KR102087120B1 - Detergent, softener and fabric deoderizer compostion containing probiotics - Google Patents

Abstract

The present invention relates to a detergent composition, a softener composition, and a deodorant composition containing probiotics, capable of improving washing power. The detergent composition of the present invention comprises 0.1 to 15 parts by weight of probiotics with respect to 100 parts by weight of the detergent composition.

Description

Detergent, softener and fabric deoderizer compostion containing probiotics

The present invention relates to detergent compositions, softener compositions and deodorant compositions containing probiotics.

Republic of Korea Patent No. 1624951 (Registration date: May 23, 2016, Name of the invention: laundry detergent composition containing lacquer extract) is at least one selected from salt, sugar, heavy ash, forget-me-not, bentonite and silicate relative to the total amount of the detergent composition 50 to 95% by weight of the particulate matter and 5 to 15% by weight of the urushiol-removed lacquer extract, wherein the lacquer extract is extracted using at least one extraction method selected from hydrothermal extraction, enzyme extraction and fermentation extraction. A detergent composition for garments is disclosed.

This prior art has excellent antibacterial effect by removing the urushiol, which is a toxic ingredient contained in lacquer, and granulating the lacquer extract with a high content of flavonoids, and has a particle containing the lacquer extract from which the urushiol is removed from the lacquer. Including the detergent, excellent storage stability and excellent antimicrobial properties can provide a clothing detergent composition that is not irritating to the skin, while there is a fundamental problem that can cause irritation to sensitive skin.

In addition, Republic of Korea Patent No. 1269647 (Registration date: May 24, 2013, Name of the invention: natural kitchen detergent composition comprising a fermentation extract of garlic and onion and a method for producing the same) garlic peel, garlic stem, and onion peel After fermenting at least one material selected from the group consisting of at a temperature of 60 ℃ to 70 ℃ without adding water, the fermented extract obtained by hot water extraction in the water (water) as an active ingredient, On the basis of 100% by weight of the natural kitchen detergent composition, at least one material selected from the group consisting of garlic peel, garlic bar, and onion peel after fermentation at a temperature of 60 ℃ to 70 ℃ without adding water to the fermentation 60% to 80% by weight of the fermented extract obtained by hydrothermal extraction of the prepared material in water, 5% to 1% by weight of thickener, 1% by weight of neutralizer 6% by weight, viscosity increases private use surfactant is a natural dishwashing detergent compositions disclosed containing 9 to 15 wt%, foam-forming agent 9 to 15% by weight, and 5 to 8% by weight of humectant.

This conventional technology is made of natural ingredients to prevent environmental pollution and water saving effect, and can use the garlic stand, garlic peel, onion peel, etc., which are discarded as conventional waste, greatly reducing the amount of garbage. While claiming to have, there was a disadvantage that the washing power is lowered.

An object of the present invention created to solve the above problems is to provide a detergent composition containing probiotics that can improve the washing power.

Another object of the present invention is to provide a deodorant composition containing probiotics that can remove odors of clothing or fibers.

It is still another object of the present invention to provide a softener composition containing probiotics capable of softening clothing or textiles.

The object of the present invention, 0.1 to 15 parts by weight of probiotics with respect to 100 parts by weight of detergent composition, the probiotics include Bacillus, Lactobacillus, Lactococcus, Enterococcus, Streptococcus and Bifidobacteria , The Bacillus bacteria are any one or more of Bacillus coagulans, Bacillus subtilis , The Lactobacillus bacteria Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgaricus, Lactobacillus helvactoba, Lactobacillus Lactobacillus Lactobacillus and Lactobacillus rhamnosus, Lactobacillus salivarius over any of one, the Lactococcus strain is Lactococcus lactis, Enterococcus the bacteria Enterococcus faecium, and any one or more of Enterococcus faecalis, wherein the Streptococcus strain is Streptococcus thermophilus, the Bifidobacteria are Bifidobacterium bifidum, Bifidobacterium breve, Bifidobacterium longum , Bifidobacterium animalis ssp. Any one or more of lactis , and further comprises 10 to 150 parts by weight of the fiber deodorant extract based on 100 parts by weight of the probiotics, wherein the fiber deodorant extract, (a) 100 to 45 parts by weight of apple rind powder And 0.5 to 1.5 parts by weight of grapefruit seed extract, and then heated at 180 to 250 ° C. for 300 to 350 minutes, and then cooled to 30 to 50 ° C., followed by further mixing 0.1 to 0.5 parts by weight of acetic acid and filtering to prepare a filtrate. Doing; (b) to 100 parts by weight of the filtrate, 1.5 to 3 parts by weight of citric acid and 0.05 to 0.1 parts by weight of the turpent extracts are mixed and prepared, and stirred, and the apple skin powder of step (a) is 100 parts of the sliced apple skin Drying at 5 ~ 10 ℃ temperature so that the moisture content is less than 3% while stirring 0.1 ~ 0.3 parts by weight of the cypress oil relative to the part, and then stored at 20 ~ 35 ℃ temperature for 30 to 45 days and then crushed to prepare a powder It can be achieved by a detergent composition containing a probiotic.

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Another object of the present invention, 0.1 to 5 parts by weight of probiotics per 100 parts by weight of fiber deodorant extract, the fiber deodorant extract, (a) 100 to 45 parts by weight of apple peel skin powder and grapefruit with respect to 100 parts by weight of purified water Mixing 0.5 ~ 1.5 parts by weight of the seed extract and then heated for 300 to 350 minutes at 180 ~ 250 ℃, then cooled to 30 ~ 50 ℃ and then further mixed 0.1 ~ 0.5 parts by weight of acid colostrum and filtered to prepare a filtrate Wow; (b) to 100 parts by weight of the filtrate, 1.5 to 3 parts by weight of citric acid and 0.05 to 0.1 parts by weight of the turpent extracts are mixed and prepared, and stirred, and the apple skin powder of step (a) is 100 parts of the sliced apple skin It is prepared as a powder by drying at 5 ~ 10 ℃ temperature so that the moisture content is less than 3% while stirring 0.1 ~ 0.3 parts by weight of the cypress oil, and then crushed after storing for 30 to 45 days at 20 ~ 35 ℃ temperature, Probiotics include Bacillus bacteria, Lactobacillus bacteria, Lactococcus bacteria, Enterococcus bacteria, Streptococcus bacteria and Bifidus bacteria, Bacillus bacteria are any one or more of Bacillus coagulans, Bacillus subtilis , The Lactobacillus bacteria Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgaricus, Lactobacillus helveticus, Lactobacillus fermentum, Lactobacillus paracasei, Lactobacillus plantarum, Lactoba one or more of cillus reuteri, Lactobacillus rhamnosus, Lactobacillus salivarius , the Lactococcus bacteria are Lactococcus lactis , the Enterococcus bacteria are any one or more of Enterococcus faecium , Enterococcus faecalis , and the Streptococcus bacteria are Streptococcus fiphilus , The fungi are Bifidobacterium bifidum, Bifidobacterium breve, Bifidobacterium longum, Bifidobacterium animalis ssp. It can be achieved by a fiber deodorant composition containing probiotics, characterized in that at least one of lactis .

Yet another object of the present invention includes 0.1 to 5 parts by weight of probiotics based on 100 parts by weight of the fabric softener extract, wherein the fabric softener extract is 12 to 15 parts by weight of goji berry, 30 to 35 parts by weight with respect to 100 parts by weight of blue plum. After mixing and sealing 100 parts to 150 parts by weight of sugar and fermentation at 30 to 45 days at 20 to 25 ℃ temperature, and then produced by filtration, the probiotics Bacillus, Lactobacillus, Lactococcus, Enterococcus, Streptococcus and bifidus, including the Bacillus is any one or more of Bacillus coagulans, Bacillus subtilis , the Lactobacillus bacteria Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgarusus, Lgargarusus Lactobacillus paracasei, Lactobacillus plantarum, Lactobacillus reuteri, Lactobacillus rhamnosus, Lactobacillus s any one or more of alivarius , the Lactococcus bacterium is Lactococcus lactis , the Enterococcus is at least one of Enterococcus faecium , Enterococcus faecalis , the Streptococcus bacterium is Streptococcus thermophilus , and the bifidus bacterium is Bifidobacterium bifidum, Bifidobacterium breve , Bifidobacterium longum, Bifidobacterium animalis ssp. It can be achieved by a fabric softener composition containing probiotics characterized in that at least one of lactis .

The present invention as described above has the effect of improving the washing power, remove the odor of the fiber and improve the flexibility of the fiber.

Hereinafter, with reference to the embodiment of the present invention will be described.

1. Selection of Probiotics

Probiotic, a functional food, is a living bacterium that enters the body and gives a healthy effect. Most lactic acid bacteria are included, but some include Bacillus. Russian scientist Elie Mechinikoff has been studying the functionalities of lactic acid bacteria and probiotics since the Nobel Prize, revealing that Bulgarians enjoy longevity because of the consumption of fermented milk fermented by Lactobacillus (Mercenier et al. 2003). To be recognized as probiotics, bacteria including lactic acid bacteria must survive in stomach and bile acids, reach the small intestine, proliferate and settle in the intestine, show useful effects in the intestine, be nontoxic and non-pathogenic.

Probiotics applied in this embodiment may be applied to Bacillus (Bacillus), Lactobacillus (Lactobacillus), Lactococcus, Enterococcus, Streptococcus (Streptococcus) and Bifidobacterium (Bifidobacterium). . Here, Bacillus bacteria Bacillus coagulans, Bacillus subtilis two species, Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgaricus, Lactobacillus helveticus, Lactobaactobacillus fermentum paracasei Lactobacillus 11 species of salivarius , 1 species of Lactococcus lactis, 1 species of Enterococcus faecium, 2 types of Enterococcus faecalis , 1 type of Streptococcus thermophilus , 2 types of Streptococcus thermophilus, 2 types of Bifidobacterium bifidum, Bifidobacterium breve, Bifidobacisium sp . 4 species of lactis .

Bacillus cereus in the Bacillus family is a by-product bacterium distributed in the natural world, and its biological characteristics are similar to anthrax, but it has a flagella, and the non-capsular formation is different from anthrax. Some strains cause bacterial food poisoning, which is diarrhea or vomiting. Here, the diarrhea type is manifested after 8 to 16 hours of incubation period, with abdominal pain and watery diarrhea as the main symptom, and the incubation period of vomiting type is 8 to 16 hours, with the main symptoms being vomiting and vomiting.

Diarrhea is regarded as a pathogen for diarrhea growth toxin produced in the intestine, and vomiting is regarded as a pathogen for vomiting poison produced in food, and food poisoning caused by Cereus bacteria is about 10 to 20 cases per year. In addition, cereus is an opportunistic pathogen, which may be caused by bronchitis, meningitis, sepsis, or ophthalmitis.

Therefore, the present embodiment does not use Bacillus cereus which causes the above problem.

Detergent composition preparation

To prepare Comparative Example 1 and Example 1 having the composition of Table 1.

Here, Comparative Example 1 is a conventional detergent, Example 1 is a probiotic was added to Comparative Example 1 and all the units are 'parts by weight' with respect to 100 parts by weight of purified water.

In addition, the composition of Comparative Example 1 is a conventional detergent as described above, the component or content may be modified according to the purpose of use.

Detergency rating

Detergency test was tested according to the KSM 2715 test method and the results are shown in Table 2. Here, the results of Table 2 is a relative calculation of the cleaning power (%) of the examples when the cleaning power (%) of Comparative Example 1 is 100.

Referring to Table 2, it was confirmed that the Examples have improved cleaning power by about 3 to 12% compared to Comparative Example 1. In addition, when the probiotics exceed 15 parts by weight, the washing power does not improve by more than 5% compared to Comparative Example 1.

Deodorant Composition Preparation

The deodorant composition containing the probiotics of this embodiment contains 0.1 to 5 parts by weight of probiotics with respect to 100 parts by weight of the fiber deodorant extract.

Here, since the probiotics of the present embodiment are the same as those of the first to fifth embodiments, detailed description thereof will be omitted.

2. Fiber Deodorant Extract

The fiber deodorant extract of this embodiment is prepared through the following extraction process.

(a) 30 to 45 parts by weight of apple rind powder and 0.5 to 1.5 parts by weight of grapefruit seed extract are mixed with respect to 100 parts by weight of purified water, and then heated at 180 to 250 ° C. for 300 to 350 minutes.

Apple peel skin powder of the present embodiment is to use the malic acid (malic acid) of the flavor component of the various organic acids contained through the following manufacturing process.

The apple rind powder is dried at a temperature of 5 to 10 ° C. so that the moisture content is less than 3% while stirring 0.1 to 0.3 parts by weight of cypress oil to 100 parts by weight of the sliced apple rind, and then 30 to 45 days at 20 to 35 ° C. After storage, it is crushed to make powder, and then kept closed. The reason why a small amount of cypress oil is added is to prevent the occurrence of odor generated during drying of the apple peel and to add a refreshing feeling peculiar to the cypress oil. In addition, the reason for the low temperature drying at 5 ~ 10 ℃ is to minimize the loss of malic acid generated during freeze drying or high temperature drying, as well as to prevent corruption. And the reason for storing for 30 to 45 days at 20 ~ 35 ℃ temperature is to concentrate the active ingredient containing malic acid.

(b) Then, the mixture is cooled to 30 to 50 ° C., and then mixed with 100 parts by weight of purified water and 0.1 to 0.5 parts by weight of acetic acid, followed by filtration to prepare a filtrate.

(c) 1.5 to 3 parts by weight of citric acid and 0.05 to 0.1 parts by weight of vortex extract are mixed with 100 parts by weight of the filtrate, followed by stirring.

Here, citric acid and turpentine extract are used as anti-scattering agents, in particular, the turmeric extract is prepared by the hydrothermal extraction method, and the turmeric is a perennial fresh grass that belongs to the rock brush (Orostachys) and grows on the roof tile.

Deodorization test for clothing and textile

In Comparative Examples 2 and 3 and Examples 5 to 10, the deodorizing effects of ammonia, trimethylamine, and hydrogen sulfide, which are representative odor sources of daily life, were evaluated by a detection tube method, and the results are shown in Table 3. Here, in the deodorizing test method, after spraying 3g of the comparative examples and examples to the cotton cloth, the cotton cloth was put in a Erlenmeyer flask and sealed, and after standing for 30 minutes, the gas concentration was measured using a detection tube for 120 minutes in a unit of 30 minutes. Test 10 times or more, the average value is listed in Table 3, the unit of the deodorizing effect is%.

Comparative Example 2 is distilled water, and Comparative Example 3 contains 97% by weight of distilled water and 3% by weight of cypress oil. In addition, the composition of Examples 6-10 is as follows.

Example 6: 100 parts by weight of the fiber deodorant extract

Example 7: 0.1 to 0.3 parts by weight of probiotics per 100 parts by weight of fiber deodorant extract

Example 8: 0.4 to 1.0 parts by weight of probiotics per 100 parts by weight of fiber deodorant extract

Example 9: 1.1 to 3.0 parts by weight of probiotics, based on 100 parts by weight of fiber deodorant extract

Example 10: 3.1 to 5.0 parts by weight of probiotics, based on 100 parts by weight of fiber deodorant extract

Referring to Table 3, Examples 6 to 10 were found to have a deodorizing effect of more than 96% of ammonia, trimethylamine and hydrogen sulfide within 120 minutes, in particular, the higher the content of probiotics was confirmed to have a good deodorizing effect.

Softener Composition Preparation

The softener composition containing the probiotics of this embodiment contains 0.1 to 5 parts by weight of probiotics based on 100 parts by weight of the fabric softener extract.

Here, since the probiotics of the present embodiment are the same as those of the first to fifth embodiments, detailed description thereof will be omitted.

3. Fabric Softener Extract

The fabric softener extract of this embodiment is prepared through the following extraction process.

The fabric softener extract of the present embodiment was sealed by mixing 12-15 parts by weight of goji berry, 30-35 parts by weight and 100-150 parts by weight of sugar with respect to 100 parts by weight of fresh plum, and then at a temperature of 20-25 ° C. It is produced by fermentation for 30 to 45 days and then filtration.

Here, the clean room, wolfberry and goblet are washed at least three times, and then dried and then used in small pieces. In addition, fresh plums are the main component of the fabric softener and goji berry and straw are provided to prevent the decay bacteria to achieve the desired fermentation.

Flexible effect test for clothing and textile

After washing commercially available 100% cotton towels in a domestic drum washing machine, adding the Comparative Examples 4 and 11 to 15 in the rinsing process, dehydrating them, preparing a natural dry towel for 10 to 14 hours, and preparing the prepared towels. After 20 sensory evaluations by the investigator (20 women with no chronic disease in their 20s to 40s), the results are shown in Table 4. Here, the results are average values and the softening effect is evaluated in units of 0.5 points from 0 to 5 points, but the higher the score, the better the softening effect.

Comparative Example 4 is distilled water, the composition of Examples 11 to 15 is as follows.

Example 11: 100 parts by weight of fabric softener extract

Example 12 0.1 to 0.3 parts by weight of probiotics per 100 parts by weight of fabric softener extract

Example 13: 0.4 to 1.0 parts by weight of probiotics per 100 parts by weight of fabric softener extract

Example 14 1.1 to 3.0 parts by weight of probiotics, based on 100 parts by weight of fabric softener extract

Example 15 3.1 to 5.0 parts by weight of probiotics, based on 100 parts by weight of fabric softener extract

Referring to Table 4, the Examples obtained a high flexibility score of 3.5 or more, in particular, the higher the content of probiotics, it was confirmed that the softness score is significantly higher.

The present invention as described above has been described with reference to one embodiment, but not limited to this embodiment is obvious that all modifications based on the technical spirit of the present invention belong to the scope of the present invention.

Claims (5)

Probiotics 0.1 to 15 parts by weight based on 100 parts by weight of the detergent composition,
The probiotics include Bacillus bacteria, Lactobacillus bacteria, Lactococcus bacteria, Enterococcus bacteria, Streptococcus bacteria and Bifidus bacteria,
The Bacillus bacteria is at least one of Bacillus coagulans, Bacillus subtilis ,
The Lactobacillus bacteria Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgaricus, Lactobacillus helveticus, Lactobacillus fermentum, Lactobacillus paracasei, Lactobacillus plantarum, Lactobacillus reuteri, Lactobacillus reuteri
The lactococcus bacteria is Lactococcus lactis ,
The enterococcus bacteria is at least one of Enterococcus faecium , Enterococcus faecalis ,
Streptococcus bacteria is Streptococcus thermophilus ,
The bifidus bacteria are Bifidobacterium bifidum, Bifidobacterium breve, Bifidobacterium longum, Bifidobacterium animalis ssp. at least one of lactis ,
Further comprising 10 to 150 parts by weight of the fiber deodorant extract based on 100 parts by weight of the probiotics,
The fiber deodorant extract is mixed with (a) 100 parts by weight of purified water, 30 to 45 parts by weight of apple rind powder and 0.5 to 1.5 parts by weight of grapefruit seed extract, and then heated at 180 to 250 ° C. for 300 to 350 minutes, and then 30 Cooling to ˜50 ° C. and further mixing 0.1 to 0.5 parts by weight of acetic acid and then filtering to prepare a filtrate; (b) to 100 parts by weight of the filtrate, 1.5 to 3 parts by weight of citric acid and 0.05 to 0.1 parts by weight of the turpent extracts are mixed and prepared by stirring, the apple skin powder of step (a) is 100 parts by weight of the sliced apple skin Drying at 5 ~ 10 ℃ temperature so that the moisture content is less than 3% while stirring 0.1 ~ 0.3 parts by weight of the cypress oil for the part, and then stored at 20 ~ 35 ℃ temperature for 30 to 45 days and then crushed to prepare a powder A detergent composition containing probiotics.
delete delete Probiotics 0.1 to 5 parts by weight based on 100 parts by weight of the fiber deodorant extract,
The fiber deodorant extract,
(a) 30 to 45 parts by weight of apple rind powder and 0.5 to 1.5 parts by weight of grapefruit seed extract are mixed with 100 parts by weight of purified water, and then heated at 180 to 250 ° C. for 300 to 350 minutes, and then cooled to 30 to 50 ° C. Next, 0.1 to 0.5 parts by weight of acidic oil is further mixed and filtered to prepare a filtrate; (b) to 100 parts by weight of the filtrate, 1.5 to 3 parts by weight of citric acid and 0.05 to 0.1 parts by weight of the turpent extracts are mixed and prepared, and stirred, and the apple skin powder of step (a) is 100 parts of the sliced apple skin It is prepared as a powder by drying at 5 ~ 10 ℃ temperature so that the moisture content is less than 3% while stirring 0.1 ~ 0.3 parts by weight of the cypress oil for about 30 to 45 days after crushing,
The probiotics include Bacillus, Lactobacillus, Lactococcus, Enterococcus, Streptococcus and Bifidus,
The Bacillus bacteria is at least one of Bacillus coagulans, Bacillus subtilis ,
The Lactobacillus bacteria Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgaricus, Lactobacillus helveticus, Lactobacillus fermentum, Lactobacillus paracasei, Lactobacillus plantarum, Lactobacillus reuteri, Lactobacillus reuteri
The lactococcus bacteria is Lactococcus lactis ,
The enterococcus bacteria is at least one of Enterococcus faecium , Enterococcus faecalis ,
Streptococcus bacteria is Streptococcus thermophilus ,
The bifidus bacteria are Bifidobacterium bifidum, Bifidobacterium breve, Bifidobacterium longum, Bifidobacterium animalis ssp. Fiber deodorant composition containing probiotics, characterized in that any one or more of lactis .
It contains 0.1 to 5 parts by weight of probiotics per 100 parts by weight of fabric softener extract,
The fabric softener extract,
It is prepared by fermentation at 20-25 ° C. for 30 to 45 days after sealing by mixing 12-15 parts by weight of wolfberry, 30-35 parts by weight of straw, and 100-150 parts by weight of sugar, and sealing the mixture. ,
The probiotics include Bacillus, Lactobacillus, Lactococcus, Enterococcus, Streptococcus and Bifidus,
The Bacillus bacteria is at least one of Bacillus coagulans, Bacillus subtilis ,
The Lactobacillus bacteria Lactobacillus acidophilus, Lactobacillus casei, Lactobacillus gasseri, Lactobacillus delbrueckii ssp bulgaricus, Lactobacillus helveticus, Lactobacillus fermentum, Lactobacillus paracasei, Lactobacillus plantarum, Lactobacillus reuteri, Lactobacillus reuteri
The lactococcus bacteria is Lactococcus lactis ,
The enterococcus bacteria is at least one of Enterococcus faecium , Enterococcus faecalis ,
Streptococcus bacteria is Streptococcus thermophilus ,
The bifidus bacteria are Bifidobacterium bifidum, Bifidobacterium breve, Bifidobacterium longum, Bifidobacterium animalis ssp. Fiber softener composition containing probiotics, characterized in that any one or more of lactis .