KR20020013021A - Manufacturing method of monofilament - Google Patents
Manufacturing method of monofilament Download PDFInfo
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- KR20020013021A KR20020013021A KR1020000046352A KR20000046352A KR20020013021A KR 20020013021 A KR20020013021 A KR 20020013021A KR 1020000046352 A KR1020000046352 A KR 1020000046352A KR 20000046352 A KR20000046352 A KR 20000046352A KR 20020013021 A KR20020013021 A KR 20020013021A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/02—Heat treatment
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D4/00—Spinnerette packs; Cleaning thereof
- D01D4/02—Spinnerettes
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
- D01D5/098—Melt spinning methods with simultaneous stretching
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/253—Formation of filaments, threads, or the like with a non-circular cross section; Spinnerette packs therefor
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/12—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyamide as constituent
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- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Artificial Filaments (AREA)
Abstract
Description
본 발명은 방사작업성이 우수한 모노필라멘트(monofilament)의 제조방법에 관한 것으로서, 더욱 상세하게는 모노필라멘트(monofilament) 제조시 섬유의 방사 단계에서, 방사구금에서 부터 권취기까지 1단계의 공정으로 1가닥의 모노필라멘트(monofilament)를 생산이 가능토록 설계하였으며 필요시 이를 2 내지8 가닥까지 합사도 가능 하도록 하였고, 고유점도가 0.9 내지 0.95인 폴리트리메틸테레프탈레이트(polytrimethyleneterephthalate), 고유점도가 0.48 내지 0.8 인 폴리에틸렌테레프탈레이트(polyethyleneterephthalate), 상대점도가 2.30 내지 3.0 폴리아미드(polyamide)를 원료수지로 하여 부드러운 촉감을 내는 모노필라멘트(monofilament)를 가장 효율적인 조건을 구비하여 안정적으로 제조하는 방법에 관한 것이다.The present invention relates to a method for producing a monofilament (monofilament) excellent spinning work, and more particularly, in the spinning step of the fiber during the production of monofilament (monofilament), from a spinneret to a winder in one step The monofilament of the strands is designed to be produced, and if necessary, it is possible to ply them up to 2 to 8 strands, polytrimethyleneterephthalate having an intrinsic viscosity of 0.9 to 0.95, and has an intrinsic viscosity of 0.48 to 0.8. The present invention relates to a method for stably producing monofilaments that give a soft touch with polyethylene terephthalate and relative viscosities of 2.30 to 3.0 polyamide as the raw material resins with the most efficient conditions.
종래의 모노필라멘트(monofilament) 제조방법은 방사공정(100)에서 섬유의 가닥수를 10내지 12가닥으로 제조하여, 사용시 다시 10 내지 12 가닥으로 구성된 섬유를 각각 1가닥으로 분리하는 분섬공정(200)을 거쳐 사용하여 결과적으로 에너지 비용의 과다 및 운반과 취급시 섬유가 선상되는 문제점이 있었다. 또한 합성섬유는 다른 천연섬유들에 비해서 우수한 물리적, 화학적 내구성을 구비하여 여러 소재로 널리 이용되고 있는 반면, 그의 밋밋한 촉감이나 단조로운 외관의 한계라는 문제점이 있었다.Conventional monofilament (monofilament) manufacturing method in the spinning process 100 to produce a number of strands of fiber 10 to 12, the splitting process 200 to separate each of the fibers consisting of 10 to 12 strands in use in each use 200 As a result, there was a problem that the excess of the energy cost and the fiber is carried on handling and handling. In addition, synthetic fibers have excellent physical and chemical durability compared to other natural fibers, while being widely used in various materials, there is a problem of their soft touch or monotonous limitations.
본 발명은 전술한 문제점을 해결하기 위해 고안한 것으로서, 효율적인 작업성과 비용의 절감과 아울러, 가공성, 부드러운 촉감과 이염성 및 고발색성, 청량감, 신축성을 가진 모노필라멘트(monofilament)를 제조하는 것을 목적으로 한다.The present invention has been devised to solve the above problems, and aims at producing monofilaments having workability, soft touch and dyeability and high colorability, coolness, and elasticity, as well as efficient workability and cost reduction. do.
상기 발명은 전술한 목적을 달성하기 위하여 모노필라멘트(monofilament) 제조시 섬유의 방사단계의 방사구금에서 부터 귄취기까지 1단계의 공정으로 1가닥의 모노필라멘트(monofilament)를 생산하는 것이 가능토록 설계되었으며 필요시 이를2 내지 8 가닥까지 합사도 가능하도록 하였고, 고유점도가 0.9 내지 0.95인 폴리트리메틸테레프탈레이트(polytrimethyleneterephthalate), 고유점도가 0.48 내지 0.80인 폴리에틸렌테레프탈레이트(polyethyleneterephthalate), 상대점도가 2.30 내지 3.0인 폴리아미드(polyamide)를 원료수지로 사용하여 미연신 모노필라멘트(monofilament), 부분 미연신 모노필라멘트(monofilament), 연신 모노필라멘트(monofilament)를 제조하는 방법을 제공한다.In order to achieve the above object, the present invention is designed to produce one strand of monofilament in a one-step process from spinneret of spinning step of fiber to odor odor when manufacturing monofilament. If necessary, it is possible to ply to 2 to 8 strands, polytrimethyleneterephthalate having an intrinsic viscosity of 0.9 to 0.95, polyethylene terephthalate having an intrinsic viscosity of 0.48 to 0.80, and a relative viscosity of 2.30 to 3.0. Provided is a method for producing undrawn monofilament, partially undrawn monofilament, and drawn monofilament using polyamide as a raw material resin.
도 1은 종래의 멀티필라멘트 제조 개략도.1 is a schematic view of manufacturing a conventional multifilament.
도 2는 본 발명인 모노필라멘트의 제조 개략도.Figure 2 is a production schematic of the present invention monofilament.
도 3은 가이드 장치를 제거한 모노필라멘트의 제조 개략도.3 is a production schematic of the monofilament with the guide device removed.
< 도면의 주요부분에 대한 부호의 간단한 설명 ><Brief description of symbols for the main parts of the drawings>
1,10 : 가이드 2,20 : 1차 고뎃롤러1,10: Guide 2,20: 1st gore roller
3,30 : 2차 고뎃롤러 4,40 : 권취기3,30: Secondary roller roller 4,40: Winding machine
50 : 냉각장치 60 : 방사구금50: cooling device 60: spinneret
100 : 방사공정 200 : 분섬공정100: spinning process 200: splitting process
300 : 분섬후 원사300: yarn after splitting
본 발명은 모노필라멘트(monofilament)의 제조방법에 있어서, 섬유를 냉각장치(50)에서 방사를 하고 방사구금(60)을 통과하여 가이드(10)에 거취되고 1차 고뎃롤러(20)와 2차 고뎃롤러(30)에서 형태를 유지하며 귄취기(40)에서 섬유를 감는 속도롤 조절하여 미연신, 부분미연신, 연신 모노필라멘트(monofilament)를 제조하는 것으로서, 방사단계의 방사구금(60)에서 부터 권취기(40)까지 한 단계의 공정으로 1가닥의 모노필라멘트(monofilament)를 생산이 가능토록 설계하였으며 필요시 이를 2 내지 8 가닥까지 합사도 가능 하도록 하였고, 제조방법에서 사용되는 폴리트리메틸테레프탈레이트(polytrimethyleneterephthalate)는 고유점도가 0.9 내지 0.95이며 폴리에틸렌테레프탈레이트(polyethyleneterephthalate)는 고유점도가 0.48 내지 0.80, 폴리아미드(polyamide)는 상대점도가 2.40 내지 3.0인 수지원료를 사용하고, 귄취속도는 미연신사 경우 800 내지 1500m/min이 적정이며, 부분연신사 혹은 연신사 경우 방사 속도범위는, 부분연신사 및 연신사의 원사강도를 2g/d(그램/데니어) 이상으로 할 수 있고, 염색성도 양호한 3100 내지 49 00m/min으로 하는 것을 특징으로 한다.The present invention is a method for producing a monofilament (monofilament), the fiber is spun in the cooling device 50 and passed through the spinneret 60 is taken in the guide 10 and the first gourd roller 20 and the second By maintaining the shape in the roller roller 30 and adjusting the speed of winding the fiber in the odor blowing machine 40 to produce undrawn, partially undrawn, drawn monofilament (monofilament), in the spinneret 60 of the spinning step To winder (40) in a one step process to produce a monofilament (monofilament) of one strand was designed to enable it to be possible to ply 2 to 8 strands, polytrimethyl terephthalate used in the manufacturing method polytrimethyleneterephthalate has an intrinsic viscosity of 0.9 to 0.95, polyethyleneterephthalate has an intrinsic viscosity of 0.48 to 0.80, and polyamide has a relative viscosity of 2.40 to 3.0. The raw material is used and the odor speed is 800 ~ 1500m / min for non-drawn yarn, and the spinning speed range for partially drawn or drawn yarn is more than 2g / d (gram / denier) of yarn strength for partially drawn or drawn yarn. It can be set as 3100-49 00m / min which is also excellent in dyeability, It is characterized by the above-mentioned.
이하 본 발명인 모노필라멘트(monofilament)의 제조방법의 가장 효율적인 작업조건에 대해서 상술하면, 기본적으로 원사의 굵기는 10 내지 70데니어(De')가 적합하나 더 상세하게는 15 내지 60데니어(De')경우가 가장 바람직한 범위이다. 70데니어(De')이상일 경우 방사섬도가 지나치게 커서 냉각이 불충분하여 방사작업성이 불량해지며 방사유체 부착이 불량하여 귄취케이크(40)의 형태도 불량해진다.Hereinafter, the detailed description of the most efficient working conditions of the manufacturing method of the monofilament (monofilament) of the present invention, the thickness of the yarn is basically 10 to 70 denier (De ') but more specifically 15 to 60 denier (De') The case is the most preferred range. If it is 70 denier (De ') or more, the radiation fineness is too large, insufficient cooling, poor spinning workability, poor adhesion of the spinning fluid is also bad shape of the odor cake (40).
방사온도는 290℃ 이상이면 고분자의 원료수지가 열화하기 쉽고 250℃ 이하의 온도에서는 방사작업성이 불량해지므로 250℃ 내지 285℃가 적합하고, 냉각공기의 온도는 15℃ 내지 18℃에서, 풍속은 60mmH20 이하일 경우 원사가 충분히 고화되기 어렵고 100mmH20 이상일 경우는 방사시 사조에서 필라멘트(filament)의 유동이 상하여 이웃하는 필라멘트(filament)간에 순간접합이 일어나거나 방사작업성이 저하되고 사균제도 즉, 굵기의 균일성이 저하되므로 60 내지 100mmH20가 적합니다.If the spinning temperature is 290 ° C or higher, the raw material resin of the polymer is easily deteriorated, and the spinning workability is poor at the temperature of 250 ° C or lower, so 250 ° C to 285 ° C is suitable, and the temperature of the cooling air is 15 ° C to 18 ° C. When 60mmH20 or less, the yarn is hard to solidify sufficiently, and when 100mmH20 or more, the flow of filament is damaged in the yarn during spinning, which causes instant bonding between neighboring filaments or decreases the workability of the yarn. Uniformity is reduced, so 60 to 100mmH20 is less.
냉각통 직하에는 원사가 고화되지 않아서 방사작업성이 불량하거나 권취자체가 불가능해질 수 있으므로 냉각효과를 극대화 시켜주기 위하여 가이드(10)를 사용하거나 자연냉각사조를 늘려 냉각고화를 충분히 시켜 주어야 한다.Since the yarn is not solidified directly under the cooling tube, the radioactive workability may be poor or the winding itself may be impossible. Therefore, in order to maximize the cooling effect, the guide 10 should be used or the natural cooling yarn should be increased to sufficiently solidify the cooling.
미연신사 경우 방사속도를 800 내지 1500m/min로 생산한 모노필라멘트 (monofilament)를 연신기에서 연신비 1.5 내지 3.5범위로 연신하며, 부분 연신사 경우 방사속도 3100 내지 4300m/min범위 에서 1,2차 고뎃롤러(Godet roller)(20,30)의 온도를 상온에서 생산하며, 연신사의 경우 1차 고뎃롤러(20)의 온도를 상온 내지 70℃, 2차 고뎃롤러(30)의 온도를 60℃ 내지 140℃로 하여 방사속도를 3800 내지 4700m/min에서 제조한다.In the case of undrawn yarn, the monofilament produced at a spinning speed of 800 to 1500 m / min is drawn in the drawing machine at a draw ratio of 1.5 to 3.5, and in the case of partially drawn yarn, the first and second high-fibers in the spinning speed of 3100 to 4300 m / min are used. The temperature of the rollers (Godet roller) (20,30) is produced at room temperature, and in the case of stretched yarns, the temperature of the first gourd roller 20 is from room temperature to 70 ° C., and the temperature of the second gourd roller 30 is from 60 ° C. to 140 °. The spinning speed is prepared at 3800 to 4700 m / min.
또한 섬유단면 형상은 방사구금의 형태를 원형, 이형단면(△형, □형, Y형, +형)으로 하여 방사구금을 통과한 섬유가 전술한 형상을 가지게 한다.In addition, the fiber cross-sectional shape is the shape of the spinneret is circular, the shape of the cross section (△ type, □ type, Y type, + type) so that the fiber passed through the spinneret has the above-described shape.
이하 본 발명인 모노필라멘트(monofilament)의 제조방법에 따른 실시예와 비교예를 들어서 상술하고자 한다.Hereinafter, the present invention will be described in detail by way of examples and comparative examples according to the manufacturing method of the monofilament (monofilament).
실시예 1Example 1
고유점도가 0.92인 폴리트리메틸테레프탈레이트(polytrimethylenetere- phthalate) 수지를 사용하여 열풍건조기에서 140℃에서 5시간 이상 건조한 후 통상의 방사기를 사용하여 모노필라멘트(monofilament)를 제조하였고, 이때 방사온도는 255℃, 방사속도는 3800m/min, 냉각풍온도는 17℃이고 풍량은 90mmH20였다. 그리고 냉각장치 직하에 가이드(10)를 사용하여 본 실시예의 물성 및 공정변수를 표1에 나타내었다.Monofilament was prepared using a conventional spinner after drying at 140 ° C. for 5 hours or more in a hot air dryer using a polytrimethylene terephthalate resin having an intrinsic viscosity of 0.92, wherein the spinning temperature was 255 ° C. , Spinning speed was 3800m / min, cooling wind temperature was 17 ℃ and air flow was 90mmH20. And the physical properties and process parameters of this embodiment using the guide 10 directly under the cooling device are shown in Table 1.
실시예 2Example 2
폴리트리메틸테레프탈레이트(polytrimethyleneterephthalate) 수지 대신 고유점도 0.6의 폴리에틸렌테레프탈레이트(polyethyleneterephthalate) 수지를 사용 방사온도 285℃로 한것을 제외하고는 실시예1과 동일한 절차를 반복하였다.The same procedure as in Example 1 was repeated except that a polyethyleneterephthalate resin having an intrinsic viscosity of 0.6 was used instead of the polytrimethyleneterephthalate resin to a spinning temperature of 285 ° C.
실시예 3Example 3
실시예 1에서 원료수지를 폴리트리메틸테레프탈레이트(polytrimethy- leneterephthalate) 대신 상대점도 2.40-3.0의 폴리아미드(polyamide) 수지와 건조온도는 100℃ 에서 4시간 건조하여 미연신사 경우 방사속도를 110-1250m/min로 생산후 연신비 1.5 내지 3.5 범위에서 처리 하였다. 부분 연신사 경우 방사속도를 4100m/min에서 1,2차 고뎃롤러(Godet roller)(20,30)를 상온에서 처리하였다. 연신사 경우 1차 고뎃롤러(Godet roller)(20)의 온도를 상온내지 60℃범위와 2차 고뎃롤러(Godetroller)(30)의 온도범위를 80-160℃로 하여 모노필라멘트 (monofilament)를 제조하였다.In Example 1, the polyamide resin having a relative viscosity of 2.40-3.0 and a drying temperature were dried at 100 ° C. for 4 hours instead of polytrimethyleneterephthalate in the raw material resin, so that the spinning speed was 110-1250 m / After production in min was treated in the draw ratio 1.5 to 3.5 range. In the case of the partially drawn yarn, the first and second Goodet rollers (20, 30) were treated at room temperature at a spinning speed of 4100 m / min. In the case of the stretched yarn, monofilament is produced by using the temperature of the first goth roller 20 at room temperature to 60 ° C. and the temperature range of the second goth roller 20 at 80-160 ° C. It was.
비교예 1Comparative Example 1
냉각풍의 풍량을 60mmH20로 변경한 것을 제외하고는 실시예1과 동일한 절차를 반복하였다.The same procedure as in Example 1 was repeated except that the air volume of the cooling wind was changed to 60 mmH20.
비교예 2Comparative Example 2
냉각장치 직하에 가이드(10) 없이 방사하는 것을 제외하고는 실시예1과 동일한 절차를 반복하였다.The same procedure as in Example 1 was repeated except that spinning without a guide 10 underneath the chiller.
○ : 우수함. △ : 보통.(Circle): Excellent. (Triangle | delta): Normal.
X : 나쁨 또는 능락 및 벌자 발생정도가 심함.X: Possibility of bad or plunging and bee
전술한 바와 같이 본 발명은 작업성, 가공성, 부드러운 촉감과 이염성 및 고발색성, 청량감, 신축성을 가진 모노필라멘트(monofilament)사를 제조할 수 있는 효과가 있다.As described above, the present invention has the effect of producing a monofilament (monofilament) yarn having workability, processability, soft touch and dyeability and high colorability, coolness, and elasticity.
Claims (6)
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KR1020000046352A KR20020013021A (en) | 2000-08-10 | 2000-08-10 | Manufacturing method of monofilament |
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KR1020000046352A KR20020013021A (en) | 2000-08-10 | 2000-08-10 | Manufacturing method of monofilament |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100419336B1 (en) * | 2001-12-12 | 2004-02-21 | 도레이새한 주식회사 | Manufacturing method of highly brightend and soften polyester shaped fiber and raising warp kitting fabric knitted up thereof |
KR20060079522A (en) * | 2004-12-31 | 2006-07-06 | 주식회사 효성 | Process for preparing easily subdivisible antibacterial polyamide yarn |
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JPS61282410A (en) * | 1985-06-04 | 1986-12-12 | Unitika Ltd | Method for high-speed spinning |
JPH01174610A (en) * | 1987-12-25 | 1989-07-11 | Toray Ind Inc | Direct spinning and drawing of polyester yarn |
KR930011316A (en) * | 1991-11-07 | 1993-06-24 | 이헌조 | Optical logic device and its manufacturing method |
JPH05295617A (en) * | 1992-04-15 | 1993-11-09 | Toray Ind Inc | Production of polyester monofilament for screen gauze |
KR950005426A (en) * | 1993-08-17 | 1995-03-20 | 츠지 요시후미 | Precursor |
KR100315506B1 (en) * | 1995-10-06 | 2002-02-19 | 구광시 | Production of polyurethane elastic yarn |
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2000
- 2000-08-10 KR KR1020000046352A patent/KR20020013021A/en not_active Application Discontinuation
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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JPS61282410A (en) * | 1985-06-04 | 1986-12-12 | Unitika Ltd | Method for high-speed spinning |
JPH01174610A (en) * | 1987-12-25 | 1989-07-11 | Toray Ind Inc | Direct spinning and drawing of polyester yarn |
KR930011316A (en) * | 1991-11-07 | 1993-06-24 | 이헌조 | Optical logic device and its manufacturing method |
JPH05295617A (en) * | 1992-04-15 | 1993-11-09 | Toray Ind Inc | Production of polyester monofilament for screen gauze |
KR950005426A (en) * | 1993-08-17 | 1995-03-20 | 츠지 요시후미 | Precursor |
KR100315506B1 (en) * | 1995-10-06 | 2002-02-19 | 구광시 | Production of polyurethane elastic yarn |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100419336B1 (en) * | 2001-12-12 | 2004-02-21 | 도레이새한 주식회사 | Manufacturing method of highly brightend and soften polyester shaped fiber and raising warp kitting fabric knitted up thereof |
KR20060079522A (en) * | 2004-12-31 | 2006-07-06 | 주식회사 효성 | Process for preparing easily subdivisible antibacterial polyamide yarn |
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