KR20130120961A - Hydrogen rich distilled liquor and its method of manufacture - Google Patents

Hydrogen rich distilled liquor and its method of manufacture Download PDF

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KR20130120961A
KR20130120961A KR1020120044217A KR20120044217A KR20130120961A KR 20130120961 A KR20130120961 A KR 20130120961A KR 1020120044217 A KR1020120044217 A KR 1020120044217A KR 20120044217 A KR20120044217 A KR 20120044217A KR 20130120961 A KR20130120961 A KR 20130120961A
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South Korea
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hydrogen
soju
water
distilled liquor
storage tank
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KR1020120044217A
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Korean (ko)
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김일봉
박인철
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김일봉
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/08Preparation of other alcoholic beverages by methods for altering the composition of fermented solutions or alcoholic beverages not provided for in groups C12G3/02 - C12G3/07

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)

Abstract

The present invention relates to distilled liquor in which hydrogen is dissolved and a manufacturing method of the same. The manufacturing method of the distilled liquor for dissolving hydrogen to the high concentration comprises the following: diluting spirit using processing water, before deodorizing and purifying; and locating an electrolysis device on the lower side of a storage tank filled with distilled liquor undiluted alcohol containing food additives, and locating a compressing and dissolving device on one side of the storage tank for the electrolysis of the distilled liquor by the electrolysis device and the dissolution of separate hydrogen by the compressing and dissolving device. A complex hydrogen dissolution method by the present invention is capable of easily being applied to an existing distilled liquor production process without any changes, and the hydrogen dissolved in the high concentration has excellent preserving force for storing the distilled liquor for a long time in a bottle. The distilled liquor produced by the present invention has excellent functionality and soft texture compare to regular distilled liquor by reducing the size of clusters of the processing water, and has an activated oxygen removal function and a detoxification function of the dissolved hydrogen for offering a fast hangover relieving effect. [Reference numerals] (AA) Original water from the water source;(BB) Filtering;(CC) 95% ethyl alcohol;(DD) Dilution solvent;(EE) First dilution;(FF) 40-60% diluted ethyl alcohol;(GG) Activated carbon deodorization, Filtering;(HH) Second dilution;(II) 20-25% final diluent;(JJ) Food additive mixing, filtering;(KK) Sojunaju (distilled liquor with high hydrogen concentration), Storage tank;(LL) Electrolysis device's electrolysis, Hydrogen dissolving by a compressing and dissolving device;(MM) Soju (Korean traditional liquor) with high hydrogen concentration;(NN) Bottle package, Commercialization

Description

Hydrogen-rich soju and its method of manufacture {Hydrogen rich distilled liquor and its method of manufacture}

The present invention relates to a method for preparing soju, which dissolves hydrogen at a high concentration. In particular, the present invention relates to a method for preparing hydrogen-rich shochu, which dissolves hydrogen at a high concentration without significant change in the existing soju manufacturing process, and maintains a high concentration of dissolved hydrogen even after time. It is about a method.

In general, a lot of hydrogen, aka hydrogen rich water is known to be excellent in the prevention and treatment of adult diseases, such as cancer or diabetes, and recently it is known at home and abroad, and research on this is being actively conducted. This is the result of analyzing the Lourdes fountain in France, known as the miracle water, the Nordenau water in Germany, and the Tracote water in Mexico, which have been known since 1990, and the concentration of dissolved hydrogen is generally 0.3 ~ 1ppm. Hundreds of times more dissolved hydrogen was found to be water. (Excerpt: Hydrogen water, now under the hydrogen water age by Dr. Eun Sang Sang, 2009, published by Health Newspaper) The medical and industrial sectors have been studying how to artificially produce hydrogen rich water that is effective for various adult diseases.

On the other hand, according to the change of alcohol consumption culture, the soju that consumers prefer is the soju that has a soft taste and quick hangover elimination characteristics by lowering the alcohol content. In line with these demands, technologies for using alkaline water, which is beneficial to the body, for the health of consumers are being developed. As such technology, alkaline reduced water obtained by electrolyzing water is disclosed in Korean Patent No. 0618329. The method of producing soju has been disclosed, which is used as a method, and in Korean Patent Publication No. 10-0664599 (the method of preparing distilled soju containing oxygen), the oxygen is dissolved as much as possible while preventing the release of oxygen to greatly increase the hangover after drinking. Disclosed is a dilute shochu containing relieving hydrogen.

However, alkali-reduced soju has recently become a major concern for the digestive system such as gastric ulcer caused by excessive acid-reduced gastric acid. Compared to 80ppm, the oxygen solubility contained in soju is 50ppm or less, and it is difficult to theoretically prove its effectiveness because it is impossible to diffuse into blood vessels.

Therefore, the present inventors invented a method for producing hydrogen rich shochu by dissolving hydrogen at a high concentration without significant change in the existing shochu manufacturing process using the results of devising the Republic of Korea Utility Model 20-0459135 portable hydrogen rich water production apparatus.

The present invention produces hydrogen-rich water by electrolyzing the detergent water with an electrolytic apparatus during the soju manufacturing process known in the shochu manufacturing industry, and pressurizing and dissolving hydrogen produced separately in dilute shochu mixed with alcohol and the detergent water at a predetermined concentration. It is an object of the present invention to provide a method for producing hydrogen rich soju, which can be dissolved in a high concentration by dissolving through an apparatus.

The method for producing hydrogen rich soju of the present invention

(a) filtering raw water from the intake source to produce the sacrificial water;

(b) blending casting water to 95% by volume of alcohol to produce 40-60% by volume of distilled alcohol and deodorizing it in an activated carbon treatment tank;

(c) adjusting the final alcohol concentration to 20-25% by volume by mixing the distilled spirit of step (b) with the distilled water of step (a);

(d) preparing a soju or liquor by filtering the mixed solution prepared by preparing a food additive in a syrup form in the final dilution of the step (c);

(e) Electrolyzing device in the soju or jujube storage tank of step (d) to electrolyze soju or soju directly to dissolve hydrogen, and construct a pressurized dissolution device connected to the tank to dissolve the extra hydrogen in soju and soju Preparing a high concentration of hydrogen rich shochu;

(f) transferring the hydrogen-rich soju of the step (e) to a bottling process to produce a high concentration of hydrogen-rich soju.

According to the present invention, there is provided a method for producing hydrogen-rich shochu liquor capable of dissolving hydrogen at a high concentration without significant change in the existing soju manufacturing process. Furthermore, as the cluster of water becomes smaller as a result of the electrolysis of the water, the taste is soft and soft. The dissolved hydrogen promotes rapid hangover and metabolism after drinking, so that alcohol is rapidly decomposed or consumed.

1 is a manufacturing method of hydrogen rich shochu to dissolve hydrogen of the present invention at high concentration.
Figure 2 is a configuration of the sojunaju storage tank including the hydrogen dissolved device of the present invention
Figure 3 is a schematic diagram of the electrolytic device for hydrogen coupled to the storage tank of the present invention
Figure 4 is a configuration diagram of the pressure dissolved dissolution device for hydrogen coupled to the storage tank of the present invention

The production of functional soju is very closely related to the preparation of functional water. That is, the production of alkaline reduced water soju is prepared by mixing alkaline reduced water as the detergent water of the shochu production process disclosed in the industry, and oxygen soju is prepared by dissolving oxygen in the detergent water in various ways. Recently, there is a hydrogen-rich water as a functional water, which is the most powerful reducing material, hydrogen is very effective in removing the active oxygen in the somatic cells that account for 90% of the disease causes a number of excellent pathological results have been reported continuously. Therefore, if you prepare a functional shochu containing hydrogen-rich water, it is possible to effectively remove the toxic substances of the hangover and aldehydes generated in the alcohol decomposition process of the liver as well as taste.

Applicant has devised a portable hydrogen-rich water production apparatus to the utility model (registration number 20-0459135)

As registered, invented a method for producing hydrogen-rich soju using the devised technology.

Hereinafter, with reference to Figure 1 with respect to the manufacturing method of the hydrogen-rich soju of the present invention will be described.

(a) step: preparing the sacrificial water

Since it is necessary to remove the foreign substances such as protozoa and sand contained in the raw water sent from the intake source is performed through a filtration device, it can be carried out using an activated carbon filtration tank or ultra-precision filtration device. This is a method known in the liquor industry, activated carbon filtration using a column filtration tank, ultra-precision filtration using a cartridge filter, etc., the pore size of the filtration membrane is 20 ~ 5 grade.

(b) step: preparing a diluted alcohol

95% by volume of the spirits prepared in step (a) is formulated with distilled water, diluted to 40-60% by volume, and activated carbon is added to the diluted alcohol and deodorized. The deodorization is performed by adding 500-1,000 ppm by weight of activated carbon in the activated carbon treatment tank and left for 2-4 hours. After deodorization, the activated carbon and the diluted alcohol are separated through ultra-precision filtration with a pore size of 0.1-10.

(c) step: preparing a final diluent

Formulation water of step (a) is added to the dilution spirit in the second step to adjust the final alcohol concentration to 20-25% by volume to prepare a final dilution.

(d) step: preparing soju or sake

In order to improve the taste of shochu in the final dilution solution, 5 to 6 or more food additives, such as salt, aspartic acid, amino acid, stevioside, sugar, glucose, citric acid and sugar alcohol, are mixed in 0.001 to 0.5% by weight, respectively. After preparing and adding the filtered sojunaju through a filter to prepare.

(e) step: hydrogen rich soju production step

The soju naju 10 is directly electrolyzed by the electrolytic apparatus 102 configured under the storage tank 100 to generate hydrogen at the negative electrode plate 102-1 to be dissolved in the soju naju. In addition, by dissolving the hydrogen in the form of a separate micro-bubble by the pressure dissolved device 101 is connected to one side of the storage tank with the dissolved hydrogen by the electrolysis, soju Naju 10 is a high concentration of hydrogen rich soju Change.

Referring to FIGS. 2 and 3, the electrolytic device 102 configured below the storage tank 100 will be described in detail. The electrolytic device 102 is the applicant's portable hydrogen rich water production apparatus utility model (registration number 20-0459135). Produced by expanding the electrolytic device devised in, 102 configuration of the electrolytic device is a negative electrode (102-1); Positive electrode 102-2; Polymer ion exchange resin film 102-3; Gasket 102-4; Tank base 103; Float valve 103-1; A power supply 104. When the soju naju 10 is filled in the storage tank 100, the negative electrode 102-1 of the electrolytic apparatus 102 is immersed in the soju naju 10, and the positive electrode 102-2 of the electrolytic apparatus 102 is a water tank. Submerged in the purified water 20 in the base, by the polymer ion exchange resin film (102-3) and the gasket (102-4), the sojunaju 10 is kept airtight, there is no leakage, the purified water 20 of the tank base The water level is always maintained at a constant level by the water level blocking function of the float valve 103-1 while being fed through the faucet. The power supply 104 typically generates a direct current of several tens of volts or less, and the following electrolysis reaction occurs when the direct current of the negative electrode 102-1 and the positive electrode 102-2 of the electrolytic device 102 is applied.

(Anode) 2H 2 O (l) = O 2 (g) + 4e - + 4H + (aq)

(Cathode) 4H + (aq) + 4e- = 2H 2 (g)

Oxygen gas is emitted from the anode by the reaction formula and dissolved in the purified water 20 in the tank base or dispersed in the gas phase in the upper space to escape to the outside air, and the chlorine component contained in the water is combined with dissolved oxygen and hypochlorous acid or dioxide. An oxidizing agent such as chlorine is generated, and such materials have bactericidal power, thereby preventing contamination of water in the tank base 103. Dissolved hydrogen ions generated in the anodic reaction move to the cathode through the polymer ion exchange resin film, and receives the electrons from the negative electrode 102-1, hydrogen gas is generated, and the hydrogen gas has a high solubility in water so that the negative cup ( 100) generated in the form of bubbles in the lower part is dissolved in most of the soju or liquor 10 during the ascension to the top to produce hydrogen-rich shochu.

In addition, referring to Figures 2 and 4, a separate pressure dissolving device 101 will be described in detail, the pressure dissolving device 101 comprises a pressure pump 101-1 by constituting a circulation passage on one side of the storage tank 100; Venturi mixer (101-2); Dissolved tube 101-3; It consists of the hydrogen container 101-4. When the hydrogen container 101-4 is connected to the gas inlet side of the venturi mixer 101-2, and the pressure pump 101-1 is operated, the soju-naju 10 is pressurized and dissolved in the circulation path 101. When the soju naju 10 passes the throttle of the venturi mixer 101-2 at high speed, negative pressure is generated, and hydrogen is sucked from the hydrogen container 101-4 to the venturi mixer 101-2. It enters and mixes in the soju naju 10 on a micro bubble. Thereafter, while passing through the narrow and long flow path of the dissolved tube 101-3, the microbubbles of hydrogen are completely dissolved in the soju naju 10, and are discharged to the storage tank 100. As such, the electrolytic device 102 and the pressure dissolving device 101 may be operated at the same time, so that the soju naju 10 filled in the storage tank 100 may be dissolved in high concentration within a short time, and the dissolved hydrogen concentration is maintained for a long time. Hydrogen-rich shochu with the characteristics that can be produced is produced.

(f) step: hydrogen-rich shochu bottled productization step

Hydrogen-rich soju is transferred to the bottling process from the storage tank 100 of the above process, but bottled into a product, it is preferable to bottle in a color bottle that can block sunlight such as green, brown, blue.

100: storage tank 101: pressure dissolved device 101-1: pressure pump
101-2: Venturi mixer 101-3: Dissolved tube 101-4: Hydrogen container
102 electrolytic device 102-1 negative electrode 102-2 positive electrode
102-3: polymer ion exchange resin film 102-4: gasket 103: water tank base
104: power supply device 10: sojunaju 20: water purification

Claims (6)

In shochu liquor mixed with filtered alcoholic alcohol and adjusted to any alcohol concentration,
The soju naju 10 filled in the storage tank 100 is directly electrolyzed by the electrolytic apparatus 102 configured under the storage tank 100 so that hydrogen generated at the negative electrode plate 102-1 is dissolved in the soju naju, At the same time, the hydrogen-rich shochu production method, characterized in that to produce a high concentration of hydrogen-rich shochu by dissolving the separate hydrogen in the soju Naju by micro-bubble pressure pressurizing device 101 is connected to one side of the storage tank.
The method of claim 1,
The electrolytic device 102 includes a negative electrode 102-1; Positive electrode 102-2; Polymer ion exchange resin film 102-3; Gasket 102-4; Tank base 103; Float valve 103-1; Consists of a power supply 104, when the soju naju 10 is filled in the storage tank 100, the negative electrode 102-1 of the electrolytic apparatus 102 is immersed in the soju naju 10, the electrolytic apparatus 102 The positive electrode 102-2 is immersed in the purified water 20 in the tank base, sojunaju 10 is kept airtight by the polymer ion exchange resin film 102-3 and the gasket 102-4, there is no leakage When the water supply base 20 of the water tank base 103 is supplied with water, the constant water level is maintained by the float valve 103-1, and the power supply 104 is connected to the negative electrode 102-1 and the positive electrode 102-2. Hydrogen-rich shochu production method characterized by supplying a direct current electricity
The method of claim 1,
The pressure dissolving device 101 constitutes a circulation flow path at one side of the storage tank 100 to pressurize the pump 101-1; Venturi mixer 101-2; Dissolved tube 101-3; Hydrogen rich shochu production method characterized by consisting of a hydrogen container (101-4)
The method of claim 1,
Hydrogen rich shochu production method characterized in that the electrolytic process of the sojunaju 10 by the electrolytic device 102 and the step of dissolving hydrogen by the pressure dissolving device 101 are sequentially performed separately.
The electrolytic device 102 is hermetically configured to have an inlet and a discharge port on the negative electrode 102-1 side, and the electrolytic device 102 is coupled to the middle of the transfer line of the soju glass 10. Hydrogen-rich water production method characterized in that the hydrogen is continuously dissolved by direct electrolysis)
Hydrogen-rich shochu prepared by the method of claim 1 and 5.

KR1020120044217A 2012-04-26 2012-04-26 Hydrogen rich distilled liquor and its method of manufacture KR20130120961A (en)

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