KR20030038871A - Manufacturing of colloidal gold solution - Google Patents
Manufacturing of colloidal gold solution Download PDFInfo
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- KR20030038871A KR20030038871A KR1020010069019A KR20010069019A KR20030038871A KR 20030038871 A KR20030038871 A KR 20030038871A KR 1020010069019 A KR1020010069019 A KR 1020010069019A KR 20010069019 A KR20010069019 A KR 20010069019A KR 20030038871 A KR20030038871 A KR 20030038871A
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- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title claims abstract description 51
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000010931 gold Substances 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000009835 boiling Methods 0.000 claims abstract description 5
- 230000036541 health Effects 0.000 claims abstract description 4
- 239000004094 surface-active agent Substances 0.000 claims abstract description 4
- 150000003839 salts Chemical class 0.000 claims abstract description 3
- 235000015041 whisky Nutrition 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 9
- 239000012153 distilled water Substances 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 235000020083 shōchū Nutrition 0.000 claims description 2
- ZBKIUFWVEIBQRT-UHFFFAOYSA-N gold(1+) Chemical compound [Au+] ZBKIUFWVEIBQRT-UHFFFAOYSA-N 0.000 claims 2
- 206010019133 Hangover Diseases 0.000 claims 1
- 239000012267 brine Substances 0.000 claims 1
- 235000013336 milk Nutrition 0.000 claims 1
- 239000008267 milk Substances 0.000 claims 1
- 210000004080 milk Anatomy 0.000 claims 1
- 235000015205 orange juice Nutrition 0.000 claims 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 claims 1
- 230000001256 tonic effect Effects 0.000 claims 1
- 235000014101 wine Nutrition 0.000 claims 1
- 206010035664 Pneumonia Diseases 0.000 abstract description 5
- 208000002874 Acne Vulgaris Diseases 0.000 abstract description 3
- 208000000260 Warts Diseases 0.000 abstract description 3
- 206010000496 acne Diseases 0.000 abstract description 3
- 201000010099 disease Diseases 0.000 abstract description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 3
- 201000010153 skin papilloma Diseases 0.000 abstract description 3
- 206010010741 Conjunctivitis Diseases 0.000 abstract description 2
- 206010018612 Gonorrhoea Diseases 0.000 abstract description 2
- 206010024229 Leprosy Diseases 0.000 abstract description 2
- 208000001786 gonorrhea Diseases 0.000 abstract description 2
- 235000019997 soju Nutrition 0.000 abstract description 2
- 239000002105 nanoparticle Substances 0.000 abstract 2
- 208000037487 Endotoxemia Diseases 0.000 abstract 1
- 241000209094 Oryza Species 0.000 abstract 1
- 235000007164 Oryza sativa Nutrition 0.000 abstract 1
- 235000009566 rice Nutrition 0.000 abstract 1
- 235000019991 rice wine Nutrition 0.000 abstract 1
- 229910052737 gold Inorganic materials 0.000 description 26
- 239000002245 particle Substances 0.000 description 19
- 235000013361 beverage Nutrition 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- -1 gold ions Chemical class 0.000 description 4
- 238000005868 electrolysis reaction Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 235000013334 alcoholic beverage Nutrition 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 208000008589 Obesity Diseases 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 206010003246 arthritis Diseases 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000003925 brain function Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 210000002751 lymph Anatomy 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000036314 physical performance Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 235000019992 sake Nutrition 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/15—Inorganic Compounds
- A23V2250/156—Mineral combination
- A23V2250/1568—Gold
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G2200/00—Special features
- C12G2200/21—Wine additives, e.g. flavouring or colouring agents
Abstract
Description
본 발명은 금 콜로이드의 제조에 관한 것으로서, 보다 구체적으로는 콜로이드 골드가 약주, 소주, 청주, 위스키 등의 각종 주류 또는 건강음료에 첨가할 수 있는 콜로이드 골드용액에 관한 것이다.The present invention relates to the production of gold colloids, and more particularly, to a colloidal gold solution that colloidal gold can be added to various alcoholic beverages or health drinks such as medicine, shochu, sake, whiskey and the like.
금(Gold)의 학명은 Aurumdm으로 아침의 태양 광선 또는 찬란히 빛나는 아침 햇빛의 의미를 지니고 있다. 금은 고대 오리엔트 문명으로부터 시작하여 인류와 인연을 맺어 온 금속으로서 지난 6 천년동안 영구성과 불변의 가치를 지니고 있어 여러 나라에서 중요한 자산 보전 수단이 되어 왔다. 금은 녹슬지 않으며, 변하지도 않으며 인체에 아무런 해가 없으며 오히려 독을 없애고 건강하게 하므로 각종 악세사리를 만들어 착용하거나 금가루를 술에 타먹기도 하여 왔다. 특히 금은 두뇌작용을 촉진시킬 뿐만 아니라 항암, 관절염, 비만, 소화촉진, 피부미용 등 다방면에 걸쳐 효력이 있는 것으로 알려져 있으며 미세 입자가 분산되어진 콜로이드 골드의 경우에는 감기, 결막염, 임질, 나병, 임파선, 폐렴, 류머티즘, 폐혈증, 사마귀, 여드름에 이르기까지 거의 모든 질환에 효과가 있는 것으로 알려져 있다.Gold's scientific name is Aurumdm, which means morning sun rays or brilliant morning sunlight. Gold is a metal that has been associated with humanity since ancient Orient civilization, and has been an important asset preservation tool in many countries for its last six thousand years of permanent and constant value. Gold does not rust, does not change, does no harm to the human body, rather detoxify and health, so make a variety of accessories to wear or wear gold powder to drink alcohol. In particular, gold is known not only to promote brain function, but also to be effective in various fields such as anti-cancer, arthritis, obesity, digestion, and skin beauty. It is known to be effective in almost all diseases, including pneumonia, rheumatism, pneumonia, warts and acne.
입자의 활용기술에서 입자의 크기가 미세단위 (30 nm이하)로 작게되면 입자의 물성 및 성능이 입자 크기가 μm 이상인 경우와는 매우 다르게 된다. 이는 입자의 표면 대 질량의 비율이 증가되어 단위 질량당 표면적이 증가되어 입자의 성능이 향상되고 입자의 융점이 감소되는 등 물성이 변화되며 입자의 색상까지 크기에 따라 변화되는 등 큰 입자의 경우와는 다른 성질을 나타낸다. 특히 입자의 효용면에서 보면 입자크기가 작을수록 그 효과는 더욱 커지게 되는데 기존의 주류에 포함된 금박 또는 금가루는 순금을 금박으로 하여 첨가한 것이므로 상대적으로 크기가 커서 효과가 그만큼 반감되는 단점이 있었다. 즉, 같은 양의 금을 넣더라도 전체적으로 균일하게 섞이는 것이 아니라 불균일하게 알갱이가 섞여 있어서 일부 용액중에는 전혀 포함되지 않을 수도 있어서 전체적으로 균일한 상태의 용액으로 만들어야 할 개선점이 있었다.When the particle size is reduced to fine units (less than 30 nm) in the particle utilization technology, the physical properties and performance of the particle are very different from those when the particle size is larger than μm. This is due to the increase in the surface-to-mass ratio of the particles, which increases the surface area per unit mass, which improves the performance of the particles, decreases the melting point of the particles, and changes the properties of the particles. Has different properties. In particular, the smaller the particle size, the more effective the effect becomes.In the existing liquor, the gold leaf or gold powder contained in pure gold was added to gold leaf, so the size was relatively large and the effect was halved. . In other words, even if the same amount of gold is not mixed uniformly as a whole, the grains are mixed unevenly, so some solutions may not be included at all, so there is an improvement to make the solution in an overall uniform state.
따라서 본 발명에서는 상기한 바와 같은 선행 기술의 단점을 감안하여 나노미터 크기의 골드 콜로이드를 제조함으로써 금박 대신 음료에 첨가하여 전체적으로 고르게 나노미터의 미세 금 입자가 포함된 기능성 음료 등을 만들 수 있는 것이다.Therefore, in the present invention, by preparing a nanometer-sized gold colloid in view of the disadvantages of the prior art as described above, it is possible to make functional drinks containing nanometer fine gold particles evenly by adding them to beverages instead of gold foil as a whole.
일반적으로 콜로이드 골드는 전기 분해를 통해 쉽게 얻을 수 있다. 가는 금봉 두 개를 증류수가 담긴 플라스틱 통에 담근 후, 가는 금봉 두 끝을 30 볼트나 9 볼트 배터리 3개를 직렬로 연결시켜 전기를 흘려주면 미세 금 이온내지는 입자들이 분산되어 있는 콜로이드 금용액을 얻을 수 있으나 가격 농도 안정성 등 문제로 상업화 하기가 힘들다. 따라서 본 발명에 의하여 화학적인 방법에 의하면 나노미터의 금이 분산된 콜로이드 골드를 만들 수 있다. 화학적인 방법에 의해 콜로이드 골드를 얻을 경우에는 인체에 직접 식용되는 것이므로 인체에 유해한 성분이 없는 것이 중요하다. 전기 분해법에 비해 화학적 방법은 짧은 시간 내에 대량의 콜로이드 골드를 제조할 수 있다는 장점을 지니고 있다. 따라서 본 발명에서는 수-수십 나노미터의 금이 분산되어 있는 인체에 유해 성분이 없는 콜로이드 골드를 제조하는 것이다. 또한 이를 각종 음료에 첨가함으로써 기존의 금이 첨가된 소주를 비롯한 각종 주류에 비해 경제성과 효능이 탁월한 새로운 기능성 주류를 제조하고자 한다.In general, colloidal gold is easily obtained through electrolysis. Dip two fine gold bars into a plastic bucket of distilled water, and connect two ends of the thin gold bars in series with three 30 volt or 9 volt batteries in series to give a colloidal gold solution in which fine gold ions are dispersed. However, it is difficult to commercialize due to price stability. Therefore, according to the chemical method according to the present invention, it is possible to make colloidal gold in which nanometer gold is dispersed. When the colloidal gold is obtained by a chemical method, since it is directly edible to the human body, it is important that there is no harmful component to the human body. Compared to the electrolysis method, the chemical method has the advantage of producing a large amount of colloidal gold in a short time. Therefore, the present invention is to produce a colloidal gold that is harmful to the human body is dispersed in the tens of tens of nanometers of gold. In addition, by adding this to a variety of beverages, it is intended to produce a new functional liquor excellent in economics and efficacy compared to various liquors including the existing soju added gold.
수용성의 Au 염이 녹은 수용액을 끓는 물에 추가하고 여기에 인체에 무해한 계면활성 물질을 미량 첨가한 다음 일정 시간 동안 이를 다시 함께 끓여준다. 계면활성제 분자는 계면에 흡착하고자하는 고유의 성질 때문에 금이온이 환원되어 입자가 형성되는 용액 내에서 금 입자 핵의 표면에 흡착하여 핵끼리의 융합을 막아주며 환원된 금 원자들이 핵 표면으로 결합되는 것을 지연 또는 막아 크기분포가 균일한 나노미터의 금 입자가 제조되도록 하는 역할을 한다. 너무 온도를 높이거나 오래 끓여주게 되면 환원된 금 입자들이 서로 클러스터를 형성하여 바닥에 침전하게 되며, 불균일한 크기의 금입자가 얻어지게 되므로 적절한 가열 온도 및 시간이 요구된다. 금의 정확한 농도 조절을 위해서는 반응 후 증류수를 일정량 가하여 주면 원하는 농도의 콜로이드 골드를 얻을 수 있다.Aqueous solution of water-soluble Au salt is added to boiling water, and a small amount of a surface active substance that is harmless to the human body is added thereto and then boiled together again for a predetermined time. Due to the inherent nature of the surfactant molecules to be adsorbed at the interface, gold ions are reduced to adsorb on the surface of the gold particle nuclei in the solution in which the particles are formed, thereby preventing fusion between the nuclei, and the reduced gold atoms are bonded to the surface of the nucleus. It delays or prevents a nanometer of gold particles having a uniform size distribution. If the temperature is too high or boiled for a long time, the reduced gold particles form clusters with each other and settle on the bottom, and gold particles of non-uniform size are obtained, so that proper heating temperature and time are required. In order to adjust the concentration of gold, a certain amount of distilled water is added after the reaction to obtain a colloidal gold of a desired concentration.
일반적으로 주류를 제조함에 있어서는 숙성 과정을 거치게 되는데 이는 주로 물과 알코올 분자가 서로 바뀌면서 서로의 분자가 공존하는 새로운 클러스터를 형성하는 과정이다. 이러한 과정을 거침으로써 알콜의 자극취가 줄어들게 되고 맛이순화되어지며, 보다 깊은 맛이 만들어지게 된다. 주류의 경우 알코올 성분이 반드시 포함되게 되는데, 전기 분해에 의해 얻어진 순금이온이 녹아 있는 콜로이드 골드를 넣어주게 되면 알코올에 의해 금 이온이 환원되어 나중에는 금 입자들끼리 뭉쳐 덩어리로 침전되므로 결국은 불균일한 주류 용액을 얻을 수밖에 없다. 그러나 본 발명에 의해 얻어진 콜로이드골드는 나노미터의 입자가 분산된 콜로이드를 사용하므로 추가적인 환원이 거의 일어나지 않아 안정한 상태로 분산되어 있어 나노미터의 금 입자가 고루 분산된 음료 등를 얻을 수 있다.In general, the liquor is aged in the process of producing liquor, which is a process of forming a new cluster in which water and alcohol molecules are interchanged with each other. This process reduces the irritant odor of alcohol, refines the taste, and creates a deeper taste. In the case of alcoholic beverages, alcohol must be included, but when colloidal gold is dissolved in pure gold ions obtained by electrolysis, the gold ions are reduced by alcohol, and later, the gold particles gather together and settle into lumps. You have no choice but to get a liquor solution. However, since the colloidal gold obtained by the present invention uses a colloid in which nanometer particles are dispersed, additional reduction hardly occurs and is dispersed in a stable state, thereby obtaining a beverage in which nanometer gold particles are evenly dispersed.
본 발명의 효과로는 인체에 전혀 무해하며 감기, 결막염, 임질, 나병, 임파선, 폐렴, 류머티즘, 폐혈증, 사마귀, 여드름에 이르기까지 거의 모든 질환에 효과가 있는 것으로 알려진 콜로이드 골드를 제조하는 것이며 또한 주류, 음료, 각종제약에 첨가함으로써 기능을 향상시킬 수 있다. 특히 기존 음료에 포함된 금박과는 달리 나노미터의 골드가 용액 전체에 고루 분산되어 있으므로 효과면에서도 보다 탁월한 음료를 제조할 수 있다. 또한 기존의 금박 대신 나노미터 크기의 미세 금 입자가 분산된 콜로이들 골드를 사용함으로써 보다 적은 양으로서 동일 내지는 그 이상의 효과를 얻을 수 있다.The effect of the present invention is to produce colloidal gold known to be harmless to the human body and is effective in almost all diseases including colds, conjunctivitis, gonorrhea, leprosy, lymph glands, pneumonia, rheumatism, pneumonia, warts and acne. By adding it to beverages, various pharmaceuticals, the function can be improved. In particular, unlike the gold leaf included in the existing beverage, nanometer gold is evenly dispersed throughout the solution, so it is possible to produce a beverage that is more effective in terms of effect. In addition, by using colloidal gold in which nanometer-sized fine gold particles are dispersed instead of the existing gold foil, the same or more effect can be obtained in a smaller amount.
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| KR20180079276A (en) * | 2018-07-02 | 2018-07-10 | (주) 아이나노 | Hangovers dringking raw materials and dietary supplement containing nano gold particles, and manufacturing method thereof |
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