prevent the distribution of uneven liquid.

Particularly, the balance control pipe 600 can replace the catch fan 200 of the high-efficiency liquid distributing apparatus according to the first to third embodiments.

9A is a perspective view showing a high efficiency liquid dispensing apparatus according to a fifth embodiment of the present invention. Referring to FIG. 9A, a high efficiency liquid dispensing apparatus according to a fifth embodiment of the present invention includes an upper portion And a down pipe 310 is mounted on each of the intermediate catch fans 200. In the case where the diameter of the column is very large, By further mounting the catch fan 200, it is possible to prevent the distribution of uneven liquid depending on the inclined level.

9B is a perspective view showing a catch fan of a high efficiency liquid distributor according to a sixth embodiment of the present invention. Referring to FIG. 9B, the high efficiency liquid distributing apparatus according to the sixth embodiment of the present invention includes the above- In the high-efficiency liquid distributor from the first embodiment to the fifth embodiment, an anti-sloshing device is provided in the upper part of the catch fan 200 in order to have a flow rate fluctuation resistance due to the fluctuation of the liquid level, (800).

That is, an anti-sloshing device is further provided on the catch pan 200 to have a flow rate variation resistance due to the fluctuation of the liquid level. The device is structured packing, Grid, Random Packing, Perforated Plate and so on.

In particular, the anti-sloshing device is installed on a down pipe connected to a collector tray so as to have a flow variation resistance in a liquid flowing downward.

Particularly, the catch pan 200 is characterized by a cylinder, a cone, or a polygonal cylinder.

Further, the down pipe 300 connected to the lower portion of the catch fan 200 is branched by a necessary amount and connected to the liquid distributor.

FIG. 10A is a perspective view showing a catch fan of a high efficiency liquid distributing apparatus according to a seventh embodiment of the present invention, FIG. 10B is a front view showing a catch fan of a high efficiency liquid distributor according to an eighth embodiment of the present invention FIG. 10C is a side view showing a catch fan of a high efficiency liquid distributor according to a ninth embodiment of the present invention, FIG. 10D is a side view of a high efficiency liquid distributor according to a tenth embodiment of the present invention, Of the catch fan.

Referring to FIG. 10A, the catch fan of the high-efficiency liquid distributor of the distillation apparatus according to the seventh embodiment of the present invention has an irregular cylindrical shape.

Referring to FIG. 10B, the catch fan of the high-efficiency liquid distributor according to the eighth embodiment of the present invention has a quadrangular pyramid shape and thus has a cylindrical shape of a polygonal pyramid.

Referring to FIG. 10C, the catch fan of the high-efficiency liquid distributor according to the ninth embodiment of the present invention has a conical shape.

Referring to FIG. 10D, the catch fan of the high-efficiency liquid distributor according to the tenth embodiment of the present invention has a shape including projections on the side surface of the catch pan.

In this way, the catch fan can be manufactured in various shapes, and can be divided into an open type and a closed type depending on the presence or absence of the upper cover of the catch fan.

Various shapes of such catch fans can be manufactured in various volumes and various shapes in order to maximize the effects of the capacity of the liquid distributor and the inflow of liquid and the branching of the down pipe.

FIG. 11A is a front view showing a vertical state of a liquid distributor according to a third embodiment of the present invention, and FIG. 11B is a front view of a liquid distributor according to a third embodiment of the present invention, FIG. 3 is a front view showing a distribution state of the liquid in FIG.

11A and 11B, the liquid distributor according to the third embodiment of the present invention overcomes the disadvantages of the conventional liquid distributor. Even when the distillation apparatus is inclined, the collector tray 500 and the catch A liquid level is formed in the fan 200 and there is no difference in the distribution of the liquid between the down pipes 300 that are coupled to the lower portion of the catch pan 200 and are respectively branched.

That is, according to the present invention, one catch fan 200 is formed below the feed pipe 100 and the collector tray 500 to form a liquid level, and a plurality of down pipes (300) to supply liquid evenly to the liquid distributor, thereby preventing uneven liquid distribution due to tilting or shaking of the marine structure.

Therefore, the present invention has such an advantage that the distribution of the liquid can be uniformly distributed over the whole column to maximize the gas-liquid contact effect, thereby increasing the efficiency. In addition, even in an offshore structure or land- This is a very useful invention that can keep the liquid distribution evenly since there is no difference in the amount of liquid dispensed between each branch pipe of the apparatus.

10: liquid 100: feed pipe
200: catch fan 300, 310: down pipe
400: liquid distributor 410: header pipe
420: side pipe 430: nipple pipe
500: Collector tray 600: Balance control pipe
700: catch fan protrusion 800: sloshing suppression device

Claims (12)

A feed pipe 100 for feeding the liquid introduced from the outside of the fractionation column,
A catch pan 200 through which the liquid 10 supplied from the feed pipe 100 flows,
Two or more down pipes 300 branched from the catch fan 200 to receive the liquid 10,
And a liquid distributor (400) into which the liquid (10) flows from the down pipe (300).
A collector tray 500 for receiving a liquid that flows from the outside of the fractionation column or descends from the upper portion or receives the liquid from the outside and the falling portion from the top,
One or more down pipes 310 through which the liquid supplied from the collector tray 500 flows,
A catch pan 200 through which the liquid 10 descending from the down pipe 310 flows,
Two or more down pipes 300 branched from the catch fan 200 to receive the liquid 10,
And a liquid distributor (400) into which the liquid (10) flows from the down pipe (300).
3. The method according to claim 1 or 2,
Further comprising a balance control pipe (600) connected to the upper or lower portion of the catch pan (200).
3. The method according to claim 1 or 2,
And a balance control pipe (600) in place of the catch pan (200).
The method according to claim 1 or 2 or 3 or 4,
Wherein the high-efficiency liquid distributing device is used in a reactor or a drum.
The method according to claim 1 or 2 or 3,
Further comprising a plurality of intermediate catch fans (200) connected to the catch fan (200) by a down pipe (310) above or below the catch fan (200).
The method according to claim 1 or 2 or 3,
Further comprising an anti-sloshing device (800) disposed on the catch fan (200) to have a flow rate variation resistance due to a fluctuation of liquid level.
The method according to claim 1 or 2 or 3,
Wherein the catch pan (200) has a cylindrical shape or a polygonal cylindrical shape.
The method according to claim 1 or 2 or 3,
Wherein the catch pan (200) has an irregular cylindrical shape.
The method according to claim 1 or 2 or 3,
Characterized in that the catch pan (200) has a cylindrical shape such as a cone barrel or a polygonal horn.
The method according to claim 1 or 2 or 3,
Further comprising a plurality of catch pan protrusions (700) on the side of the catch pan (200).
The method according to claim 1 or 2 or 3,
Wherein the catch pan (200) is configured to be closed and open depending on the presence or absence of the upper cover.
KR1020140172306A 2014-10-22 2014-12-03 High performance Liquid Distributor KR20160047368A (en)

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KR20140143247 2014-10-22

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117735660A (en) * 2024-02-06 2024-03-22 爱德士制鞋(枣庄)有限责任公司 Rinsing wastewater treatment equipment for clothing production

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117735660A (en) * 2024-02-06 2024-03-22 爱德士制鞋(枣庄)有限责任公司 Rinsing wastewater treatment equipment for clothing production

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