KR20140068708A - Sterilized wet tissue and manufacturing mehotd of the same - Google Patents
Sterilized wet tissue and manufacturing mehotd of the same Download PDFInfo
- Publication number
- KR20140068708A KR20140068708A KR1020120136535A KR20120136535A KR20140068708A KR 20140068708 A KR20140068708 A KR 20140068708A KR 1020120136535 A KR1020120136535 A KR 1020120136535A KR 20120136535 A KR20120136535 A KR 20120136535A KR 20140068708 A KR20140068708 A KR 20140068708A
- Authority
- KR
- South Korea
- Prior art keywords
- wet tissue
- present
- sterilization
- sterilized
- manufacturing
- Prior art date
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Classifications
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47K—SANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
- A47K10/00—Body-drying implements; Toilet paper; Holders therefor
- A47K10/16—Paper towels; Toilet paper; Holders therefor
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47K—SANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
- A47K7/00—Body washing or cleaning implements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B31—MAKING ARTICLES OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER; WORKING PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER
- B31D—MAKING ARTICLES OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER, NOT PROVIDED FOR IN SUBCLASSES B31B OR B31C
- B31D1/00—Multiple-step processes for making flat articles ; Making flat articles
- B31D1/04—Multiple-step processes for making flat articles ; Making flat articles the articles being napkins, handkerchiefs, towels, doilies, or the like
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
Abstract
The present invention provides a method for manufacturing a sterile wet tissue comprising the step of immersing a material for a wet tissue in a stock solution and sterilizing the material at 100 to 140 ° C and 1.5 to 3.0atm for 10 to 60 minutes, and a sterile wet tissue produced by the method. According to the present invention, sterilization is carried out in a non-chemical and physical manner without addition of a chemical substance or radiation, so that it is safe for human body and has excellent effect of inhibiting fungal and bacterial infections. The present invention can be applied to a wet tissue for oral use sensitive to bacteria, Lt; / RTI >
Description
The present invention relates to a sterile wet tissue and a method for manufacturing the same, and more particularly, to a sterile wet tissue which is sterilized physically and chemically under high temperature and high pressure, and a method for producing the same.
In general, almost all wet tissues contain chemical preservatives such as benzoic acid (sorbic acid, sorbic acid, etc.) to prevent bacteria and fungi from propagating in the course of distribution and use of moisture and packaging of pulp or nonwoven tissue materials. Methylparaben, ethylparaben, ethylparaben, propylparaben, butylparaben, butylparaben, carbamates: 3-iodo-2-propynyl bytyl carbamate, 4-thiazolyl-benzimidazole, 2- Benzodiazonium chloride, polyvinyl butyral, diiodomethyl p-tolithrosulfone, 2,4,5,6-tetrachloroisobutyronitrile, p-oxybenzoic acid, etc.) or radiation sterilization And
However, even if the use amount of the preservative is less than the legal preservative use standard, there are still harmful components such as skin seizure, erythema and other skin irritation which are common phenomenon of the preservative, The risk of skin contact is high. Radiation sterilization also has the potential to cause adverse effects in humans.
Furthermore, even if the antibacterial tissue is manufactured and sold, a certain amount of preservative may be required to maintain anti-fungi, which is a common problem and a problem to be solved by the related industry .
In some cases, it is a practical matter to use antiseptic agents such as silver ion, chitosan, and various chemical agents strongly antimicrobial, even if they are manufactured and sold as antibacterial wet tissue.
In order to solve the above-mentioned problems, the present invention provides a method for producing a sterile wipe which sterilizes under high temperature and pressure conditions at a specific temperature, atmospheric pressure, and time so as to have an excellent sterilization effect without chemical preservative and irradiation with radiation, And to provide a sterile wet tissue.
In order to solve the above-mentioned problems, the present invention provides a method for manufacturing a sterile wipes, comprising: immersing a wet tissue for a wet tissue in a stock solution, and sterilizing the wet tissue at 100 to 140 DEG C for 1.5 to 3.0 atm for 10 to 60 minutes.
In one embodiment of the present invention, the method may further include packaging the sterilized wet tissue material.
In an embodiment of the present invention, the material for the wet tissue may be a nonwoven fabric of an organic cotton face.
In one embodiment of the present invention, the stock solution may be ultrapure pure water obtained by reverse osmosis (R / O) method.
In one embodiment of the present invention, the ultra pure water may have a resistance of 18.2 M or more.
The present invention also provides a sterile wet tissue produced according to the above production method.
In an embodiment of the present invention, the wet tissue may be an oral wet tissue, a newborn wet tissue, or an infant wet tissue.
According to the method for producing a sterile wipes according to the present invention, sterilization is carried out in a non-chemical and physical manner without chemical addition or irradiation of radiation, so that it is safe to the human body and has excellent effect of inhibiting fungal and bacterial infections. , Can be used for newborn and infant skin.
Hereinafter, preferred embodiments of the present invention will be described in detail in order to facilitate the present invention by those skilled in the art.
The present invention provides a method for manufacturing a sterile wet tissue including a step of immersing a wet tissue for a wet tissue in a stock solution and sterilizing the wet tissue at 100 to 140 DEG C for 1.5 to 3.0 atm for 10 to 60 minutes.
In addition, the present invention may further include packaging the sterilized wet tissue material.
Hereinafter, the production method of the present invention will be described in detail.
First, a material for wet tissue and a stock solution are prepared.
In the present invention, the material for the wet tissue can be generally selected from materials used for wet tissues, non-woven fabric, cotton fabric, and paper.
Preferably, a nonwoven fabric may be used, and more preferably, the nonwoven fabric may be a 100% organic cotton face. Conventionally, rayon / polyester synthetic fibers have been used as a nonwoven fabric for wet tissues or general cotton has been used. However, the present invention introduces a material that has not been treated with chemicals compared to synthetic fibers or general cotton using organic certified cotton.
In the present invention, the undiluted solution may be ultrapure pure water obtained by a reverse osmosis (R / O) method. The ultrapure pure water preferably has a resistance of 18.2 M OMEGA or higher, and the presence of foreign matter, microorganisms, and ions can be suppressed in ultrapure water having a resistance of 18.2 M OMEGA or higher.
Ground and cut the prepared wet tissue material and immerse it in the stock solution. This can be sealed and packaged.
Then, the material for wet tissue immersed in the stock solution is sterilized. The sterilization is carried out at 100 to 140 캜, 1.5 to 3.0 atm for 10 to 60 minutes. At this time, no chemical preservative or chemical is added, and no radiation is applied. That is, by non-chemical and physical sterilization.
The sterilization temperature may be 100-140 캜, more preferably 110-130 캜, and most preferably 121 캜. If the temperature is lower than 100 ° C., the product may not be completely sterilized. If the temperature is higher than 140 ° C., the nonwoven fabric or the packaging material may be deformed.
The sterilizing air pressure may be 1.5 to 3.0 atm (atmospheric pressure) (0.15 to 0.3 MPa), more preferably 1.5 to 2.3 atm. If the air pressure is less than 1.5 atm, the temperature may not sufficiently rise and sterilization may not be performed. If the air pressure is more than 3.0 atm, there is a problem that deformation may occur in the packaging material.
The sterilization time may be 10 to 60 minutes, more preferably 30 to 60 minutes. If the time is less than 10 minutes, the sterilization may not be completed, and if it exceeds 60 minutes, the nonwoven fabric or the packaging material may be deformed.
According to the high-temperature high-pressure sterilization satisfying the above-mentioned temperature, pressure and time conditions, the microorganism sterilization effect is excellent and there is no mold or bacterial infection even after a few days after the production of the product. Such an excellent sterilization effect occurs when the conditions of 100 to 140 DEG C and atmospheric pressure of 1.5 to 3.0 atm are all satisfied.
The sterilization step of the present invention is harmless and safe to the human body since it is physically sterilized at high temperature and high pressure and does not contain any other chemical sterilization or irradiation.
Thereafter, the material for the wet tissue as described above is packed.
That is, it can be sterilized and packed in the manufacturing process of the wetted wipes before packaging. According to the prior art, the wipes are packaged after the wipes are manufactured, and then the radiation (gamma ray) sterilization is carried out. However, the present invention can have a manufacturing advantage by proceeding the packaging after sterilization.
The present invention also provides a sterile wet tissue produced according to the above-described method.
The sterilized wet tissue of the present invention was confirmed to be free of mold and bacterial infection in the microorganism test conducted 15 days or more after the preparation (see Experimental Example 1).
The sterilized wet tissue according to the present invention is excellent in sterilization effect and is harmless and safe to human body, so that it is not particularly limited, but it can be used as an oral wet tissue, a newborn baby wet tissue or a baby wet tissue, which are sensitive to bacteria.
The present invention will be described in more detail through the following examples. However, the examples are for illustrating the present invention, and the scope of the present invention is not limited thereto.
[Example 1] Manufacture of oral wet tissue
Pure water produced in the ultrapure water producing apparatus was prepared in a pure water introducing apparatus. A 450 mm wide roll made of organic cotton-made nonwoven fabric was prepared in a fabric feeder as a manufacturing facility. The cutter was cut to a width of 75 mm used for the product in the fabric feeder, and cut to a length of 185 mm while making it into a grounding form suitable for use. The ground organic woven nonwoven fabric was inserted into a three-ply packing material in a packing machine, and simultaneously 5 g of ultra pure water prepared above was injected. The packaging material containing the nonwoven fabric into which the undiluted solution was put was adhered to the four sides by a heat bar in the packaging machine. When a certain amount of the glued packaging material was collected, the sterilization device was put into a high-temperature high-pressure sterilizer. The high-temperature high-pressure sterilizer was a three-stage shelf, and 2,000 products were placed in each shelf, the temperature was raised to 126 DEG C, the internal pressure was increased to 2.5 atm (atmospheric pressure), and the product was sterilized for 50 minutes. The sterilized products were cooled to room temperature and then put in a paper box of 30 pieces each. At this time, the test was performed to check whether the product was correctly adhered. The paper box was put in a corrugated cardboard box for transportation again, sealed with tape, and stored in a warehouse
[Experimental Example 1] Microorganism test
The microorganism was tested with the oral wet tissue prepared in Example 1 above. The test method is the aseptic test method in the general test method of the Korean Pharmacopoeia, and the aseptic test method is a method for testing the presence or absence of microorganisms (bacteria or fungi) that can be propagated by the culture method. All necessary items such as water, reagent, test solution and instrument substrate used in this test were sterilized. The test was carried out on a clean bench in a clean room and the operation was thoroughly sterilized. The aseptic method is a direct method, which involves culturing all or part of the specimen directly into the medium.
1-1. Preparation of medium
To confirm the presence or absence of bacteria and fungi, a separate medium was prepared.
1-1-1. Preparation of bacterial culture medium
The bacterial medium was a modified thioglycolic acid medium. The following drugs and doses were used for the medium.
El-cystine 0.5 g
2.5 g of sodium chloride
Glucose 5.0 g
Yeast extract 5.0 g
15.0 g of casein-derived peptone
0.5 g of sodium thioglycolate
Water 1000 mL
L-cystine, sodium chloride, glucose, yeast extract, and peptone casein were added to a beaker, mixed with water and heated to dissolve. Then sodium thioglycolate was dissolved and sodium hydroxide solution was added to adjust the pH to 7.1 ± 0.2 after sterilization Respectively. After filtration of the solution with filter paper, it is divided into the required amount in the container having the surface area and the depth ratio in which the pale red portion of the medium becomes 1/2 or less from the top when the culture is finished, and the autoclave is autoclaved at 2 ~ 25 ° C Respectively.
1-1-2. Preparation of fungal media
The fungal medium was soybean casein digestion medium. The following drugs and doses were used for the medium.
17.0 g of casein-derived peptone
Soybean peptone 3.0 g
5.0 g of sodium chloride
2.5 g of potassium dihydrogenphosphate
Glucose 2.3 g
Water 1000 mL
All ingredients were added to a beaker and heated to dissolve. If necessary, sodium hydroxide solution was added to adjust the pH after sterilization to 7.3 ± 0.2. After filtering with filter paper, it was divided into the required amount in the test vessel, sterilized by autoclave and stored at 2 ~ 25 ° C.
1-2. Aseptic testing of products
Six samples of 5 g product samples were prepared. For the test, 40 ml of each of three 50 ml containers with a lid were placed in a modified thioglycolic acid medium for bacterial test prepared in 1-1-1 above and a soybean casein digestion medium for fungal test prepared in 1-1-2. Each of the prepared product samples was put into each of the three containers containing the soybean casein digestive medium for fungal test and the specimen, and a small amount (0.5 g or less) of chloramphenicol was added to remove the bacteria. The culture medium for bacterial test in the container containing the specimen was incubated at 35 DEG C, and the culture medium for fungal test was cultured at 25 DEG C for 14 days. After 14 days, the presence or absence of the culture solution was confirmed as follows.
The culture for bacterial test was initially pink but changed to yellow when the bacteria were proliferated and the first pink when the bacteria did not proliferate. The culture for the fungus test was initially yellowish but changed turbidly when the fungus proliferated, and was kept as a transparent yellow when the fungus did not proliferate.
1-3. Aseptic test result
The results of sterilization test of the product were as follows.
Date Bacterial abnormality Presence or absence of fungi
Oct 15 Not detected Not detected
October 22 Not detected Not detected
October 29 Not detected Not detected
November 5 Not detected Not detected
Claims (9)
And packaging the sterilized wet tissue material.
Wherein the material for the wet tissue is a non-woven fabric of an organic cotton face.
Wherein the raw liquid is pure water obtained by reverse osmosis (R / O) method.
Wherein the ultra pure water has a resistance of 18.2 M? Or more.
The wet tissue is an oral wet tissue.
The wet tissue is a wet tissue for a newborn baby.
The wet tissue is a wet tissue for infant.
Priority Applications (1)
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KR1020120136535A KR20140068708A (en) | 2012-11-28 | 2012-11-28 | Sterilized wet tissue and manufacturing mehotd of the same |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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KR1020120136535A KR20140068708A (en) | 2012-11-28 | 2012-11-28 | Sterilized wet tissue and manufacturing mehotd of the same |
Publications (1)
Publication Number | Publication Date |
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KR20140068708A true KR20140068708A (en) | 2014-06-09 |
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KR1020120136535A KR20140068708A (en) | 2012-11-28 | 2012-11-28 | Sterilized wet tissue and manufacturing mehotd of the same |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20210059237A (en) * | 2019-11-15 | 2021-05-25 | (주)다사요윙윙 | Cleaning tissue based on anti ammonia composition, and manufacturing method thereof |
CN114306184A (en) * | 2021-12-30 | 2022-04-12 | 华药生物科技(浙江)有限公司 | Preparation method of baby wet tissue with sterilizing and moisturizing core |
-
2012
- 2012-11-28 KR KR1020120136535A patent/KR20140068708A/en not_active Application Discontinuation
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20210059237A (en) * | 2019-11-15 | 2021-05-25 | (주)다사요윙윙 | Cleaning tissue based on anti ammonia composition, and manufacturing method thereof |
CN114306184A (en) * | 2021-12-30 | 2022-04-12 | 华药生物科技(浙江)有限公司 | Preparation method of baby wet tissue with sterilizing and moisturizing core |
CN114306184B (en) * | 2021-12-30 | 2023-07-25 | 华药生物科技(浙江)有限公司 | Preparation method of infant wet tissue with sterilization and moisturizing cores |
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