KR102070153B1 - Beverage Composition comprising Normal Temperature Soluble and Non coagulable Agar-Agar - Google Patents
Beverage Composition comprising Normal Temperature Soluble and Non coagulable Agar-Agar Download PDFInfo
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- KR102070153B1 KR102070153B1 KR1020170176278A KR20170176278A KR102070153B1 KR 102070153 B1 KR102070153 B1 KR 102070153B1 KR 1020170176278 A KR1020170176278 A KR 1020170176278A KR 20170176278 A KR20170176278 A KR 20170176278A KR 102070153 B1 KR102070153 B1 KR 102070153B1
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- 229920001817 Agar Polymers 0.000 title claims abstract description 76
- 239000000203 mixture Substances 0.000 title claims abstract description 19
- 235000013361 beverage Nutrition 0.000 title claims abstract description 18
- 235000010419 agar Nutrition 0.000 title description 64
- 241000206672 Gelidium Species 0.000 title 1
- 239000008272 agar Substances 0.000 claims abstract description 74
- 238000000034 method Methods 0.000 claims abstract description 23
- 239000000843 powder Substances 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 21
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000008213 purified water Substances 0.000 claims abstract description 14
- 238000010306 acid treatment Methods 0.000 claims abstract description 11
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000005979 Citrus limon Nutrition 0.000 claims abstract description 8
- 244000131522 Citrus pyriformis Species 0.000 claims abstract description 8
- 239000002253 acid Substances 0.000 claims abstract description 8
- 239000004376 Sucralose Substances 0.000 claims abstract description 7
- 235000019408 sucralose Nutrition 0.000 claims abstract description 7
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims abstract description 7
- 239000004386 Erythritol Substances 0.000 claims abstract description 6
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000019414 erythritol Nutrition 0.000 claims abstract description 6
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims abstract description 6
- 229940009714 erythritol Drugs 0.000 claims abstract description 6
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 6
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 5
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 5
- 239000011718 vitamin C Substances 0.000 claims abstract description 5
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical class O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 claims abstract description 4
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 3
- 238000005406 washing Methods 0.000 claims abstract description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 4
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 4
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims 1
- 238000005345 coagulation Methods 0.000 abstract description 17
- 230000015271 coagulation Effects 0.000 abstract description 16
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 238000001035 drying Methods 0.000 abstract description 5
- 239000004267 EU approved acidity regulator Substances 0.000 abstract description 3
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 description 6
- 235000019634 flavors Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 4
- 238000010411 cooking Methods 0.000 description 3
- 235000005911 diet Nutrition 0.000 description 3
- 230000037213 diet Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 229920001282 polysaccharide Polymers 0.000 description 3
- 239000005017 polysaccharide Substances 0.000 description 3
- 150000004804 polysaccharides Chemical class 0.000 description 3
- 244000020518 Carthamus tinctorius Species 0.000 description 2
- 235000003255 Carthamus tinctorius Nutrition 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 244000155437 Raphanus sativus var. niger Species 0.000 description 2
- 235000013325 dietary fiber Nutrition 0.000 description 2
- 235000003599 food sweetener Nutrition 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 239000003765 sweetening agent Substances 0.000 description 2
- 239000001052 yellow pigment Substances 0.000 description 2
- WQNHWIYLCRZRLR-UHFFFAOYSA-N 2-(3-hydroxy-2,5-dioxooxolan-3-yl)acetic acid Chemical compound OC(=O)CC1(O)CC(=O)OC1=O WQNHWIYLCRZRLR-UHFFFAOYSA-N 0.000 description 1
- 229920000936 Agarose Polymers 0.000 description 1
- 244000247812 Amorphophallus rivieri Species 0.000 description 1
- 235000001206 Amorphophallus rivieri Nutrition 0.000 description 1
- 241000258957 Asteroidea Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 208000006558 Dental Calculus Diseases 0.000 description 1
- 229920002752 Konjac Polymers 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 240000003273 Passiflora laurifolia Species 0.000 description 1
- 235000013762 Passiflora laurifolia Nutrition 0.000 description 1
- 238000012356 Product development Methods 0.000 description 1
- 235000005733 Raphanus sativus var niger Nutrition 0.000 description 1
- 244000228451 Stevia rebaudiana Species 0.000 description 1
- 229920001284 acidic polysaccharide Polymers 0.000 description 1
- 150000004805 acidic polysaccharides Chemical class 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000000701 coagulant Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 235000013365 dairy product Nutrition 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000015094 jam Nutrition 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 239000000252 konjac Substances 0.000 description 1
- 235000010485 konjac Nutrition 0.000 description 1
- 235000020845 low-calorie diet Nutrition 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 235000013615 non-nutritive sweetener Nutrition 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 235000011962 puddings Nutrition 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- KINGXFAMZNIVNL-SXQDSXCISA-N safflor yellow A Natural products OC[C@@H]1O[C@H]2[C@H](OC3=C2C(=O)C(=C(O)C=Cc4ccc(O)cc4)C(=O)[C@]3(O)[C@@H]5O[C@H](CO)[C@@H](O)[C@H](O)[C@H]5O)[C@@H](O)[C@H]1O KINGXFAMZNIVNL-SXQDSXCISA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000019614 sour taste Nutrition 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000036642 wellbeing Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/256—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from seaweeds, e.g. alginates, agar or carrageenan
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0036—Galactans; Derivatives thereof
- C08B37/0039—Agar; Agarose, i.e. D-galactose, 3,6-anhydro-D-galactose, methylated, sulfated, e.g. from the red algae Gelidium and Gracilaria; Agaropectin; Derivatives thereof, e.g. Sepharose, i.e. crosslinked agarose
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Materials Engineering (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Organic Chemistry (AREA)
- Sustainable Development (AREA)
- Dispersion Chemistry (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
본 발명은, 한천을 포함하는 음료조성물에 관한 것으로, 원료를 수세하고 이물을 제거한 후 수세한 원료의 15 ~ 25배의 정제수를 원료에 투입하는 (1)과정과; 1차 산처리 하는 (2)과정과; 여과하고 중화하여 건조, 분쇄하는 (3)과정;를 포함포함하고, 상기 (2) 산처리과정에서 산은 염산을 포함하되, 산의 양은 상기 원료의 수용액 100wt%에 대하여 4wt% ~ 8wt% 범위이며, 처리 시간은 8시간 ~16시간 사이이고, 처리 온도는 60~70℃ 범위에서 제조된 한천을 상온(15~25℃ 범위)의 정제수 100wt%에 대하여 1 ~ 3wt% 범위로, 상기 정제수 100wt%에 대하여 레몬과즙 분말 0.04wt% ~ 0.10wt% 범위로, 에리스리톨(Erythlitol)을 4.90wt% ~ 5.90wt% 범위로, 수크랄로스(Sucralose) 및 효소처리스테비아(Enzymatically Modified Stevia) 중 어느 하나 이상을 0.01wt ~ 0.05wt 범위로, 비타민C, 구연산으로 구성된 산도조절제군으로부터 선택된 하나 이상을 0.01wt ~ 0.10wt 범위로 더 포함하여 상기 한천은 용해되면서(용해도 78.0 ± 4.0wt% 범위) 응고되지 않는 것을 특징으로 한다.
이에, 본 발명에 따르면, 한천이 상온에도 용해가 잘 될 수 있어 다양하게 한천을 응용한 제품에 적용할 수 있으며 고농도로 첨가하여도 응고가 되지 않으므로 한천에 대한 거부감을 없앨 수 있고 한천 특유의 기능성을 그대로 가질 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공할 수 있다.The present invention relates to a beverage composition comprising agar, the process of (1) the process of injecting 15-25 times purified water of the washed raw material to the raw material after washing the raw material and removing the foreign matter; (2) process of primary acid treatment; (3) the process of filtering, neutralizing, drying and pulverizing; and (2) the acid in the acid treatment process includes hydrochloric acid, the amount of acid ranges from 4wt% to 8wt% with respect to 100wt% of the aqueous solution of the raw material. , The treatment time is between 8 hours and 16 hours, and the treatment temperature is in the range of 1 to 3 wt% with respect to 100 wt% of purified water at room temperature (15 to 25 ℃) of agar prepared in the range of 60 to 70 ℃, the purified water 100 wt% Lemon juice powder in the range of 0.04wt% to 0.10wt%, erythritol in the range of 4.90wt% to 5.90wt%, at least one of sucralose and Enzymatically Modified Stevia ˜0.05 wt%, further comprising one or more selected from the group of acidity regulators consisting of vitamin C and citric acid in the range of 0.01 wt% to 0.10 wt%, wherein the agar is dissolved (solubility range 78.0 ± 4.0 wt%). do.
Therefore, according to the present invention, the agar can be easily dissolved even at room temperature, it can be applied to a variety of products applied agar and can not be coagulated even when added to a high concentration, eliminating the rejection of agar, and agar unique functionality It can provide a method for producing agar having a room temperature solubility and non-coagulation that can have the same and a beverage composition using the same.
Description
본 발명은 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물에 관한 것으로. 특히 상온에 용해될 수 있으며 응고가 되지 않는 구조를 갖는 한천과 이를 이용한 음료조성물을 제조할 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물에 관한 것이다.The present invention relates to a method for preparing agar having room temperature solubility and non-coagulation and a beverage composition using the same. In particular, the present invention relates to a method for preparing agar having a solubility and non-coagulation property and a beverage composition using the same, which can be dissolved at room temperature and have a structure that does not solidify, and a beverage composition using the same.
조리, 요리, 음료, 건강식품 등의 먹거리에는 다양한 종류의 재료들이 사용되고 있으며 그 중에 한천이 사용되기도 한다.Various types of ingredients are used for cooking, cooking, drinks, and health foods, and agar may be used.
한천은 원소재인 우뭇가사리를 채취 후 자숙 및 여과, 건조시켜 제조하는 것이 일반적이다. 한천은 식이섬유 및 미네랄이 풍부하여 고식이섬유, 저당, 저지방이라는 특징을 가져 최근 웰빙, 다이어트 등과 관련된 가공 식품에 많이 사용되고 있으며 이러한 용도로 개발 내지 활용되고 있다. 다른 한편, 한천은 우무요리 및, 양갱, 잼, 푸딩, 젤리 등의 제과용으로 많이 사용되고, 유제품 및 미생물용 배지 등에도 사용되고 있다.Agar is generally manufactured by collecting raw starfish, ripened, filtered and dried. Agar is rich in dietary fiber and minerals, and has been characterized by high dietary fiber, low sugar, low fat, and has been widely used in processed foods related to well-being and diet. On the other hand, agar is widely used for daikon cooking, confectionery such as yokan, jam, pudding, and jelly, and is also used for medium for dairy products and microorganisms.
이러한 한천의 제조방법은 두 가지로 분류된다. 원래 한천이라고 하면 자연적으로 만드는 자연한천(自然寒天)을 지칭했으나 요즘은 기계적으로 제조하는 공업한천(工業寒天)도 있다. 자연한천은 원조를 고아서 만든 우무를 묵통(응고상자)에 넣어 응고시킨 뒤 이를 잘라 추운 겨울 옥외에서 야간에는 -5∼-10℃의 한기로 동결시키고, 주간에는 5∼10℃의 저온에서 건조시키는 일을 일정 기간 예를 들면, 약 보름간 반복적으로 건조하여 제조한다. 이렇게 제조되는 자연한천은 야외에서 건조되기 때문에 건조과정에서 불순물이 혼입될 수 있고, 야외의 기온이 영하로 내려가는 겨울철에만 생산할 수 있다는 단점이 있다. There are two methods for producing such agar. Originally, agar refers to a natural agar made by nature, but nowadays there is also an industrial agar made mechanically. Natural agar is solidified by putting the original daikon radish into a jegtong (coagulation box), then cutting it and freezing it at -5 ~ -10 ℃ at night in cold winter outdoor, and drying it at low temperature of 5 ~ 10 ℃ during the day. The work is prepared by repeated drying for a period of time, for example about full. Since the natural agar produced in this way is dried in the open air, impurities may be mixed in the drying process, and the natural agar may be produced only in winter when the outdoor temperature drops to below zero.
이러한 단점을 보완하기 위하여 개발된 것이 공업한천으로, 자연적인 조건하에서 이루어지는 탈수공정을 기계화로 대체하였다.The industrial agar was developed to compensate for these shortcomings, replacing the dehydration process under natural conditions with mechanization.
그리고, 최근 비만이 질환으로 간주될 정도로 사회적인 문제로 등장하고 있고, 이와 더불어 다이어트에 대한 관심이 상당히 증가하고 있는 추세로 이를 개선하기 위한 많은 연구 및 제품개발이 진행되고 있다. 한천 특유의 성질인 저칼로리, 기능성으로 인하여 한천을 이용한 저칼로리 다이어트 식품과 관련된 개발이 이루어지고 있다.Recently, obesity is a social problem that can be regarded as a disease, and the interest in the diet is increasing significantly, and a lot of research and product development has been conducted to improve this. Due to the low calorie and functional properties of agar, developments related to low calorie diet food using agar are being made.
한천은 단백질 2wt%, 회분 3.5wt%, 지방 0.5wt% 이하로서 대부분은 다당류이다. 다당류는 중성다당류인 아가로오스(agarose) 70wt%와 산성다당류인 아가로펙틴(agaropectin) 30wt%로 구성된다. 한천 용액은 응고력이 세고, 응고한 것은 비교적 용융점이 높고 잘 부패하지 않으며, 또 물과의 친화성이 강하여 수분을 일정한 형태로 유지하는 능력이 크기 때문에 젤리·잼 등의 과자와 아이스크림, 양조시의 찌꺼기 앉힘 등의 식품가공에 많이 이용되고 있으며, 세균의 작용으로 잘 분해되지 않고 응고력이 강하기 때문에 세균배양용으로도 쓰인다. 또한, 곤약과 비슷하게, 다이어트 식품 용도로 많이 사용된다. 우뭇가사리로 만든 묵은, 소화가 어려운 탄수화물, 섬유질을 많이 포함하고 있으며, 대부분의 성분은 물이 차지하고 있다. 특별한 맛이 없다는 것에서, 저열량 요리를 만드는 각종 요리에 사용될 수 있다. 하지만 한천의 90℃라는 높은 용융점으로 인해 활용도가 다양하지 않고 응고가 되는 특성으로 인해 제품에 고용량의 한천을 사용하기가 어렵다는 단점이 있다.Agar is 2 wt% protein, 3.5 wt% ash, 0.5 wt% fat or less, most of which are polysaccharides. The polysaccharide is composed of 70 wt% of agarose, a neutral polysaccharide, and 30 wt% of agaropectin, an acidic polysaccharide. The agar solution has a high coagulation power, and the coagulated water has a relatively high melting point, does not rot well, and has a high affinity with water, and has a high ability to maintain water in a constant form. It is widely used in food processing, such as sit-ups, and is used for bacterial cultivation because it is hardly decomposed by the action of bacteria and its coagulation power is strong. Also, similar to konjac, it is widely used for diet food. Old, hard to digest carbohydrates and fiber made from wood, most of the water is occupied. In that it has no special taste, it can be used in various dishes to make low calorie dishes. However, due to the high melting point of the agar 90 ℃ because of the characteristics of the application and the solidification is difficult to use a high capacity agar in the product.
따라서, 한천이 다양한 용도를 위하여 농도가 높더라도 응고가 되지 않으면서 상온에 잘 용해될 수 있는 것이 바람직하다.Therefore, it is desirable that the agar can be dissolved well at room temperature without coagulation even if the concentration is high for various uses.
[참고 문헌][references]
특허공보 특1997-0009899호 (1997.06.19. 공고)Patent Publication No. 1997-0009899 (June 19, 1997)
본 발명의 목적은, 한천이 상온에도 용해가 잘 될 수 있어 다양하게 한천을 응용한 제품에 적용할 수 있으며 제조하는 과정에서 각 원료의 향미나 성분을 그대로 유지할 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공하는 것이다.The object of the present invention is that the agar can be easily dissolved even at room temperature so that it can be applied to a variety of products applied agar and the room temperature solubility and non-coagulation property that can maintain the flavor component of each raw material in the process of manufacturing It is to provide a method of manufacturing agar having and a beverage composition using the same.
또한, 본 발명의 다른 목적은, 고농도로 첨가하여도 응고가 되지 않으므로 한천에 대한 거부감을 없앨 수 있고 한천 특유의 기능성을 그대로 가질 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공하는 것이다.In addition, another object of the present invention, because it does not coagulate even when added to a high concentration can eliminate the rejection to agar and have a room temperature solubility and non-coagulability that can have the characteristics of agar as it is, and using the same It is to provide a beverage composition.
본 발명의 목적은, 한천을 포함하는 음료조성물에 있어서, 원료를 수세하고 이물을 제거한 후 수세한 원료의 15 ~ 25배의 정제수를 원료에 투입하는 (1)과정과; 1차 산처리 하는 (2)과정과; 여과하여 여과액을 중화하여 건조, 분쇄하는 (3)과정;를 포함하고, 상기 (2) 산처리과정에서 산은 염산을 포함하되, 산의 양은 상기 원료의 수용액 100wt%에 대하여 4wt% ~ 8wt% 범위이며, 처리 시간은 8시간 ~16시간 사이이고, 처리 온도는 60~70℃ 범위에서 제조된 한천을 상온(15~25℃ 범위)의 정제수 100wt%에 대하여 1 ~ 3wt% 범위로, 상기 정제수 100wt%에 대하여 레몬과즙 분말 0.04wt% ~ 0.10wt% 범위로, 에리스리톨(Erythlitol)을 4.90wt% ~ 5.90wt% 범위로, 수크랄로스(Sucralose) 및 효소처리스테비아(Enzymatically Modified Stevia) 중 어느 하나 이상을 0.01wt ~ 0.05wt 범위로, 비타민C, 구연산으로 구성된 산도조절제군으로부터 선택된 하나 이상을 0.01wt ~ 0.10wt 범위로 더 포함하여 상기 한천은 용해되면서(용해도 78.0 ± 4.0wt% 범위) 응고되지 않는 것을 특징으로 하는 음료조성물에 의하여 달성된다.An object of the present invention, in the beverage composition comprising agar, (1) the process of injecting purified water 15 to 25 times of the washed raw material to the raw material after washing the raw material and removing the foreign matter; (2) process of primary acid treatment; (3) the process of neutralizing the filtrate by filtration to dry and pulverize; wherein (2) the acid in the acid treatment process contains hydrochloric acid, the amount of acid is 4wt% ~ 8wt% with respect to 100wt% of the aqueous solution of the raw material The treatment time is between 8 hours and 16 hours, and the treatment temperature is in the range of 1 to 3 wt% based on 100 wt% of purified agar at room temperature (15 to 25 ℃) of agar prepared in the range of 60 to 70 ℃, the purified water Lemon juice powder in the range of 0.04wt% to 0.10wt% with respect to 100wt%, erythritol 4.90wt% to 5.90wt%, at least one of sucralose and Enzymatically Modified Stevia In the range of 0.01 wt to 0.05 wt, the at least one selected from the group of acidity regulators consisting of vitamin C and citric acid is further included in the range of 0.01 wt to 0.10 wt, and the agar is not dissolved (solubility in the range of 78.0 ± 4.0 wt%). Achieve by drink composition characterized The.
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또한, 상기 (3)과정의 중화처리시에 사용되는 알칼리는 가성소다를 포함하고, 0.1wt% ~ 10wt% 범위를 포함하는 것이 바람직하다.In addition, the alkali used in the neutralization treatment of step (3) includes caustic soda, and preferably contains 0.1 wt% to 10 wt%.
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본 발명에 따르면, 한천이 상온에도 용해가 잘 될 수 있어 다양하게 한천을 응용한 제품에 적용할 수 있으며 제조하는 과정에서 각 원료의 향미나 성분을 그대로 유지할 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공할 수 있다.According to the present invention, the agar can be well dissolved at room temperature, so that it can be applied to a variety of products to which agar is applied, and has room temperature solubility and non-coagulation property which can maintain the flavor component of each raw material as it is produced. It is possible to provide a method for preparing agar and a beverage composition using the same.
또한, 고농도로 첨가하여도 응고가 되지 않으므로 한천에 대한 거부감을 없앨 수 있고 한천 특유의 기능성을 그대로 가질 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공할 수 있다.In addition, it is possible to provide a method for producing agar having a room temperature solubility and non-coagulation, which can eliminate the objection to agar because it does not solidify even when added to a high concentration, and can have a functional characteristic peculiar to agar. .
본 발명의 일실시예에 따른 상온 용해성과 무응고성을 갖는 한천 및 이를 이용한 음료조성물의 제조 방법을 이하에서 구체적으로 설명하면 다음과 같다.Agar having a room temperature solubility and non-coagulation property and a method of preparing a beverage composition using the same according to an embodiment of the present invention will be described in detail below.
먼저, 분말 한천의 원료를 수세하고 난 다음 수세된 원료에 중량 대비 15 ~ 25배의 정제수를 넣는다. 바람직하게는 15 ~ 25배이며 너무 적게 넣으면 교반과 여과가 힘들어진다. First, the raw material of the powder agar is washed with water, and then 15-25 times the weight of purified water is added to the washed raw material. Preferably it is 15 to 25 times and adding too little makes stirring and filtration difficult.
다음, 원료와 정제수가 교반된 후에 산처리를 한다. 이러한 산처리시 사용되는 산은 염산이고, 산처리시 산의 양은 원료의 4wt% ~ 8wt% 범위로 첨가하는 것이 바람직하다. 처리 온도는 60 ~ 70℃ 범위로 설정하고 처리 시간은 8시간 ~ 16시간이 바람직하다.Next, the acid treatment is performed after the raw material and the purified water are stirred. The acid used in the acid treatment is hydrochloric acid, and the amount of acid in the acid treatment is preferably added in the range of 4 wt% to 8 wt% of the raw material. The treatment temperature is set in the range of 60 to 70 ° C., and the treatment time is preferably 8 hours to 16 hours.
이러한 산처리 후 여과하고 여과액을 가성소다 자체 농도로 0.1 ~ 10wt% 범위로 알칼리 처리하여 pH를 6~7로 중화시킨다. 중화과정을 끝낸 원료를 동결 건조, 분쇄 과정을 거쳐서 분말한천을 만들다.After this acid treatment, the filtrate was neutralized with an aqueous solution of caustic soda in an alkaline concentration of 0.1 to 10 wt% to neutralize the pH to 6 to 7. Freeze-drying and grinding of raw materials after neutralization to make powdered agar.
이렇게 제조된 분말한천은 상온에도 용해되고 농도가 고농도가 되더라도 응고되지 않는 무응고성임을 알 수 있었다.The powder agar thus prepared was found to be non-coagulant which is dissolved even at room temperature and does not coagulate even when the concentration is high.
또한, 이러한 상온 용해성과 무응고성을 갖는 분말한천을 포함하는 음료 조성물은, 정제수 중량 100wt%에 대하여 상온 용해성과 무응고성을 가지는 분말 한천 1.00 ~ 3.00wt%범위로, 레몬과즙 분말 0.04wt% ~ 0.10wt%범위로, 에리스리톨(Erythlitol)을 4.90wt% ~ 5.90wt%범위로, 수크랄로스(Sucralose) 및 효소처리스테비아(Enzymatically Modified Stevia) 중에서 선택된 하나 이상을 0.01wt% ~ 0.05wt%범위로, 비타민C, 구연산을 포함하는 산도조절제군으로부터 선택되는 하나 이상을 0.01wt% ~ 0.10wt범위로 혼합하여 제조되는 것이 바람직하다.In addition, the beverage composition comprising a powder agar having such room temperature solubility and non-coagulation, the powder agar having a room temperature solubility and non-coagulation 1.00 ~ 3.00wt% with respect to 100wt% of purified water, lemon juice powder 0.04wt% ~ 0.10wt%, erythritol (Erythlitol) 4.90wt% ~ 5.90wt%, at least one selected from sucralose (Sucralose) and Enzymatically Modified Stevia (0.01wt ~ 0.05wt%), It is preferably prepared by mixing at least one selected from the group of acidity regulators including vitamin C and citric acid in the range of 0.01wt% to 0.10wt.
여기서, 레몬과즙 분말은 분말 형태로 물에 타 먹을 수 있게 가공하였고, 에리스리톨은 감미도가 설탕의 70 ~ 80% 정도이며 청량한 감미를 가지고 있는 감미료로 체내에 거의 흡수되지 않고 배출되므로 저칼로리 감미료로 사용되며, 수크랄로스는 설탕에 비해 600배의 단맛을 가진 무열량 감미료이고, 효소처리스테비아스테비아는 효소처리한 것으로 칼로리가 없지만 감미도가 설탕의 약 100~200배로 비타민 항산화물질로 사용되고 최근에는 체중 감량 효과가 있다고 발표되고있으며, 구연산은 신맛을 내며 산미료로 사용된다.Here, the lemon juice powder is processed to be eaten in water in the form of powder, and erythritol is a low-calorie sweetener because it has a sweetness of about 70 to 80% of sugar and is a sweetener with a refreshing sweetness and is hardly absorbed by the body. Sucralose is a calorie-free sweetener with 600 times sweeter sugar, and enzyme-treated stevia stevia is enzyme-treated and has no calories, but its sweetness is about 100-200 times that of sugar and used as a vitamin antioxidant. Citric acid has a sour taste and is used as an acidulant.
<실시예1 : 상온용해성과 무응고성을 가지는 한천의 제조>Example 1 Preparation of Agar with Solubility and Non-Coagulation at Room Temperature
분말한천의 원료가 되는 수세된 원료에 대하여 중량 대비 20배 되는 정제수를 넣고, 염산을 4wt% 첨가하여 10시간 70℃에서 교반한다. 여과 후 여과액을 가성소다를 사용하여 pH 6으로 중화시킨다. 그 후 동결건조, 분쇄하여 분말한천을 제조하였다. Purified water 20 times the weight is added to the washed raw material, which is the raw material of powder agar, and 4 wt% of hydrochloric acid is added and stirred at 70 ° C. for 10 hours. After filtration, the filtrate is neutralized to pH 6 using caustic soda. Thereafter, lyophilized and ground to prepare a powder agar.
이렇게 제조된 분말한천에 대한 용해도는 다음과 같이 실험하였다.The solubility of the powder agar thus prepared was tested as follows.
분말한천 시료 10g를 원심분리관에 취하고 온도 18℃ 증류수 90ml을 가하여 8,000 rpm으로 20분간 원심분리하였다. 상등액을 105℃에서 12시간 건조 후, 고형물을 그대로 측정하여 다음 식의 용해도를 표 1로 정리하였다. 10 g of the powdered agar sample was taken in a centrifuge tube, and 90 ml of temperature 18 ° C. distilled water was added, followed by centrifugation at 8,000 rpm for 20 minutes. After drying the supernatant at 105 ° C. for 12 hours, the solid was measured as it is and the solubility of the following equation was summarized in Table 1.
용해도(%)= (상등액을 건조한 고형물의 무게(g)/처음 시료의 무게(g)) X100Solubility (%) = (weight of dried supernatant (g) / weight of first sample (g)) X100
즉, 표 1에서 알 수 있는 바와 같이 본 발명에 따른 분말한천을 일반한천과 달리 상온(15 ~ 25℃ 범위)와 같이 낮은 온도에서도 용해가 매우 잘 되는 것을 알 수 있었다.That is, as can be seen in Table 1, the powder agar according to the present invention was found to dissolve very well even at a low temperature, such as room temperature (15 ~ 25 ℃ range) unlike the general agar.
여기서 비교예의 일반한천은 전술한 본 발명의 한천 제조 과정 중에서 산처리를 실시하지 않았습니다.Here, the general agar of the comparative example was not subjected to acid treatment in the agar manufacturing process of the present invention described above.
<실시예2 : 한천 음료 제조>Example 2 Preparation of Agar Beverage
정제수 100wt%에 분말한천 1.00wt%, 레몬과즙 분말 0.07wt%, 에리스리톨 5.40wt%, 수크랄로스 0.03wt%, 무수구연산 0.33wt%, 비타민C 0.07wt%, 홍화황색소 0.03wt%, 레몬향분말 0.67wt%를 넣고 교반하며 분말한천 및 각 성분들을 용해시켜 본 발명에 따른 분말한천을 포함하는 음료조성물을 제조하였다. 이때 정제수의 온도는 상온에 해당하는 18℃이므로 본 발명에 따른 분말한천은 상온에서도 용해 가능함을 확인할 수 있었다. 이렇게 제조한 음료조성물의 최종 당도는 4.6~5.6 브릭스(brix), pH는 2.1~2.5로 확인되었다.Purified water 100wt% powdered agar 1.00wt%, lemon juice powder 0.07wt%, erythritol 5.40wt%, sucralose 0.03wt%, citric anhydride 0.33wt%, vitamin C 0.07wt%, yellow safflower 0.03wt%, lemon flavor powder 0.67 To prepare a beverage composition comprising the powder agar according to the present invention by adding and stirring wt% powder agar and each component. At this time, since the temperature of the purified water is 18 ℃ corresponding to room temperature, it could be confirmed that the powder agar according to the present invention can be dissolved even at room temperature. The final sugar content of the beverage composition thus prepared was found to be 4.6-5.6 brix and pH 2.1-2.5.
여기서, 홍화황색소는 비타르계 천연색소로 홍화잇꽃의 관상화를 물로 추출하여 얻을 수 있으며 다른 황색소에 비하여 안정성이 우수하고 수용액은 노란색이다. 또한, 레몬향분말은 레몬향을 내기 위해 첨가하는 분말 형태가 바람직하다.Here, the safflower yellow pigment is a non-tartar-based natural pigment, which can be obtained by extracting the coronary flower of safflower flower with water, and has better stability than other yellow pigments and the aqueous solution is yellow. In addition, the lemon flavor powder is preferably in the form of a powder to add a lemon flavor.
이에, 본 발명에 따르면, 한천이 상온에도 용해가 잘 될 수 있어 다양하게 한천을 응용한 제품에 적용할 수 있으며 제조하는 과정에서 각 원료의 향미나 성분을 그대로 유지할 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공할 수 있다.Therefore, according to the present invention, the agar can be easily dissolved even at room temperature so that it can be applied to a variety of products applied agar, the room temperature solubility and non-coagulation property that can maintain the flavor component of each raw material in the process of manufacturing It can provide a method for producing agar having a beverage composition with the same.
또한, 고농도로 첨가하여도 응고가 되지 않으므로 한천에 대한 거부감을 없앨 수 있고 한천 특유의 기능성을 그대로 가질 수 있는 상온 용해성과 무응고성을 갖는 한천의 제조 방법 및 이를 이용한 음료조성물을 제공할 수 있다.In addition, it is possible to provide a method for producing agar having a room temperature solubility and non-coagulation, which can eliminate the objection to agar because it does not solidify even when added to a high concentration, and can have a functional characteristic peculiar to agar. .
여기서, 본 발명의 일 실시예를 도시하여 설명하였지만, 본 발명의 속하는 기술 분야의 통상의 지식을 가진 자라면 본 발명의 원칙이나 정신에서 벗어나지 않으면서 본 실시예를 변형할 수 있음을 알 수 있을 것이다. 발명의 범위는 첨부된 청구항과 그 균등물에 의해 정해질 것이다.Here, although an embodiment of the present invention has been illustrated and described, it will be appreciated by those skilled in the art that the present embodiment may be modified without departing from the spirit or spirit of the present invention. will be. It is intended that the scope of the invention be defined by the claims appended hereto and their equivalents.
Claims (5)
원료를 수세하고 이물을 제거한 후 수세한 원료의 15 ~ 25배의 정제수를 원료에 투입하는 (1)과정과; 1차 산처리 하는 (2)과정과; 여과하여 여과액을 중화하여 건조, 분쇄하는 (3)과정;를 포함하고,
상기 (2) 산처리과정에서 산은 염산을 포함하되, 산의 양은 상기 원료의 수용액 100wt%에 대하여 4wt% ~ 8wt% 범위이며, 처리 시간은 8시간 ~16시간 사이이고, 처리 온도는 60~70℃ 범위에서 제조된 한천을 상온(15~25℃ 범위)의 정제수 100wt%에 대하여 1 ~ 3wt% 범위로,
상기 정제수 100wt%에 대하여 레몬과즙 분말 0.04wt% ~ 0.10wt% 범위로, 에리스리톨(Erythlitol)을 4.90wt% ~ 5.90wt% 범위로, 수크랄로스(Sucralose) 및 효소처리스테비아(Enzymatically Modified Stevia) 중 어느 하나 이상을 0.01wt ~ 0.05wt 범위로, 비타민C, 구연산으로 구성된 산도조절제군으로부터 선택된 하나 이상을 0.01wt ~ 0.10wt 범위로 더 포함하여 상기 한천은 용해되면서(용해도 78.0 ± 4.0wt% 범위) 응고되지 않는 것을 특징으로 하는 음료조성물.In the beverage composition containing agar,
(1) a process of washing raw materials and removing foreign substances and then inputting 15-25 times purified water to the raw materials; (2) process of primary acid treatment; (3) process of neutralizing the filtrate by filtration to dry and pulverize;
The acid (2) in the acid treatment process includes hydrochloric acid, the amount of acid ranges from 4wt% to 8wt% with respect to 100wt% of the aqueous solution of the raw material, the treatment time is between 8 hours and 16 hours, the treatment temperature is 60 ~ 70 Agar prepared in the range of ℃ 1 to 3wt% relative to 100wt% of purified water at room temperature (15 ~ 25 ℃ range),
Lemon juice powder in the range of 0.04wt% to 0.10wt% with respect to 100wt% of the purified water, 4.90wt% to 5.90wt% of erythritol, any one of sucralose and Enzymatically Modified Stevia The agar is dissolved in the range of 0.01wt ~ 0.05wt, more than one selected from the acidity regulator group consisting of vitamin C, citric acid in the range of 0.01wt ~ 0.10wt and dissolved (solubility 78.0 ± 4.0wt% range) Beverage composition, characterized in that not.
상기 (3)과정의 중화처리시에 사용되는 알칼리는 가성소다를 포함하고, 0.1wt% ~ 10wt% 범위를 포함하는 것을 특징으로 하는 음료조성물.The method of claim 1,
Alkali used in the neutralization process of the step (3) comprises a caustic soda, characterized in that the beverage composition comprises a 0.1wt% ~ 10wt% range.
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