KR20130126221A - Composition for sikhae premix and thereof manufacturing method - Google Patents
Composition for sikhae premix and thereof manufacturing method Download PDFInfo
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- KR20130126221A KR20130126221A KR1020120050140A KR20120050140A KR20130126221A KR 20130126221 A KR20130126221 A KR 20130126221A KR 1020120050140 A KR1020120050140 A KR 1020120050140A KR 20120050140 A KR20120050140 A KR 20120050140A KR 20130126221 A KR20130126221 A KR 20130126221A
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- South Korea
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- weight
- premix
- parts
- powder
- sikhae
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 34
- 239000000203 mixture Substances 0.000 title claims abstract description 31
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 claims abstract description 56
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- OGNSCSPNOLGXSM-UHFFFAOYSA-N (+/-)-DABA Natural products NCCC(N)C(O)=O OGNSCSPNOLGXSM-UHFFFAOYSA-N 0.000 description 5
- FYGDTMLNYKFZSV-URKRLVJHSA-N (2s,3r,4s,5s,6r)-2-[(2r,4r,5r,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5r,6s)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1[C@@H](CO)O[C@@H](OC2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-URKRLVJHSA-N 0.000 description 5
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- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical class [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/84—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/198—Dry unshaped finely divided cereal products, not provided for in groups A23L7/117 - A23L7/196 and A23L29/00, e.g. meal, flour, powder, dried cereal creams or extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/20—Malt products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2124—Ginseng
Abstract
Description
본 발명은 식혜 프리믹스 조성물 및 식혜 프리믹스를 이용한 식혜의 제조방법이다. 보다 상세한 내용은 식혜분말 조성물의 제조 방법은 보리 엿기름(맥아), 홍삼, 두충 각각의 재료를 기류분쇄기로 15∼35℃의 온도 조건으로 80nm∼45㎛로 입도로 세포벽를 파괴하는 나노입도까지 분쇄하여 이루어지는 공정과, 여기서 얻어진 엿기름 분말 80nm∼45㎛의 홍삼분말, 80nm∼45㎛의 두충분말과 팽화미분, 설탕, 올리고당류, 환원당알콜류, 비타민C, 유기산으로 이루어진 식혜 프리믹스 조성물을 제조하는 방법이다. The present invention is a Sikhye premix composition and a method for producing Sikhye using Sikhye premix. For more details, the method of preparing the Sikhye powder composition is that barley malt (malt), red ginseng, and worms are pulverized to nanoparticle granularity, which breaks down the cell wall with a particle size of 80 nm to 45 μm under a temperature condition of 15 to 35 ° C. It is a method for producing a Sikhye premix composition composed of a malting step powder, 80 nm to 45 μm red ginseng powder, 80 nm to 45 μm soybean meal powder and expanded powder, sugar, oligosaccharide, reducing alcohol, vitamin C and organic acid.
엿기름 성분은 일반적으로 전분 50∼55%, 단백질 11∼12.5%, β-glucan 2∼5%로 구성되어 있으며, 나머지 20%는 수분, 지방, 회분, 섬유소 그리고 소량의 비타민류 등 미량 성분 등을 포함하고 있다. 최근에는 혈압강하(상승억제) 작용 등이 알려진 Gamma Amino Butyric Acid(GABA)도 함유하고 있어 이들 영양 성분이 함유하고 있는 엿기름(맥아)를 나노입도 까지 분쇄하여 식혜를 만들어 유용 물질을 그대로 섭취하기도 한다.Malt is generally composed of 50 to 55% of starch, 11 to 12.5% of protein, and 2 to 5% of β-glucan. The remaining 20% contains water, fat, ash, fiber and trace components such as small amounts of vitamins. It is included. Recently, Gamma Amino Butyric Acid (GABA), which is known to lower blood pressure (suppressive action), also contains nutrients, which contain crushed malt (malt) to `` nano particle size '', which makes it useful for ingesting useful substances. .
본 발명은 식혜를 만들 때 엿기름을 활성화 시켜 추출하는 번거로움을 해소하기 위한 방안을 연구하던 차에 2∼3시간 정도 당화 과정을 거쳐 간편하게 식혜를 만드는 방법을 발명하게 되어 본 발명을 완성하게 되었다. The present invention has been completed the present invention to make a method of making Sikhye easily after going through a saccharification process for about 2 to 3 hours while studying a method for eliminating the hassle of activating and extracting syrup oil when making Sikhye.
전통식품에 대한 관심이 높아지고, 건강식품과 건강기능성식품에 대한 욕구가 증가되면서 천연 식품에 대한 기호가 높아지고 있다. 식혜도 캔 음료로서 시장에서 확고한 위치를 확보하고 있다. As interest in traditional foods increases and the desire for health foods and functional foods increases, the preference for natural foods increases. Sikhye also has a firm position in the market for canned beverages.
식혜의 제조방법은 멥쌀 또는 찹쌀 1㎏에 엿기름 가루 0.5㎏∼1㎏, 적당량(약 1ℓ) 물을 넣어 온도 약 55℃로 2∼3시간 효소를 미리 활성화 시킨 다음 체로 받쳐 엿기름 찌거기를 제거하고, 엿기름액(맥아액)을 만든 후 고두밥(멥쌀을 밥으로 환산) 1.4kg, 물 1∼1.5ℓ를 혼합하여 온도 55∼65℃, 4∼8 시간 동안 몇 개 정도의 밥알이 뜰 때까지 당화시키고 약 5분 정도 끓여 식힌 후 단맛의 기호에 따라 꿀 또는 설탕을 넣어 단맛을 조절하는 것으로 보고되어 있다.Sikhye manufacturing method: 1kg of uncooked rice or glutinous rice, 0.5kg-1kg of starch oil powder, water (approximately 1L), add water (approximately 1L) to the enzyme for 2 hours to 3 hours at 55 ℃, and then sieve it. After making malt liquid (malt liquid), mix 1.4kg of red bean rice (converted from rice into rice) and mix 1 ~ 1.5ℓ of water, and saccharify until several grains of rice grains for 55 ~ 6 ℃ and 4 ~ hours. It is reported to adjust sweetness by adding honey or sugar according to the symbol of sweetness after boiling for about 5 minutes.
이러한 전통적인 식혜 제조법은 효소를 추출하기 위하여 약 2시간 정도 엿기름에서 효소를 추출하는 과정이 있고, 이 추출액에 밥을 4∼8시간 당화시키는 과정을 거쳐야 하는 번거로움이 있다. 상기의 전통적인 식혜제조 방법의 번거로움을 극복하기 위하여 간편한 식혜를 만드는 방법의 개발이 다양하게 이루어져 왔다.This traditional Sikhye manufacturing method has a process of extracting the enzyme from the starch oil for about 2 hours to extract the enzyme, and has to go through the process of glycosylating the rice 4 to 8 hours in this extract. In order to overcome the inconvenience of the traditional method of manufacturing Sikhye has been made a variety of ways to make a simple Sikhye.
식혜를 보다 편리하게 음용할 수 있도록 가공하는 방법은 자동판매기용 분말식혜의 제조방법 (공개특허 1996-33323호), 즉석식혜의 분말과 그의 제조방법는 전분기질에 소정량의 물을 첨가하여 반죽 성형한 다음 팽화기로 팽화시켜 수분함량 5.5∼9.0 % 인 알파화 전분분말을 만드는 단계와 맥아에 드라이아이스를 혼합하고 분쇄하여 맥아분말을 만드는 단계에서 제조된 알파화 전분분말과 제조된 맥아분말에 정제효소, 설탕, 구연산, 아스코르빈산을 혼합하는 단계를 포함하여 구성하는 방법(공개특허 2003-046526), 분말식혜의 제조방법은 엿기름을 물에 침지시켜 상온에서 방치하고 95-100℃의 뜨거운 물로 그 엿기름의 가용성분을 추출시켜 진공 농축한 후 분무 건조하여 분말화 한다(특허공개 1994-0010939), 식혜용 엿기름 티백의 제조방법(공개특허 1999-0084020), 누룽지를 이용한 즉석 감주 제조방법(공개특허 1997-064467) 동결건조한 밥에 엿기름을 첨가하여 세트로 만든 것을 동결건조한 밥을 이용하여 간편하게 제조하는 방법(공개특허 1999-0086234) 고활성 엿기름 티백의 제조 방법은 엿기름 품질을 높이기 위하여 액화(α-아밀라제) 및 (β-아밀라제) 효소의 첨가(등록번호 10-0474977)등이 출원 되어 있다. The method of processing Sikhye to drink more conveniently is a method of manufacturing powdered Sikhye for vending machine (Patent No. 1996-33323), the instant Sikhye powder and its manufacturing method is kneading dough molding by adding a predetermined amount of water to the starch And then swelling with an swelling machine to make an alpha starch powder having a water content of 5.5 to 9.0%, and mixing the dry ice to malt and grinding to make a malt powder. Method comprising the step of mixing sugar, citric acid, ascorbic acid (Public Patent 2003-046526), the manufacturing method of powdered Sikhye is distilled malt in water and left at room temperature and the hot water of 95-100 ℃ Soluble powder of malt is extracted, concentrated in vacuo, concentrated, sprayed and dried to be powdered (Patent Publication 1994-0010939). 99-0084020), Method of preparing instant persimmon liquor using nurungji (public patent 1997-064467) Method of preparing a simple made by adding the malt to lyophilized rice using lyophilized rice (Public Patent 1999-0086234) In order to improve the malt quality, malt tea bags have been applied for the addition of liquefied (α-amylase) and (β-amylase) enzymes (registration No. 10-0474977).
이들 즉석식혜 제조 방법은 간편성을 추구하여 만들어진 발명으로 엿기름 추출액을 이용하거나 액화효소와 당화효소를 첨가하는 기술로 이루어져 있어 맥아에 들어 있는 영양소를 충분히 이용하기 어렵고, 식혜의 맥즙으로 부터 발생되는 향과 깊은맛을 나타내는데 한계가 있다. 또한 엿기름 티백을 이용하는 즉석식혜의 제조방법이 상용화 되어 다행이다.These instant sikhye manufacturing method is an invention made in pursuit of simplicity, and it is difficult to fully use the nutrients in malt, using malt extract or adding liquefied enzyme and glycosylated enzyme. There is a limit to the deep taste. Also, it is fortunate that the method of manufacturing instant snacks using tea bag with tea malt is commercially available.
식혜의 제조방법은 일반적으로 보리나 밀을 발아시켜 엿기름을 제조한 다음, 발아 시켜 제조된 엿기름 속에 함유되어 있는 당화 효소인 아밀라아제로 당화를 시키고, 효소가 물속으로 용출 될 수 있도록 하기 위해 분쇄하게 되어있다. 먼저 제피기를 이용하여 싹과 뿌리 및 껍질을 제거한 다음 20∼80메쉬(약 850∼180㎛)로 엿기름을 조분쇄하며 통상적으로 해머밀로 분쇄시 냉풍을 연속적으로 불어 넣어 온도를 70℃이하로 유지하면서 분쇄시키는 공정으로 이루어져 있다.Sikhye's manufacturing method is to germinate barley or wheat to make malt, and then saccharify with amylase, a glycosylation enzyme contained in malt, which is produced by germination, and then crushed to allow the enzyme to be eluted into water. have. First, the roots and the husks are removed using a kneader, and then the malt is pulverized to 20 to 80 mesh (about 850 to 180 탆). Normally, when the kneaded with the hammer mill, the cold air is continuously blown to maintain the temperature at 70 ° C or lower And crushing it.
조분쇄된 엿기름을 미지근한 물(50∼60℃)에 담가 약2시간 정도 정치한 후 잘 주무르거나 비비고, 체로 받치거나 3∼ 5시간 정체시켜 잔사인 엿기름가루를 가라 안친 다음 맑은 상등액 만을 취하고, 그 상등액의 절반을 증숙된 고두밥과 함께 발효시킨 다음, 나머지 상등액의 반을 마저 붓고 약 10분 정도 가열하여 효소를 실활(失活) 시키는 방법으로 식혜를 제조하여 왔다. 가정에서 식혜를 만들 때에도 불편하게 느끼는 것은 효소 활성화 과정이 번거롭기 때문에 기피하는 경향이 있다.After immersing the coarse malt in lukewarm water (50-60 ℃) for about 2 hours, settle and rub it well, support it with a sieve or stagnate it for 3 to 5 hours to remove the residue, and then remove only the clear supernatant. Half of the supernatant was fermented with steamed gourd rice, and then half of the remaining supernatant was poured and heated for about 10 minutes to inactivate enzymes (失 活). Even at home, making unpleasant feelings tends to be unavoidable because the process of enzyme activation is cumbersome.
보리는 식물섬유 함량이 많고 수용성 식물섬유와 불용성 식물섬유의 균형이 잘 잡혀 있다. 수용성 식물섬유인 β-glucan은 혈중 콜레스테롤 저하 작용을 가지며, 혈당치 상승억제, 면역조절 기능 등의 효과도 기대되고 있다. FDA는 2006년 일정량 이상의 수용성 식물섬유(β-glucan)를 함유한 보리 식품에 관상동맥 심장질환 위험 저감의 강조 표시(FDA21 CFR101.81)를 허가하였다. Barley is rich in plant fiber and well balanced in water-soluble and insoluble plant fibers. Water-soluble plant fiber β-glucan has the effect of lowering cholesterol in the blood, and is also expected to have an effect of inhibiting blood sugar rise and immune regulation. In 2006, the FDA approved a label for reducing the risk of coronary heart disease (FDA21 CFR101.81) for barley foods containing more than a certain amount of water-soluble plant fiber (β-glucan).
보리의 성분은 일반적으로 전분 55∼65%, 단백질 11∼17%, β-glucan 3∼6%로 구성되어 있으며, 나머지 수분 6.5∼8.5%, 기타 지방, 회분, 섬유소, 그리고 소량의 비타민 등 미량 성분 등을 포함하고 있다. 최근 보리에는 혈압강하(상승억제) 작용 등이 알려진 Gamma Amino Butyric Acid(GABA)도 함유하고 있다. GABA 함유량을 높이면 혈압상승 억제효과도 기대되고, 대사증후군(metabolic syndrome)억제로서 더욱 유효한 소재가 될 것으로 기대하고 있다.Barley is generally composed of 55 to 65% of starch, 11 to 17% of protein, and 3 to 6% of β-glucan, remaining 6 to 5 to 5% of water, other fats, ash, fiber, and small amounts. And trace components such as vitamins. Recently, barley also contains Gamma Amino Butyric Acid (GABA), which is known to lower blood pressure. Increasing the GABA content is expected to suppress the increase in blood pressure, and is expected to be a more effective material for suppressing metabolic syndrome.
보리와 맥아 추출물에는 강력한 산화 방지 활성으로 야채, 과일의 높은 산화 방지 활성이 있다. 이것은 페놀 수지 화합물이 무수히 포함되어 있다는 사실을 증명하고 있다. 또는 보리의 맥즙을 이용하는 맥주 경우에도 탄수화물, 단백질, 폴리펩티드, 미량원소를 제공하는 중요한 원료 중 하나로 널리 알려져 있다.Barley and malt extract have strong antioxidant activity and have high antioxidant activity of vegetables and fruits. This proves that a myriad of phenolic resin compounds are included. Beers that use barley wort are also widely known as one of the important sources of carbohydrates, proteins, polypeptides and trace elements.
보리를 엿기름(맥아)으로 제조하기 위하여 침맥하여 발아를 시키는 과정 중에 전분질 배유부가 가수 분해되어 변형되는데 이는 보리의 호분 층 세포에서 가수분해 효소들이 합성되어 호분 층 세포벽으로 부터 배유로 분비됨에 따른다. 이때 보리의 세포벽 분해가 전분의 분해에 앞서 진행되는데 발아 중에 세포벽을 구성하고 있는 대표적인 구조적 다당류 물질인 β-glucan과 arabinoxylan을 분해시키는 β-glucanase와 xylanase와 같은 세포벽 분해효소의 작용이 일어나고 배유 전분질을 분해하는 효소인 α-amylase와 β-amylase의 작용이 계속적으로 진행된다. 보리에 수분을 가해 싹을 튀운 엿기름에는 전분 분해 효소인 α-amylase, β-amylase, glucoamylase 등이 있으며, α-amylase는 전분의 α-1,4-결합을 무작위로 가수 분해시키는 효소로 휴지 상태의 보리에는 존재하지 않으나 발아할 때 생성된다. 또한 보리가 발아할 때 지베렐린 유사 물질인 gibberellic acid(GA3)가 생성되어 배유로 이송되면서 α-amylase, β-amylase, β-glucanase, xylanase, protease, cellulase의 활성 및 생성을 촉진시킨다. 이때 일부는 잠재형 zymogen β-amylase로 존재하며, 이들은 덩어리로 묶여있기 때문에 효소로서 작용하지 못하지만 발아, 즉 싹을 틔우는 과정을 통하여 각 효소 사이를 묶고 있던 결합이 절단되면 그때에 비로소 효소로서 작용하게 된다. 엿기름의 품질과 보리 품질의 상관관계는 엿기름 제조와 양조의 생화학에 관해서는 맥아를 만드는 과정과 분쇄하여 열수에 담그는 과정에서 생화학 반응의 가장 중요한 점은 전분 분해, 단백질 가수분해, 세포의 분해이다. 전분 분해시 사용되는 맥아 효소는 α-amylase, β-amylase, 가지분해효소(debraching enzyme), α-glucosidase, β-fructosidase, phosphoylrase, glucoiltransferase 등 이다. α-amylase, β-amylase의 최적 pH는 5.7과 5.3이고, 최적 온도는 55∼65℃와 50∼60℃이다. 생화학적인 측면에서 엿기름 발아(제맥)과 분쇄는 열수 추출하여 이용하는 방법에서 엿기름을 이용한 식혜 제조 과정에서 보리 중에 있는 생리활성 물질을 효율적으로 섭취하느냐는 중요한 연구 대상이라고 본다. In order to produce barley as malt (malt), the starch endosperm is hydrolyzed and deformed during the process of acupuncture and germination, which is followed by the synthesis of hydrolytic enzymes in the basal layer cells of barley and secreted into the endosperm from the cell wall. At this time, the cell wall decomposition of barley proceeds prior to the decomposition of starch. During germination, the action of cell wall degrading enzymes such as β-glucanase and xylanase, which break down the representative structural polysaccharides constituting the cell wall and β-glucan and arabinoxylan, takes place. The action of degrading enzymes α-amylase and β-amylase continue to proceed. Malt, which has been sprouted by hydrating barley, contains starch degrading enzymes such as α-amylase, β-amylase, and glucoamylase, and α-amylase is an enzyme that randomly hydrolyzes the α-1,4-linkage of starch. It does not exist in barley but is produced when it germinates. In addition, when barley germinates, gibberellic acid (GA3), a gibberellic-like substance, is produced and transported to endosperm, promoting the activity and production of α-amylase, β-amylase, β-glucanase, xylanase, protease, and cellulase. At this time, some exist as latent type zymogen β-amylase, and because they are bound together, they do not act as enzymes, but when they break through the germination, ie, sprouting, the bonds between the enzymes are broken. do. The correlation between malt quality and barley quality of starch oil is the starch decomposition, protein hydrolysis, and cell breakdown in the production of malt and biochemistry of brewing. Malt enzymes used for starch degradation are α-amylase, β-amylase, debraching enzyme, α-glucosidase, β-fructosidase, phosphoylrase, and glucoiltransferase. The optimum pH of α-amylase and β-amylase is 5.7 and 5.3, and the optimum temperature is 55-65 ° C and 50-60 ° C. In terms of biochemical aspects, malt oil germination (milling) and milling are considered as important research subjects to efficiently ingest bioactive substances in barley during the process of extracting hydrolyzed oil using syrup oil.
하기 표 1과 같이 발아하는 보리의 품질 특성 중 효소의 활성은 매우 중요하며, 적절한 발아 조건의 확립은 엿기름을 제조할 때 품질의 절대적인 요소가 되며, 생성된 효소를 효율적으로 이용하는 것이 식혜의 품질을 결정한다. 앞으로 보리 중에 있는 식이섬유의 효율적 이용을 통한 식혜음료의 연구도 필요하다.As shown in Table 1 below, the activity of enzymes is very important among the quality characteristics of barley germinating, and the establishment of proper germination condition is an absolute factor of quality in the production of malt, and the efficient use of the produced enzymes makes the quality of Sikhye Decide. There is also a need for further research on dietary beverages through efficient use of dietary fiber in barley.
엿기름을 약 50∼60℃의 열수 추출로 유용물질을 효과적으로 이용하는 데는 한계가 있다. 본 발명에서는 보리에 들어 있는 효소, 식이섬유,단백질,펩타이드,무기질,비타민을 최대로 활용 할수 있도록 기류분쇄기를 이용하여 15∼35℃ 온도조건으로 80nm∼45㎛ 나노입도로 분쇄하여 세포막을 파괴하고, 식혜 프리믹스 조성물은 엿기름의 효소 활성을 높이기 위하여 가정에서 물을 혼합하면 효소 활성 최적 pH가 되도록 완충제의 역할이 필요하다. 음료로써 기능을 강화하기 위하여 홍삼과 강장제의 역할을 하는 천연 홍삼과 두충으로 이루어진 건강기능성 소재를 배합하여 음료와 기능성식품을 동시에 섭취하여 건강 증진에 도움을 주고 자 한다.
There is a limit to the effective use of the useful material by extracting the malt from the hot water of about 50 ~ 60 ℃. In the present invention, using the air pulverizer to maximally utilize enzymes, dietary fibers, proteins, peptides, inorganic substances, and vitamins contained in barley to break the cell membrane by grinding to 80nm ~ 45㎛ nanoparticles at 15 ~ 35 ℃ temperature conditions In order to increase the enzyme activity of malt, Sikhye premix composition needs the role of a buffer so that the optimum pH of the enzyme activity when water is mixed at home. In order to enhance the function as a drink, by combining the health functional material consisting of red ginseng and natural red ginseng and tofu as a tonic, it is intended to help improve health by ingesting drinks and functional foods at the same time.
상기와 같은 목적을 달성하기 위하여 본 발명의 즉석식혜 프리믹스 조성물 제조방법은, 기류분쇄기로 엿기름을 분쇄하는 단계와, 음료로써 기능성을 강화하기 위하여 첨가되는 건조홍삼, 건조두충을 분쇄하는 제1분말제조공정과, 팽화미분에 제1분말 제조공정에서 얻어진 엿기름분말, 정제효소, 홍삼분말, 설탕, 올리고당, 아스팔탐, 구연산, 토코페롤을 고속 분체 믹서기로 혼합하여 분말로 이용하거나 과립화하는 제2프리믹스 제조공정으로 이루어 진다. 또한 제2공정 프리믹스 제조공정에서 알파미를 제외하고 혼합하여 얻어진 제품을 제3프리 제조공정으로 한다. 제2공정에서 얻어진 식혜프리믹스 조성물에 물을 1:40∼80비율로 가한 후 온도 58±0.2℃로 2∼5시간 당화 시킨 후 90∼100℃로 30초∼2분 가열하여 미분해 전분의 호화 및 효소를 실활 시키는 단계로 이루어진 간편한 식혜의 제조 방법이다.
In order to achieve the above object, the instant food preparation premix composition preparation method of the present invention comprises the steps of pulverizing malt with an airflow mill, and preparing a first powder for pulverizing dried red ginseng and dried tofu which is added to enhance functionality as a beverage. Preparation of the second premix which mixes the malt powder, refined enzyme, red ginseng powder, sugar, oligosaccharide, aspartame, citric acid and tocopherol obtained in the first powder manufacturing process with the expanded powder, using a high-speed powder mixer or granulate. The process is done. In addition, the product obtained by mixing except alphami in the 2nd premix manufacturing process is made into the 3rd prefabrication process. Water was added to the Sikhye premix composition obtained in the second step at a ratio of 1:40 to 90%, then saccharified for 2 to 5 hours at a temperature of 58 ± 0.2 ° C, and then heated to 90 to 100 ° C for 30 seconds to 2 minutes to produce undigested starch. The preparation of the simple Sikhye made of gelatinization and deactivation of the enzyme.
엿기름의 유용한 영양을 간편하게 섭취하기 위해서 엿기름, 홍삼, 두충을 나노입도(80nm∼45㎛)까지 분쇄하여 그대로 당류, 효소류, 유기산류, 비타민류와 함께 프리믹스 조성물을 만들어 식혜를 제조하므로 당화력이 증강되고, 영양 성분이 식혜로 이용 되도록 하는 방법이다. 기존의 50∼60℃ 효소를 활성화 하는 방법은 식물 조직내의 cellulose fibril 때문에 중심에 침투 할수 없기 때문에 추출 수율이 낮다. 본 발명에서는 나노입도로 분쇄하여 세포벽을 파괴하여 투과성(permeability)을 증가시켜 추출물의 수량을 높일 수 있고, 나도 입도까지 분쇄하여 맥아 성분을 당화과정을 통하여 그대로 식혜 음료로 이용할 수 있다.
In order to easily consume the useful nutrients of malt, malt, red ginseng, and worms are pulverized to nanoparticle size (80nm ~ 45㎛), so that sugars, enzymes, organic acids, and vitamins are prepared together with the premix composition to make Sikhye. It is a way to make use of nutritional ingredients. Existing methods for activating enzymes at 50 ~ 600 ℃ have low extraction yield because they cannot penetrate into the center due to cellulose fibril in plant tissues. In the present invention, by crushing the nanoparticles to break the cell wall to increase the permeability (permeability) to increase the yield of the extract, I can also be used as a Sikhye drink through the malt component by grinding to the particle size.
도 1은 본 발명의 제조공정을 나타낸다.
도 2는 건조 엿기름 등 혼합물의 기류 분쇄 입도분포이다.1 shows a manufacturing process of the present invention.
2 is a particle size distribution of a stream of air mixture such as dried malt.
본 발명은 프리믹스 분말을 제조하는 공정과, 프리믹스를 제조하는 공정과, 팽화미분를 제외하는 프리믹스를 이용하여 식혜를 제조하는 공정으로 구성된다.
The present invention comprises a process for producing a premix powder, a process for preparing a premix, and a process for producing Sikhye using a premix except for expanded powder.
〈프리믹스 분말 제조 〉〈Premix Powder Manufacturing〉
기류분쇄기(Micro Ferm Co., model MD-101, korea)를 뿌리, 배아, 껍질을 제피한 시판 엿기름(김포맥아식품, 대주식품)에서 당화력이 양호한 품질을 고려하여 2개 업체를 선별하여 1:1.0∼1.5 비율로 혼합한 엿기름과 홍삼, 두충 각각의 온도 15∼35℃의 조건으로 80nm∼45㎛ 분쇄하여 엿기름 분말, 홍삼분말, 두충 분말을 제조한다.이 때의 분쇄 온도 때문에 효소의 실활 방지를 위하여 15∼35℃로 미분쇄하여 사용하는 것이 중요하다. 일반적으로 기류분쇄기는 운전 시간에 따라 점차 온도가 상승하게 되고, 기류분쇄기 내의 품온이 약50℃를 초과하는 경우도 있다.
Micro Ferm Co. (model MD-101, korea) was used to select two companies from the commercial malt (Gimpo Malt Food, Daeju Food), which had been stripped of roots, embryos, and shells. Malt powder, red ginseng powder, and Tofu powder are prepared by grinding 80 to 1.5 µm of malt, red ginseng, and tofu mixed with each other at a ratio of 1.0 to 1.5 at a temperature of 15 to 35 ° C. In order to prevent inactivation of the enzyme, it is important to use the finely ground at 15∼35 ℃. In general, the temperature of the air mill is gradually increased with the operation time, the product temperature in the air mill may exceed about 500 ℃.
〈프리믹스의 제조〉 <Premix>
Extruder로 제조한 팽화미분(삼창산업)100중량부에 프리믹스분말 제조공정에서 얻어진 엿기름분말 20∼60중량부, 홍삼분말0.1∼5.0중량부, 두충분말 0.1∼3.0중량부, 말토게닉아밀라제(Novoenzyme)0.04∼0.08중량부, Pullunase(Novoenzyme)0.02∼0.09중량부, 설탕 10∼70중량부, 올리고당1.0∼10중량부, 아스팔탐 0.05∼0.2중량부, 구연산 0.05∼0.5중량부, 토코페롤 0.5∼1.0중량부를 고속 분체 믹서기로 혼합하는 공정 또는 과립으로 제조한다.
100 parts by weight of expanded powder made by extruder (Samchang Industries) 20 to 60 parts by weight of malt powder obtained by the premix powder manufacturing process, red ginseng powder by 0.01 to 5.0 parts by weight, and two to three parts by weight Part, Maltonic amylase (Novoenzyme) 0.04 to 0.000 parts by weight, Pullunase (Novoenzyme) 0.02 to 0.000 parts by weight,
<프리믹스를 이용한 식혜의 제조><Production of Sikhye using premix>
프리믹스 제조공정에서 얻어진 제품을 프리믹스 조성물 100중량부에 물 80∼170중량부를 가하여 pH 5.6∼5.9, 온도 60℃에서 4시간 당화시켜 식혜를 제조한다.
Sikhye is prepared by adding 80 to 70 parts by weight of water to 100 parts by weight of the premix composition, and then saccharifying for 4 hours at a pH of 5.6-5.9 and a temperature of 60 ° C.
〈실시예1〉; 프리믹스 분말의 제조<Example 1> Preparation of Premix Powder
분쇄입도별 효소 활성을 조사하기 위하여 기존 시판 엿기름 중에서 뿌리, 배아, 껍질을 제피한 제품(대주식품)을 본 발명의 분쇄 장치인 기류분쇄기(Micro Ferm model MTM - 101)로 15∼35℃의 온도에서 분쇄한 제품과 비교 분석하였다(도 2 참조).In order to investigate the enzyme activity according to the particle size, a micro-ferm grinder (Micro Ferm model MTM-101) of the present invention, which is a product (Taju) that avoids roots, embryos, and shells from existing commercial syrup oil, has a temperature of 15 ~ 35 ℃. The product was analyzed in comparison with the crushed product (see FIG. 2).
입도분포의 측정 : 표준체를 이용하여 시료 100그램을 로탑 진동체(바이브로 코리아)로 분석하였다. 나노 입도로 분쇄 된 발명품의 입도는 나노입도의 분석이 가능한 입도기(HELOS Particle Size Analyzer Model WINDOX 5)를 사용하였다.Measurement of particle size distribution: A sample of 100 grams was analyzed with a tower vibrator (Vibro Korea) using a standard. The particle size of the invention, which was pulverized into nanoparticles, was used for the particle size analysis (HELOS Particle Size Analyzer Model WINDOX 5).
Diastatic Power(DP) 의 당화력 : 분쇄된 시료 5그램을 채취하여 AACC방법으로 측정 하였다.Glycosylation Power of Diastatic Power (DP): Five grams of ground samples were taken and measured by AACC method.
β-Amylase = 0.5그램의 시료를 Betamyl β-Amylase assay kit (Megazyme, Ireland)를 이용하여 분석.β-Amylase = 0.5 grams of samples were analyzed using the Betamyl-Amylase assay kit (Megazyme, Ireland).
α-Amylase = 0.5그램의 시료를 Ceralpha α-Amylase assay kit Megazyme, Ireland)를 이용하여 분석.α-Amylase = 0.5 grams of samples were analyzed using the Ceralpha α-Amylase assay kit Megazyme, Ireland.
〈실시예2〉; 프리믹스 조성물의 제조<Example 2> The manufacture of a premix composition
시판 팽화미분(삼창산업)100중량부에 엿기름분말 40중량부, 말토게닉아밀라제(Novo사) 0.06중량부, 풀루나아제(Novo사)0.09중량부, 홍삼분말 0.5중량부, 두충분말 0.3중량부, 설탕 12중량부, 올리고당 3.0중량부, 아스파탐 0.05중량부, 구연산 0.05중량부, 비타민C 0.07중량부, 토코페롤 0.5중량부 을 고속 분체 믹서기로 혼합한다.
Commercially-expanded fine powder (Samchang Industries) 100 parts by weight of the
<실시예 3> ; 프리믹스를 이용한 식혜의 제조 <Example 3>; Preparation of Sikhye Using Premix
실시예 2와 동일하게 만든 프리믹스를 100중량부에 대하여 물 150중중량부를 넣고 pH 5.8, 온도 60 ℃에서 4시간 동안 당화시키면서 매시간 일정량의 시료를 취하여 2분간 끓이고 냉각한 후 25℃에서 이화학적 및 관능적 품질을 평가하였으며 다음 표 4 및 표 5에 나타낸 바와 같다.Prepare 100 mg by weight of premixed water in the same manner as in Example 2, add 일정 15 weight parts of water, and pH5. The physical and sensory qualities were evaluated and are as shown in the following Tables 4 and 5.
대조구의 식혜는 엿기름 300g(대주식품)에 물 1.2ℓ와 혼합하여 60℃ 항온수조에서 2시간 침출 후 여과하여 엿기름 추출액을 만들어 사용하였다. 엿기름 추출액에 고두밥 1.4kg와 혼합하여 60℃에서 당화 후 5분간 끓이고 냉각한 후 25℃에서 관능평가의 대조구로 사용하였다.Sikhye of control was mixed with 1.2l of water in 300g of malt oil (Daeju Food), and leached in a 60 ℃ constant temperature water bath for 2 hours and filtered to make malt extract. The malt extract was mixed with 1.4kg of soybean rice, saccharified at 6 ° C, boiled for 5 minutes, cooled, and used as a control for sensory evaluation at 25 ° C.
당도: hand refractometer(Model N-1E, Atago, Tokyo, Japan)를 이용하여 측정Sugar content: measured using a hand refractometer (Model N-1E, Atago, Tokyo, Japan)
색도: Hunter 색차계(Minolta CT-310, Tokyo, Japan)를 이용하여 L, a, b값으로 측정이 되나 a 값을 기준으로 분석.Chromaticity : Measured by L, a, b values using a Hunter color difference meter (Minolta CT-310, Tokyo, Japan), but a value is analyzed based on a value.
PH: 당화 제조과정 중의 pH는 pH meter(Satrious, PB-101,Germany)로 측정PH: pH during saccharification and manufacturing process is measured by pH meter (Satrious, PB-101, Germany)
탁도: 식혜물의 탁도는 spectrophotometer(U-2000, Hitachi, Japan)를 사용하여 파장 600 nm에서 투과도(transmittance)를 측정.Turbidity: The turbidity of fresh fruits is measured using a spectrophotometer (U-2000, Hitachi, Japan) at 600 nm wavelength.
(대조품대비)evaluation
Of control
*관능평가는 판넬요원 남 4명, 여 6명(20대 남 2명, 여 2명,30대 남 1명, 여 2명, 40대 남 1명, 여 2명)구성하여 선호도 위주로 평가.
* The sensory evaluation consisted of 4 panelists, 6 females (2 males in 20s, 2 females, 1 female in 30s, 1 male, 2 females, 1 female in 40s, and 2 females).
종래 엿기름(맥아)의 일부 효소와 수용성 아미노산, 비타민을 열수 추출하여 이용하던 방식을 나노입도로 분쇄하여 사용하므로서 세포내 잠재형 zymogen β-amylase까지 활용으로 효소의 역가를 높히고,석이섬유, GABA 성분, 펩타이드, 아미노산, 비타민 등 생리활성 물질 의 유용성분을 식혜음료로 음용할수 있다.By using some of the enzymes, water-soluble amino acids, and vitamins of malt, malt extracts are used to crush them into nano-particles, they increase the potency of enzymes and increase the potency of enzymes in the cells. Useful ingredients of physiologically active substances such as peptides, amino acids and vitamins can be taken as food and beverages.
본 발명은 맥아효소 추출과정의 번거로움을 해결하여 각종 맥즙의 응용을 통한 식품에의 이용이 기대되고, 천연적으로 이루어진 기능성 식혜음료를 간편하게 만들 수 있는 프리믹스의 조성물이다.The present invention is a composition of a premix that can solve the hassle of the malt enzymatic extraction process is expected to be used in food through the application of various types of wort juice, and can easily make a functional food and beverage made naturally.
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