KR20030061110A - Offset printable silicon transcription sheet and preparation thereof - Google Patents

Offset printable silicon transcription sheet and preparation thereof Download PDF

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Publication number
KR20030061110A
KR20030061110A KR1020020001484A KR20020001484A KR20030061110A KR 20030061110 A KR20030061110 A KR 20030061110A KR 1020020001484 A KR1020020001484 A KR 1020020001484A KR 20020001484 A KR20020001484 A KR 20020001484A KR 20030061110 A KR20030061110 A KR 20030061110A
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South Korea
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silicone resin
layer
transfer paper
liquid silicone
offset
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KR1020020001484A
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Korean (ko)
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KR100488674B1 (en
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전영한
전인섭
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전영한
전인섭
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/26—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used
    • B41M5/40—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used characterised by the base backcoat, intermediate, or covering layers, e.g. for thermal transfer dye-donor or dye-receiver sheets; Heat, radiation filtering or absorbing means or layers; combined with other image registration layers or compositions; Special originals for reproduction by thermography
    • B41M5/42—Intermediate, backcoat, or covering layers
    • B41M5/44—Intermediate, backcoat, or covering layers characterised by the macromolecular compounds
    • B41M5/443—Silicon-containing polymers, e.g. silicones, siloxanes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
    • B32B7/04—Interconnection of layers
    • B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
    • B41M5/52—Macromolecular coatings
    • B41M5/529—Macromolecular coatings characterised by the use of fluorine- or silicon-containing organic compounds

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  • Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Decoration By Transfer Pictures (AREA)

Abstract

PURPOSE: Provided is a silicone transfer paper for possible offset printing which adds a flow preventer to silicone resin to form a pattern printed layer so that it produces the transfer paper to show transparent picture by offset printing. CONSTITUTION: The production process for the silicone transfer paper for possible offset printing comprises the steps of: (i) coating a releasing paper with transparent liquid silicone resin to form a protection layer; (ii) coating liquid silicone resin including the flow preventer on the protection layer to form the pattern printed layer; (iii) offset-printing transfer patterns on the pattern printed layer; and (iv) coating white liquid silicone resin including white pigment on the pattern printed layer to form a sticking layer.

Description

오프셋 인쇄가능한 실리콘 전사지 및 그 제조방법{Offset printable silicon transcription sheet and preparation thereof}Offset printable silicon transcription sheet and preparation method thereof

본 발명은 실리콘 전사지에 관한 것으로서, 보다 구체적으로는 오프셋 인쇄가능한 실리콘 전사지 및 그 제조방법에 관한 것이다.BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a silicone transfer paper, and more particularly, to an offset printable silicone transfer paper and a method of manufacturing the same.

전사지는 재질, 형상적으로 직접 인쇄를 하기 어려운 피인쇄체에 인쇄할 때, 또는 다색 그림을 단번에 피인쇄체 위에 형성할 때 사용하는 것으로, 인쇄에 여러 가지 판식이 사용되는데, 그림의 형성은 전사지 위에 반대 보기로 인쇄된다.Transfer paper is used when printing onto a printed material that is difficult to print directly in material or shape, or when a multicolored picture is formed on the printed material at one time. Various plates are used for printing. Printed as an example.

전술한 전사 인쇄 방법은 종이나 합성수지 필름으로 된 전사원지의 표면에 가열 용융 박리층, 필요에 따른 인쇄 보호층, 무늬 인쇄층 및 접착층을 순차적으로 적층되게 형성하여 전사지를 제조하고 이 전사지를 피전사체, 예를들면 합성수지 제품 표면에 접촉시켜 가열 압착하므로써 접착층이 합성 수지 제품 표면에 고착되도록한 다음 전사원지를 인쇄층으로부터 분리제거하는 방법으로 구성된다.The above-described transfer printing method is to form a transfer paper by sequentially forming a hot melt peeling layer, a print protection layer, a patterned printing layer, and an adhesive layer on the surface of a transfer paper made of paper or a synthetic resin film, and transferring the transfer paper, For example, the adhesive layer is adhered to the surface of the synthetic resin product by contact with the surface of the synthetic resin product to be pressed to the surface of the synthetic resin product, and then the transfer base is separated from the printed layer.

한편, 실리콘 수지는 탄성, 신축성, 내열성 및 방수성이 우수하여 수영복이나 수영모자 등과 같이 신축성이 높은 제품에 적용하기 위한 전사지의 소재로 적합하나 실리콘 수지 막이 오프셋 인쇄시 잉크 흡착능력이 미흡하여, 오프셋 인쇄로 선명한 그림을 형성한 실리콘 전사지를 제조하는 것이 불가능한 것으로 인식되어져 왔다.On the other hand, silicone resin is excellent in elasticity, elasticity, heat resistance and waterproofness, so it is suitable as a transfer paper material to be applied to products with high elasticity such as swimwear and swimming caps, but the silicone resin film has insufficient ink adsorption capacity when offset printing. It has been recognized that it is impossible to produce a silicon transfer paper having a sharp picture.

따라서 본 발명은 오프셋 인쇄로 선명한 그림을 부여할 수 있는 새로운 전사지를 제공하는 것을 기술적 과제로 한다.Therefore, it is a technical object of the present invention to provide a new transfer paper capable of giving a clear picture by offset printing.

상기한 과제를 해결하기 위하여 본 발명자는 장기간에 걸쳐 다양한 실험을 거듭한 결과 실리콘 수지에 흐름방지제를 배합하여 조면화된 무늬인쇄층을 형성하는 경우 오프셋 인쇄로 선명한 그림을 부여한 전사지를 제조할 수 있다는 사실을 알게 되어 본 발명을 완성하게 된 것이다.In order to solve the above problems, the present inventors have conducted various experiments over a long period of time, and thus, when a roughening pattern printing layer is formed by mixing a flow inhibitor with a silicone resin, the present invention can produce a transfer paper with a clear picture by offset printing. Knowing the facts to complete the present invention.

그러므로 본 발명에 의하면 이형지 위에 보호층, 무늬인쇄층, 인쇄무늬 및 접착층이 순차적으로 형성된 실리콘 전사지에 있어서, 상기 무늬 인쇄층이 조면화된 표면을 가질 수 있는 정도의 양으로 흐름방지제를 함유한 투명 액상 실리콘 수지로 형성된 것을 특징으로 하는 오프셋 인쇄가능한 실리콘 전사지가 제공된다.Therefore, according to the present invention, in a silicone transfer paper in which a protective layer, a pattern printing layer, a printed pattern, and an adhesive layer are sequentially formed on a release paper, a transparent agent containing a flow inhibitor in an amount sufficient to have a roughened surface. Provided are offset printable silicone transfer papers formed from a liquid silicone resin.

또한 본 발명에 의하면 상기한 전사지를 제조하는데 바람직한 방법의 하나로서 다음의 단계를 포함하는 실리콘 전사지의 제조방법이 제공된다:According to the present invention, there is also provided a method for producing a silicone transfer paper, which comprises the following steps as one of the preferred methods for producing the transfer paper described above:

이형지에 액상 실리콘 수지를 도포하여 보호층을 형성하는 공정,Forming a protective layer by applying a liquid silicone resin to a release paper,

보호층 위에 조면화된 표면을 가질 수 있는 정도의 양으로 흐름방지제를 함유한 액상 실리콘 수지를 도포하여 조면화된 무늬인쇄층을 형성하는 공정,Forming a roughened pattern printing layer by applying a liquid silicone resin containing a flow inhibitor in an amount sufficient to have a roughened surface on the protective layer,

무늬인쇄층 위에 전사무늬를 오프셋 인쇄하는 공정, 및Offset printing the transfer pattern on the pattern printing layer, and

오프셋 인쇄된 무늬 인쇄층 위에 백색 안료를 함유하는 백색의 액상 실리콘 수지를 도포하여 접착층을 형성하는 공정.A step of forming an adhesive layer by applying a white liquid silicone resin containing a white pigment on an offset-printed patterned printing layer.

이하, 본 발명을 보다 상세하게 설명하기로 한다.Hereinafter, the present invention will be described in more detail.

본 발명의 실리콘 전사지는 무늬인쇄층이 흐름방지제를 함유한 투명한 액상 실리콘 수지로 형성되어 조면화된 표면을 가짐으로써 오프셋 인쇄로 소망하는 무늬를 선명하게 형성시킬 수 있도록 한 것에 주된 특징이 있다.The silicon transfer paper of the present invention is characterized in that the pattern printing layer is formed of a transparent liquid silicone resin containing a flow inhibitor to have a roughened surface so that the desired pattern can be clearly formed by offset printing.

통상적으로 실리콘 전사지의 제조에서 액상 실리콘 수지에 흐름방지제를 넣으면 광택이 적고 텐션이 불량해지기 때문에 첨가하지 않거나 소량만을 첨가해 왔다. 이와 같이 흐름방지제를 첨가하지 않거나 소량 첨가한 액상 실리콘 수지로 무늬인쇄층을 형성할 경우 다른 인쇄 방법으로는 무늬를 형성할 수 있으나 오프셋 인쇄방법으로는 잉크가 잘 흡착되지 않아서 선명한 무늬를 인쇄할 수가 없었다.In general, in the manufacture of the silicone transfer paper, when the flow preventing agent is added to the liquid silicone resin, the gloss is poor and the tension is poor. Therefore, only a small amount has been added. When the pattern printing layer is formed with the liquid silicone resin without the addition of the flow inhibitor or a small amount as described above, the pattern may be formed by another printing method, but the offset printing method may not print the ink so that the clear pattern may be printed. There was no.

그러나 본 발명에 따라 무늬인쇄층 표면이 조면화될 수 있을 정도의 양으로 흐름방지제를 배합한 투명 액상 실리콘 수지로 무늬인쇄층을 형성할 경우 흐름방지제가 실리콘 수지막의 광택을 떨어뜨리는 대신에 인쇄잉크의 흐름을 방지하여 오프셋 인쇄로 선명한 무늬를 형성시킬 수가 있게 되고, 무늬인쇄층 표면의 조면화로 인한 광택성 저하 문제는 무늬 인쇄층 표면과 이면에 적층되는 보호층과 접착층의적절한 선택에 의해 보완할 수가 있다. 예를 들어 보호층을 광택이 우수한 투명 액상 실리콘 수지로 형성시키고 접착층을 백색안료로 백색을 부여한 액상 실리콘 수지로 형성시키면 흐름방지제의 첨가에 의한 무늬인쇄층의 광택성 저하 문제를 해결할 수 있게 된다.However, when the pattern printing layer is formed of a transparent liquid silicone resin containing a flow inhibitor in an amount such that the surface of the pattern printing layer can be roughened according to the present invention, the flow inhibitor prevents the gloss of the silicone resin film from the printing ink. It is possible to form a vivid pattern by offset printing by preventing the flow of water, and the problem of gloss deterioration due to the roughening of the surface of the pattern printing layer can be compensated by appropriate selection of the protective layer and the adhesive layer laminated on the surface and the back surface of the pattern printing layer. There is a number. For example, when the protective layer is formed of a transparent liquid silicone resin having excellent gloss and the adhesive layer is formed of a liquid silicone resin imparted with white pigment, the problem of deterioration of glossiness of the pattern printing layer due to the addition of a flow inhibitor can be solved.

본 발명 전사지의 무늬인쇄층을 형성하는데 사용되는 투명 액상 실리콘 수지중의 흐름방지제 함량은 흐름방지제의 종류에 따라 다소 다를 수 있으나, 오프셋 인쇄에 적합한 조면화된 표면을 갖는 무늬인쇄층을 형성시키기 위해서는 액상 실리콘 수지중의 흐름방지제 함량이 10∼20중량%, 보다 바람직하게 10∼15중량%가 정도가 되어야 한다. 이러한 흐름방지제의 함량이 너무 적으면 표면이 매끄러워 오프셋 인쇄시 잉크가 잘 먹히지 않아 선명한 오프셋 인쇄 무늬를 부여하는 것이 곤란할 수 있으며, 너무 많으면 실리콘 전사지의 전사후에 나타나는 특성인 탄성, 신축성 등이 불량하게 될 수 있다.Flow inhibitor content in the transparent liquid silicone resin used to form the pattern printing layer of the transfer paper of the present invention may vary slightly depending on the type of flow inhibitor, but in order to form a pattern printing layer having a roughened surface suitable for offset printing The flow inhibitor content in the silicone resin should be about 10 to 20% by weight, more preferably about 10 to 15% by weight. If the content of the flow inhibitor is too small, it may be difficult to give a clear offset print pattern because the surface is smooth and ink does not eat well when offset printing, and if too much, elasticity, elasticity, etc., which are characteristics that appear after transfer of silicon transfer paper, are poor Can be.

이러한 흐름 방지제는 당분야에 잘 알려져 있으며, 그 중 대표적인 것은 미립자상의 무기광물이다. 이러한 미립자상 무기광물계 흐름방지제의 시중구입가능한 예로는 일본 아에로실사 제품인 에어로실(Aerosil)이 있다. 에어로실은 초미분말 무수실리카로서 수지에 첨가하여 분산시킴으로써 수지의 흐름을 방지하는데 이용되고 있다.Such flow inhibitors are well known in the art, representative of which are particulate minerals. Commercially available examples of such particulate inorganic mineral flow inhibitors include Aerosil, manufactured by Aerosil Japan. Aerosil is used as an ultra fine powder anhydrous silica to prevent the flow of the resin by adding and dispersing the resin.

바람직하게 본 발명의 실리콘 전사지는 이형지에 투명 액상 실리콘 수지를 도포하여 보호층을 형성하고, 그 위에 흐름방지제를 함유한 투명 액상 실리콘 수지를 도포하여 조면화된 표면을 갖는 무늬인쇄층을 형성한 다음, 형성된 무늬인쇄층위에 전사무늬를 오프셋 인쇄하여 부여하고 나서 그 위에 백색 안료를 함유하는 백색의 액상 실리콘 수지를 도포하여 접착층을 형성시키는 것에 의해 제조할 수 있다.Preferably, the silicone transfer paper of the present invention is coated with a transparent liquid silicone resin on a release paper to form a protective layer, and a transparent liquid silicone resin containing a flow inhibitor is formed thereon to form a pattern printing layer having a roughened surface. It can be produced by offset printing a transfer pattern on the formed pattern printing layer, and then applying a white liquid silicone resin containing a white pigment thereon to form an adhesive layer.

보호층과 접착층의 제조에 사용되는 실리콘 수지에는 흐름방지제를 첨가하지 않거나 또는 첨가하더라도 광택을 떨어뜨리지 않을 정도의 소량만을 첨가하는 것이 바람직하다.It is preferable to add only a small amount of silicone resin used in the production of the protective layer and the adhesive layer to the extent that the flow inhibitor is not added or the gloss is not degraded even if it is added.

이와 같이 전사지를 제조한 상태에서 피인쇄체 표면에 접촉시켜 가열 압착하므로써 접착층이 합성 수지 제품 표면에 고착되도록 한 다음 이형지를 인쇄층으로부터 분리제거하여 전사인쇄를 할 수도 있으나, 전사지의 취급 및 유통 안정성을 부여하기 위해서는 상기한 접착층 위에 실리콘 러버 희석액을 도포하여 추가적인 접착층을 형성한 후 폴리에틸렌 필름과 같은 박리성 보호필름을 적층시키는 것이 바람직하다.As described above, the adhesive layer is fixed to the surface of the synthetic resin product by contact with the surface of the printed material in a state where the transfer paper is prepared, and then the release paper is separated and removed from the printing layer to perform transfer printing. In order to apply, it is preferable to apply a silicone rubber diluent on the adhesive layer to form an additional adhesive layer and then to laminate a peelable protective film such as a polyethylene film.

또한 상기한 액상 실리콘 수지 및 러버상 실리콘 수지에는 경화제를 적정량 첨가하여 열전사시에 실리콘 수지의 열경화를 촉진시키는 것이 바람직하다.In addition, it is preferable to add an appropriate amount of a curing agent to the above-mentioned liquid silicone resin and rubber-like silicone resin to promote thermosetting of the silicone resin during thermal transfer.

이상 설명한 바와 같은 본 발명의 특징 및 기타의 장점은 후술되는 실시예로부터 보다 명백하게 될 것이다.Features and other advantages of the present invention as described above will become more apparent from the following examples.

[실시예 1]Example 1

크래프트지 표면에 박리층용 왁스를 피복시킨 다음 흐름방지제를 함유하지 않은 투명 액상 실리콘 수지를 얇게 도포하고 건조하여 보호층을 형성하고, 그 위에 1차입경 12㎛, BET 표면적 200㎡/g인 에어로실 200(일본 아에로실사의 상품명) 13중량%의 양으로 분산시킨 투명 액상 실리콘 수지를 얇게 도포하고 건조하여 무늬인쇄층을 형성시킨 다음 오프셋 인쇄로 소망하는 무늬를 형성시켰다. 다음, 그 위에 백색 안료를 첨가하여 백색을 부여한 액상 실리콘 수지를 얇게 도포하고 건조하여 전사지를 제조하였다. 제조된 전사지를 수영모자용 탄성섬유재 원단 표면에 부착시키고 가열, 압착하여 전사인쇄한 후 원단을 늘여본 결과 흔들리거나 비틀림이 없는 선명한 무늬가 전사되었음을 확인할 수 있었다.After coating the release layer wax on the surface of the kraft paper, apply a thin layer of transparent liquid silicone resin containing no flow inhibitor, and dry it to form a protective layer, on which aerosil having a primary particle diameter of 12 µm and a BET surface area of 200 m 2 / g. A transparent liquid silicone resin dispersed in an amount of 13% by weight of 200 (trade name of Aerosil Japan Co., Ltd.) was thinly applied and dried to form a pattern printing layer, and then a desired pattern was formed by offset printing. Next, a white pigment was added thereto, and the liquid silicone resin giving a white color was applied thinly and dried to prepare a transfer paper. The prepared transfer paper was attached to the surface of the elastic fiber material for swimming caps, and transferred by heating and pressing, and then printed and stretched. As a result, it was confirmed that a vivid pattern without shaking or twisting was transferred.

이상 설명한 바와 같이 본 발명에 의하면 오프셋 인쇄방식으로 선명한 무늬를 부여할 수 있으며 실리콘 수지 고유의 탄성, 신축성, 내열성 및 방수성을 발현할 수 있는 고부가가치의 실리콘 전사지를 제조하는 것이 가능하게 된다.As described above, according to the present invention, it is possible to produce a high value-added silicone transfer paper capable of giving a vivid pattern by an offset printing method and expressing elasticity, elasticity, heat resistance, and waterproofness inherent in silicone resin.

Claims (4)

이형지 위에 보호층, 무늬인쇄층, 인쇄무늬 및 접착층이 순차적으로 형성된 실리콘 전사지에 있어서, 상기 무늬 인쇄층이 조면화된 표면을 가질 수 있는 정도의 양으로 흐름방지제를 함유한 액상 실리콘 수지로 형성되는 것을 특징으로 하는 오프셋 인쇄가능한 실리콘 전사지.A silicon transfer paper in which a protective layer, a patterned printing layer, a printed pattern, and an adhesive layer are sequentially formed on a release paper, wherein the patterned printing layer is formed of a liquid silicone resin containing a flow inhibitor in an amount sufficient to have a roughened surface. Offset printable silicone transfer paper, characterized in that. 제 1 항에 있어서, 상기 무늬인쇄층을 형성하는 액상 실리콘 수지 중 흐름방지제의 함량이 10∼20중량%인 것을 특징으로 하는 오프셋 인쇄가능한 실리콘 전사지.The offset printable silicone transfer paper according to claim 1, wherein the content of the flow inhibitor in the liquid silicone resin forming the pattern printing layer is 10 to 20% by weight. 다음의 단계를 포함하는 오프셋 인쇄가능한 실리콘 전사지의 제조방법:A method of making an offset printable silicone transfer paper comprising the following steps: 이형지에 투명한 액상 실리콘 수지를 도포하여 보호층을 형성하는 공정,Applying a transparent liquid silicone resin to the release paper to form a protective layer, 보호층 위에 조면화된 표면을 가질 수 있는 정도의 양으로 흐름방지제를 함유한 액상 실리콘 수지를 도포하여 조면화된 무늬인쇄층을 형성하는 공정,Forming a roughened pattern printing layer by applying a liquid silicone resin containing a flow inhibitor in an amount sufficient to have a roughened surface on the protective layer, 무늬인쇄층 위에 전사무늬를 오프셋 인쇄하는 공정, 및Offset printing the transfer pattern on the pattern printing layer, and 오프셋 인쇄된 무늬 인쇄층 위에 백색 안료를 함유하는 백색의 액상 실리콘 수지를 도포하여 접착층을 형성하는 공정.A step of forming an adhesive layer by applying a white liquid silicone resin containing a white pigment on an offset-printed patterned printing layer. 제 3 항에 있어서, 상기 접착층 위에 실리콘 러버 희석액을 도포하여 추가의 접착층을 형성한 후 그 위에 이형지를 적층시키는 공정을 더 포함하는 것을 특징으로 하는 오프셋 인쇄가능한 실리콘 전사지의 제조방법.4. The method of claim 3, further comprising the step of applying a silicone rubber diluent on the adhesive layer to form an additional adhesive layer and then laminating the release paper thereon.
KR10-2002-0001484A 2002-01-10 2002-01-10 Offset printable silicon transcription sheet and preparation thereof KR100488674B1 (en)

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KR100786216B1 (en) * 2006-11-09 2007-12-17 주식회사 에스에프에이 Print sheet comprising silicon and method for fabricating the same
KR101509406B1 (en) * 2014-09-24 2015-04-08 박자일 Printing Composition and Ceramic Transfer Paper Using the Same

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KR101069917B1 (en) * 2008-10-02 2011-10-05 주식회사 패트론 a cooking pot, and a method of manufacturing the same
KR102104963B1 (en) 2019-10-01 2020-04-27 이상우 Method for manufacturing silicon transfer sheet having top layer flocking

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KR100786216B1 (en) * 2006-11-09 2007-12-17 주식회사 에스에프에이 Print sheet comprising silicon and method for fabricating the same
KR101509406B1 (en) * 2014-09-24 2015-04-08 박자일 Printing Composition and Ceramic Transfer Paper Using the Same

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