KR20070075074A - Dental zirconia block - Google Patents

Dental zirconia block Download PDF

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Publication number
KR20070075074A
KR20070075074A KR1020060003405A KR20060003405A KR20070075074A KR 20070075074 A KR20070075074 A KR 20070075074A KR 1020060003405 A KR1020060003405 A KR 1020060003405A KR 20060003405 A KR20060003405 A KR 20060003405A KR 20070075074 A KR20070075074 A KR 20070075074A
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South Korea
Prior art keywords
block
hours
mixture
dental
dental zirconia
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KR1020060003405A
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Korean (ko)
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성광모
이은희
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성광모
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Priority to KR1020060003405A priority Critical patent/KR20070075074A/en
Publication of KR20070075074A publication Critical patent/KR20070075074A/en

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    • AHUMAN NECESSITIES
    • A41WEARING APPAREL
    • A41DOUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
    • A41D27/00Details of garments or of their making
    • A41D27/08Trimmings; Ornaments

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Dental Prosthetics (AREA)
  • Materials For Medical Uses (AREA)
  • Dental Preparations (AREA)

Abstract

A dental zirconia block is provided to improve strength, biocompatibility, and aesthetic sense, and to reduce medical expenses by frequent break of existing alumina block by using zirconia instead of alumina. The dental zirconia block is manufactured by planning an optimum chemical composition with an excellent material property such as 50-70% of SiO2,10-20% of ZrO2, 10-30% of K2O and Na2O, and 5% of others, mixing raw materials according to the composition, drying the mixture, melting the mixture at 1300-1700 deg.C for 2 hours, and calcining the mixture at 700-1000 deg.C for 2 hours.

Description

치과용 지르코니아 블록 {Dental Zirconia Block}Dental Zirconia Blocks {Dental Zirconia Block}

도 1은 본 발명과 기존의 치과용 블록의 비교도1 is a comparison of the present invention and the conventional dental block

도 2는 치과용 블록의 유리분말 제조과정의 순서도2 is a flow chart of the glass powder manufacturing process of the dental block

도 3은 성형체가 나오기까지의 제조 공정도3 is a manufacturing process diagram until a molded product comes out

도 4는 완성된 성형체(블록)4 is a completed molded body (block)

<도면의 주요부분에 대한 부호의 설명><Description of the symbols for the main parts of the drawings>

1,4 : 도재(Porcelain) 2 : 불투명층(Opaque)1,4 Porcelain 2 Opaque

3 : 금속(Metal) 5 : 세라믹(블록)3: Metal 5: Ceramic (Block)

6 : 원재료(Raw Materials) 7,16 : 혼합(Mixing)6: Raw Materials 7,16: Mixing

8,19 :건조(Drying) 9 : 용해(Melting)8,19: Drying 9: Melting

10 : 하소(Calcination) 11,17; 성형(Forming)10: Calcination 11,17; Forming

12 : 분쇄(Milling) 13,14:유리분말(Glass powder)12: Milling 13, 14: Glass powder

15 : 루사이트(Leucite) 18 : 열처리(Heating)15: Leucite 18: Heating

20,22: 성형체(Pellet,Block) 21: 평가항목20,22: molded body (Bellet, Block) 21: evaluation items

본 발명은 치과용 보철물에 사용되는 인공치아 세라믹의 재료에 관한 것으로, 더욱 상세하게는 지르코니아 세라믹스 소재로 자연치아 수복 및 인공치아 수복과정의 보철물로 사용되는 심미성과 강도가 높은 지르코니아 블록을 만드는 방법에 관한 것이다.The present invention relates to a material of an artificial tooth ceramic used in a dental prosthesis, and more particularly, to a method of making a zirconia block having high aesthetics and strength, which is used as a prosthesis for a natural tooth restoration and an artificial tooth restoration process using a zirconia ceramic material. It is about.

일반적으로 금속(합금)-> 금속+알루미나-> 알루미나(세라믹)의 소재로 사용하고 있다.Generally, it is used as a material of metal (alloy)-> metal + alumina-> alumina (ceramic).

그 일례로서 도 1에서의 (가)와 같이 금속(3)위에 금속 색상을 없애기 위해 불투명층(2)으로 감싸고 그 위에 도재(1)를 입혀 인공치아를 만들었으나 금속의 부식이나 잇몸변색 문제와 알레르기 및 darkline 형성으로 최근에는 금속대신 생체친화성이 좋은 강도가 높은 Al2O3로 대체함으로서 더욱 심미성을 개선시킬 수 있었다. 그러나 현재 많이 사용되고 있는 Al2O3로 심미적인 장점을 개선할 수 있었으나 세라믹의 취성적인 성질로 파절의 위험에 노출되어 있어 더욱이 개선요구가 증가되고 있다.As an example, as shown in (a) of FIG. 1, an artificial tooth was formed by wrapping it with an opaque layer (2) and coating a ceramic material (1) on the metal (3) to remove metal color. Allergy and darkline formation have recently improved the esthetics by replacing Al2O3 with high biocompatibility with high strength instead of metal. However, Al2O3, which is currently used a lot, could improve the aesthetic advantages, but the brittle nature of ceramics exposed to the risk of fracture, which further increases the demand for improvement.

본 발명은 상기와 같은 취성적인 문제점을 해소하기 위해 Al2O3를 강도가 높고 생체친화성 및 심미성이 좋은 ZrO2로 대체하였다. 이와같은 목적을 달성하기 위 한 발명은, 예비 성형체의 제조 과정에 있어서 SiO2(50~70%) ZrO2(10~20%) K2O+Na2O(10~30%) other 5% 조성으로 자연치보다 우수한 물성치를 갖는 최적 화학 조성 설계, 상기 설계 후 제조 과정에서의 1300~1700℃에서 약 2시간 동안 Melting시 환경변수의 단계The present invention replaced Al2O3 with ZrO2 having high strength, good biocompatibility and aesthetics to solve the brittle problem. In order to achieve the above object, the invention is superior to natural teeth with the composition of SiO2 (50 ~ 70%) ZrO2 (10 ~ 20%) K2O + Na2O (10 ~ 30%) other 5%. Optimal chemical composition design with, the step of environmental variables during Melting for about 2 hours at 1300 ~ 1700 ℃ in the manufacturing process after the design

상기 단계 후 700~1000℃에서 약 2시간 동안 열처리하는 단계로 이루어진 것에 특징이 있다.After the step is characterized in that the heat treatment for about 2 hours at 700 ~ 1000 ℃.

이하 첨부된 도면에 의해 상세히 설명하면 다음과 같다.Hereinafter, described in detail by the accompanying drawings as follows.

도 2는 치과용 블록의 유리분말 제조과정으로서, 원재료(6) SiO2(50~70%) ZrO2(10~20%) K2O+Na2O(10~30%) other 5% 조성으로 최적의 화학조성을 설계하여 최대한 미세하게 잘 혼합(7)될 수 있게 섞은 후 건조(8)시킨 분말을 백금도가니에 장입하여 1300~1700℃ 전기로에서 용해(9) 후 하소(10)한다.Figure 2 is a glass powder manufacturing process of the dental block, raw material (6) SiO2 (50 ~ 70%) ZrO2 (10 ~ 20%) K2O + Na2O (10 ~ 30%) other 5% composition of the optimum chemical composition design After mixing so that it can be finely mixed (7) as finely as possible, the dried (8) powder is charged into a platinum crucible and dissolved (9) in an electric furnace at 1300 to 1700 ° C., followed by calcination (10).

다음 급냉 후 성형(11)과 분쇄(12)를 하게 되면 유리분말(13)을 얻을 수 있다. 도 3은 이러한 상태에서 나온 유리분말(14)과 접착력과 강도가 뛰어나게 하는 루사이트(15)를 미세하게 혼합(16)하여 일정한 틀에 성형(17)을 하고 전기로에서 500~1000℃ 열처리 후 건조 시킨 후 성형체인 펠렛(블록)을 얻을 수 있다. 블록을 얻은 후 기계적 강도 및 성질 등을 평가(21)하여 완전한 블록을 얻게 된다.Next, after the quenching, the molding 11 and the crushing 12 may be performed to obtain the glass powder 13. 3 is finely mixed (16) the glass powder 14 and the lusite (15) having excellent adhesion and strength in this state to form (17) in a constant mold and dried after heat treatment 500 ~ 1000 ℃ in an electric furnace After this, pellets (blocks) that are shaped bodies can be obtained. After the block is obtained, mechanical strength and properties are evaluated (21) to obtain a complete block.

도 4는 완성된 블록으로서 지름 11.24, 높이 8.36을 가지는 성형체를 얻을 수 있다.4 shows a molded body having a diameter of 11.24 and a height of 8.36 as a completed block.

이상에서 상술한 바와 같이 본 발명은 높은 가격으로 전량 수입되던 치과용 알루미나 블록을 국내 개발된 지르코니아 블록으로 대체함으로서 막대한 수입대체효과를 기대할 수 있으며, 역수출도 기대되고 있다. 뿐만 아니라 기존 알루미나 블록에 의한 잦은 파절로 추가 발생하던 의료비도 크게 절감될 수 있으며, 자연치와 유사한 심미성으로 비용 대비하여 높은 만족감을 줄 수 있다.As described above, the present invention can expect enormous import substitution effects by replacing dental alumina blocks, which were imported at a high price, with domestically developed zirconia blocks, and also expecting back exports. In addition, medical expenses, which were additionally generated due to frequent fractures due to the existing alumina blocks, can be greatly reduced, and aesthetics similar to natural teeth can provide high satisfaction for the cost.

Claims (1)

치과 보철물로 사용되기에 앞서 예비 성형체의 제조 과정에 있어서, In the process of manufacturing the preform prior to being used as a dental prosthesis, 자연치보다 우수한 물성치를 갖는 최적 화학 조성 설계,Optimum chemical composition design with better physical properties than natural teeth SiO2(50~70%) ZrO2(10~20%) K2O+Na2O(10~30%) other 5% SiO2 (50 ~ 70%) ZrO2 (10 ~ 20%) K2O + Na2O (10 ~ 30%) other 5% 상기 설계 후 제조 과정에서의 환경변수의 단계Step of environmental variables in the manufacturing process after the design 1300~1700℃에서 약 2시간 동안 Melting단계,Melting step for about 2 hours at 1300 ~ 1700 ℃, 상기 단계 후 700~1000℃에서 약 2시간 동안 열처리하는 단계 Heat treatment at 700-1000 ° C. for about 2 hours after the step
KR1020060003405A 2006-01-12 2006-01-12 Dental zirconia block KR20070075074A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20200047468A (en) 2020-04-20 2020-05-07 주식회사 하스 A method of manufacturing a zirconia-coating glass for inducing chemical bonding between a zirconia prosthesis and resin cement and a zirconia-coating glass

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20200047468A (en) 2020-04-20 2020-05-07 주식회사 하스 A method of manufacturing a zirconia-coating glass for inducing chemical bonding between a zirconia prosthesis and resin cement and a zirconia-coating glass

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