KR20090114984A - A method for preparing the extract of processed horse bone comprising high mineral - Google Patents

Abstract

PURPOSE: A method for preparing a mineral-enriched horse bone extract is provided to blend medicinal herbs with mineral water or underground water in a rock mass for use in medicine, cosmetics, or health supplementary food. CONSTITUTION: A method for preparing a mineral-enriched horse bone extract comprises the following steps of: mixing horse bone and mineral water or underground water in a rock mass at a ratio of 1 to 1-30 by volume, and heating at 200°C for 1-30 hours to obtain an extract; concentrating the extract in vacuum for 1-50 hours to obtain a concentrate; and adding herb medicine components to the concentrate, drying them at 10-200°C for 1-30 hours, and grinding them. The herb medicine components are selected from the group consisting of tissue-cultured wild ginseng roots, Phellinus linteus mycelium, brown rice germ, Cnidii Rhizoma, Cordyceps sinensis, Acanthopanacis Cortex, Carthami semen, Angelicae Radix, Talcum crystallinum, Glycyrrhizae Radix, Menthae Herba, Gypsum Fibrosum, Scutellariae Radix, and Platycodi Radix.

Description

 A method for preparing the extract of processed horse bone comprising high mineral}

 The present invention relates to a horse bone processing extract containing a large amount of minerals.

[Document 1] Korea Institute of Science and Technology Information, the scientific and product trend of water

[Document 2] http://www.geocities.co.jp/beautycare/9506/water/01kozo.html

[Document 3] Water Quality and Environmental Analysis, Shinkwang Cultural History

Along with the increase in horse breeding, horse meat consumption is also increasing.

Jeju's pony is grown in a clean, clean area. Jeju's pony is smaller than other horses, but it is more resistant to rough food, drought or disease, has a milder endurance, and is endured with disease resistance and endurance. None (Nanji Agricultural Research Center). Horse meat is not degraded in protein quality compared to other meats, and it has been found to be amino acids such as threonine and has a high proportion of fatty acids. The resulting resource, horse bone, is used as a health food by the private sector and is sold at high prices. Horse meat is used as an important food resource in some European countries and Japan, and it seems that Korea used horse meat a lot as can be seen in the historical records. During the Joseon Dynasty, horse meat was made in Jeju, and horses were eaten not only in private but also in Guanga. In the past, horse meat and by-products were naturally used in Jeju, the main production area of horses. Recently, the number of breeding heads of Jeju horses has increased drastically due to the use of racing, and the consumption of horse meat and by-products has also increased as slaughtered horses have been increased for the purpose of using meat or bones as the number of retired horses has increased. However, the scientific data and research results are insignificant, and through research and development, the bioactive substances contained in horse bones are identified and the evidence of efficacy is accumulated to provide an opportunity to develop into health functional food using Jeju horses. do.

It is known that there are about 70 kinds of minerals that play an important role in regulating and maintaining various physiological functions in the body. According to the required amount, it is classified into macro mineral and micro mineral (Micromineral or Tracemineral) (Korea Institute of Science and Technology Information, the scientific and product trend of water).

In general, minerals that require more than 100mg per day are called large-scale minerals. This includes seven minerals: calcium, magnesium, potassium, chlorine, sodium, sulfur and phosphorus. Trace minerals that require less than 100mg per day include iron, fluorine, copper, iodine, chromium, cobalt, manganese, silicon, selenium, nickel, vanadium, zinc, silicon, tin, and molybdenum.

To date, 22 minerals, including a large amount of minerals, have been proved essential, but other minerals are not academically established and can be said to be inseparable from the human body. The degree to which these various minerals are used in the human body is influenced by several factors in the body (05, Korea Institute of Science and Technology Information, the scientific and commercialization of water). Among them, the balance of minerals in the body, that is, the mineral balance is greatly affected. In particular, in the case of trace minerals, the absolute amount of each mineral in the body is small, but the variety of types and the human body will react sensitively even to small concentration changes, so should not neglect the balance of trace minerals. This is because the minerals are synergistic and antagonistic between each other and regulate the body's physiology. For example, excessive calcium intake lowers the body's zinc content, magnesium and iron interfere with phosphorus absorption, and potassium and sodium are mutually excessive intakes of one another that inhibit absorption of the other. There is an unimaginable variety of synergism and antagonism among minerals (http://www.geocities.co.jp/beautycare/9506/water/01kozo.html). In addition, the balance of minerals in the body inhibits the absorption of heavy metals, promotes excretion and may have the effect of preventing various diseases caused by heavy metal poisoning in the body. For example, selenium is said to mitigate toxicity from the toxic effects of cadmium (particularly in tobacco), a heavy metal (http://www.geocities.co.jp/beautycare/9506/water/01kozo.html). .

Therefore, by transforming the awareness of processed products using horse bones, Jeju natural rock-rich water and mineral water-containing horse bone extracts, as well as conventional extracts using simple water, are used to make Jeju natural rich in minerals as well as useful ingredients of horse bones. If we get horse bone extract using rock water and samdasoo, we can make horse bone extract rich in useful ingredients and processed products. Therefore, in making products using horse bone extract, the optimal conditions for horse bone extract and the product using horse bone extract are needed to make it easier for the general public to consume useful ingredients of horse bone.

Accordingly, the present inventors have completed the present invention by inventing a method for preparing horse bone extracts containing more mineral components than horse bone extracts extracted with conventional water using natural rock mineral water or samdasu containing a large amount of minerals.

In order to accomplish the above object, the present invention provides a method for producing a horse bone processing extract containing a large amount of minerals.

In detail, the present invention is a step of selecting only the bone well from the slaughtered horse meat, washing it; About 1 to 30 times the weight of the horse bone obtained in the first step, preferably about 1 to 15 times the volume of water, natural rock or hemp water containing a large amount of minerals 10 to 200 ℃, preferably 50 to A second step of heating at 150 ° C. for 1 to 30 hours, preferably 10 to 20 hours, to obtain a horse bone primary extract; A third step of removing the horse bone to obtain a horse bone secondary extract by vacuum concentrating the primary extract obtained in step 2 for 1 to 50 hours, preferably 10 to 30 hours in a quadruple effect concentrator; A fourth step of preparing an auxiliary ingredient by mixing the composite herbal ingredient; After mixing the secondary raw material of the fourth step to the secondary extract of the third step, a fifth step of drying and pulverizing at 10 to 200 ℃, preferably 50 to 150 ℃ for 1 to 30 hours, preferably 1 to 10 hours It provides a method for producing a horse bone processing extract comprising.

The second mineral is one selected from the group consisting of sodium, calcium, magnesium, potassium, zinc, iron, fluorine, copper, iodine, chromium, cobalt, manganese, silicon, selenium, nickel, vanadium, silicon, tin and molybdenum It is characterized by containing the above minerals.

The secondary extract of the third step is concentrated to a volume of 1/2 to 1/10 times, preferably 1/2 to 1/5 times, more preferably 1/2 to 1/3 of the primary extract It is characterized by.

The herbal composition of the fourth step is one or more herbal medicines selected from the group consisting of wild ginseng culture root, situation mushroom mycelium, brown rice embryo, cheonggung, Cordyceps sinensis Ogapi, safflower seed, Sooji Port, donkey, talc, licorice, peppermint, gypsum, gold and Giltyeong Ingredients, preferably, wild ginseng culture root, situation mushroom mycelium, brown rice embryo, and one or more herbal ingredients selected from the group consisting of uterus.

Preferred blending weight ratio (w / w%) of the complex herbal medicine is 5 to 20% of wild ginseng culture root, 20 to 40% of green mushroom mycelium, 20 to 70% of brown rice embryo, 5 to 20% of uterus, more preferably wild ginseng It is characterized in that it is formulated in a weight ratio (w / w%) of 10 to 15% culture root, 30 to 35% of mushroom mycelium, 35 to 50% of brown rice embryos, 10 to 15% of uterus.

The mixing of the subsidiary materials of the fifth step is about 1 to 50%, preferably 5 to 20% by weight of the secondary extract divided into five equal parts, respectively, and the weight ratio (w / w) to the dry weight of the secondary extract. %) And then mix into one.

The fifth step of the grinding process is characterized in that the horse bone processing extract is ground to particles of 1 ~ 150 mesh (mesh), preferably 10 ~ 100 mesh (mesh).

In addition, the first step of drying the horse bone processed extract prepared by the above production method for 1 to 20 hours, preferably 1 to 10 hours at 10 to 100 ℃, preferably 50 to 80 ℃; A second step of drum-drying the dried horse bone processing extract of the first step; It provides a method of producing a horse bone processing extract powder comprising a third step of grinding the dried horse bone processing extract of the second step 1 ~ 250 mesh (mesh), preferably 10 ~ 150 mesh (mesh).

A first step of drying the horse bone processed extract prepared by the above production method at 10 to 100 ° C., preferably at 50 to 80 ° C. for 1 to 20 hours, preferably 1 to 10 hours; A second step of drum-drying the dried horse bone processing extract of the first step; A third step of obtaining powder by grinding the dried horse bone extract of step 2 in a particle size of 1 to 250 mesh, preferably 10 to 150 mesh; After mixing the powder of the third step with the secondary horse bone processing extract in a weight ratio (w / w%) of 1: 0.01 ~ 1, preferably 1: 0.1 ~ 0.8, 1 to 10 minutes, preferably 1 A fourth step of stirring for 5 minutes; It provides a method for producing a horse bone extract extract ring comprising a fifth step of preparing a ring 1 to 10cm, preferably 1 to 5cm after stirring.

The drying step of the second step is characterized in that the moisture content of 1 to 10%, preferably 1 to 5%.

The present invention provides a powder or ring of horse bone processing extract prepared by the above method.

The method for producing a horse bone extract containing a large amount of mineral of the present invention is a composite herbal ingredient in a horse bone extract that is rich in minerals than conventional water extracts by using natural rock water or Samdasoo as well as general water. As a manufacturing method that can be easily taken by the general public by mixing, it can be used as a raw material of various medicines, cosmetics, health supplements, etc., using the horse bone processing extract as an active ingredient.

Hereinafter, the present invention will be described in detail by the following Examples and Experimental Examples.

However, the following Examples and Experimental Examples are merely illustrative of the present invention, and the content of the present invention is not limited by the following Examples and Experimental Examples.

Example  One. Horse Bone Processing Extract  Produce

1-1. 1st extract manufacturing step

Select only bones from the slaughtered horse meat (Jeju World) Heat at 100 ° C. in a autoclave pot (EX3000, thawing plant) for 24 hours. After the extraction process, the horse bone remaining in the extract was filtered, filtered using filter paper (3M), and the filtrate was concentrated under reduced pressure using a rotary decompression concentrate (EYELA FDU-1100) to obtain 500 kg of horse bone primary extract.

1-2. 2nd extract manufacturing step

The horse bone extract having a weight of 500 kg of Example 1-1 was concentrated in a vacuum for 24 hours until the horse bone extract was 250 kg (50% of the original weight) in a four-effect concentrator to increase drying capacity and increase the solid content.

After the concentration process, the secondary extract after the concentration step (solid content 6%) from the solid content of the primary extract (3%) can obtain a high concentration horse bone extract.

1-3. Subsidiary Manufacturing

10 kg of wild ginseng culture root (Jeju Bio Value, Jeju), 25 kg of situation mushroom mycelium, 30 kg of brown rice germ, or 10 kg of Cheongung purchased from Seoul Gwangju, based on 75 kg of 15% weight ratio of 500 kg of the secondary extract of Example 1-2 The mixture was divided into 5 portions of 5 parts of the secondary extract, and the mixture was sufficiently stirred, and then pulverized into 80 mesh so as to have a uniform size primarily at 120 ° C. for 4 hours, and evenly mixed.

Example  2. Preparation of Horse Bone Extract

The horse bone processing extract powder obtained in Example 1 was dried at 70 ° C. for 6 hours, drum dried to a moisture content of 1 to 2% to make a horse bone extract powder solution, and then the horse bone processing extract powder was ground to 130 mesh. The glass bottles were filled with a filling machine (DS-S132A-1, Korea Electronics Industry), and then packaged and commercialized.

Example  3. Preparation of Circulation of Horse Bone Extract

The horse bone processing extract powder obtained in Example 1 was dried at 70 ° C. for 6 hours, drum dried to a moisture content of 1 to 2% to make horse bone extract powder solution, and then the horse bone processing extract powder was ground to 130 mesh. After mixing the powder and horse bone extract in a weight ratio of 1: 0.6, the mixture was stirred for 1 ~ 2 minutes in a stirrer (W-NEADER, PM TECH), and then put into a recirculator (PT-6025, PM TECH) for 2 ~ 4cm diameter In order to make the water content of 1 to 3% by drying in a hot air dryer at 80 ℃ for 30 hours, put the dried ring in a filler and then packed into a glass bottle and commercialized.

Experimental Example  1. Mineral Content Analysis

In order to analyze and compare the minerals of horse bone processing extracts using water, natural rock or Samdasoo water, the following experiments were conducted using the methods described in the existing literature (Water Quality and Environmental Analysis, Shinkwang Culture History).

Inorganic materials containing heavy metals were analyzed using Inductively Coupled Plasma Mass Spectrometer (ICP / MS: Varian820.Australia), which is a heavy metal analyzer. Water quality components were analyzed using standard methods. In order to optimize the interference effect of the interference material (interface martrix) of the sample was analyzed by applying a CRI (collision reaction interface) system, the analysis conditions are shown in Table 1 below.

ICP / MS Analysis Conditions item parameters setting range Gas flow (L / min) plasma flow 16.5 ~ 18.5 Auxiliary flow 1.45-1.55 Sheath gas flow 0.22-0.25 Nebulizer flow 1.0 RF power (kw) RF power (kw) 1.4 CRI gases (L / min) Skimmer (with H2) 0.085-0.090 Scan mode peak hopping Dwell time (ms) 20 Quardrupole scan Points per peak One Scan / Replicate 50 Replicates / Sample 3

As shown in Table 2, general water contains almost no vanadium, whereas natural rock water contains 600 times or more than normal water, and Samdasu contains 50 to 70 times that of normal water. It was confirmed that there is. In addition, it was confirmed that natural rock water or Samdasu water contained abundant minerals in addition to vanadium, compared to general water.

mineral water Natural rock Samdasoo Vanadium (V) (μg / l) 0.1-0.3 60-64 5 ~ 7 Sodium (Na) (mg / l) 4.1 ~ 4.3 4.5 ~ 4.7 4.2-4.6 Calcium (Ca) (mg / l) 6.1-6.3 7.6 ~ 7.9 9.5-9.8 Mg (mg / l) 1.2 to 1.5 2.5 ~ 2.9 3.1 ~ 3.2 Potassium (K) (mg / l) 1.1 to 1.3 2.1 ~ 2.3 3.1 ~ 3.4 Zinc (Zn) (μg / l) 7.2 ~ 7.8 5.2 ~ 5.6 6.2 to 6.7 Silicon (Si) (ppm) 7.2 ~ 7.4 13.5-13.8 14.8-15.0

1 is a view showing a powder manufacturing method using a horse bone processing extract,

Figure 2 is a view showing a ring manufacturing method using a horse bone processing extract.

Claims (10)

Selecting only the bone area from the slaughtered horse meat and washing it; The first step of obtaining a primary extract by heating for 1 to 30 hours at 10 to 200 ℃ in natural rock water or hemp water containing a large amount of water, minerals of about 1 to 30 times the weight of the horse bone obtained in the first step Step 2; A third step of removing the horse bone to obtain a secondary extract by vacuum concentrating the primary extract obtained in step 2 for 1 to 50 hours in a quadruple effect concentrator; A fourth step of preparing an auxiliary ingredient by mixing the composite herbal ingredient; Method for producing a horse bone processing extract comprising a fifth step of drying and pulverizing for 1 to 30 hours at 10 to 200 ℃ after mixing the secondary raw material of the fourth step to the secondary extract of the third step. The method of claim 1, wherein the mineral of the second step is sodium, calcium, magnesium, potassium, zinc, iron, fluorine, copper, iodine, chromium, cobalt, manganese, silicon, selenium, nickel, vanadium, silicon, tin and molybdenum Manufacturing method characterized in that it comprises one or more selected from the group consisting of. The method of claim 1, wherein the secondary extract of the third step is characterized in that concentrated to 1/2 to 1/10 times the primary extract. According to claim 1, wherein the herbal compound of the fourth step is composed of wild ginseng culture root, situation mushroom mycelium, brown rice embryo, Cheongung, Cordyceps sinensis Ogapi, safflower seed, Sooji Port, Angelica, talc, licorice, peppermint, gypsum, gold and Gilt Method for producing a herbal ingredient selected from the group comprising one or more. According to claim 1, wherein the compounding weight ratio (w / w%) of the complex herbal medicine is 5 to 20% of wild ginseng culture root, 20 to 40% of mushroom mycelium, 20 to 70% of brown rice embryo, 5 to 20% of uterus ( w / w%)). The method according to claim 1, wherein the mixing of the subsidiary materials of the fifth step is performed by mixing subdivided subdivided into 5 equal parts, respectively, in a weight ratio (w / w%) of about 1 to 50% of the secondary extract. After the production method characterized in that it is blended into one. The method according to claim 1, wherein the grinding step of the fifth step comprises grinding horse bone extract into 1 to 150 mesh particles. A first step of drying the horse bone processing extract prepared by the method of claim 1 for 10 to 100 ℃ for 1 to 20 hours; A second step of drum-drying the dried horse bone processing extract of the first step; Method for producing a horse bone processing extract powder comprising a third step of grinding the dried horse bone processing extract of the second step 1 ~ 250 mesh (mesh). A first step of drying the horse bone processing extract prepared by the method of claim 1 for 10 to 100 ℃, for 1 to 20 hours; A second step of drum-drying the dried horse bone processing extract of the first step; A third step of obtaining powder by grinding the dried horse bone processing extract of 2 steps in a particle size of 1 to 250 mesh; A fourth step of mixing the powder of the third step with the second horse bone processing extract in a weight ratio of 1: 0.01 to 1, and then stirring for 1 to 10 minutes in a stirrer; Method of producing a horse bone extract extract ring comprising a fifth step of preparing a ring of 1 to 10cm after stirring into the reactor. The method of claim 8 or 9, wherein the drying step of the second step is characterized in that the moisture content of 1 to 10%.

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