KR101857430B1 - Method for manufacturing the extract of dendropanax morbifera - Google Patents
Method for manufacturing the extract of dendropanax morbifera Download PDFInfo
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- KR101857430B1 KR101857430B1 KR1020150154598A KR20150154598A KR101857430B1 KR 101857430 B1 KR101857430 B1 KR 101857430B1 KR 1020150154598 A KR1020150154598 A KR 1020150154598A KR 20150154598 A KR20150154598 A KR 20150154598A KR 101857430 B1 KR101857430 B1 KR 101857430B1
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- South Korea
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- extract
- drying
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- heating
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Links
- 238000000034 method Methods 0.000 title claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 241000392544 Dendropanax morbifer Species 0.000 title description 3
- 238000010438 heat treatment Methods 0.000 claims abstract description 25
- 238000004108 freeze drying Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002023 wood Substances 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 238000003303 reheating Methods 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims description 15
- 230000032683 aging Effects 0.000 claims description 4
- 238000005520 cutting process Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 239000008213 purified water Substances 0.000 abstract description 6
- 238000010298 pulverizing process Methods 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000000605 extraction Methods 0.000 description 7
- 239000004615 ingredient Substances 0.000 description 5
- 239000004480 active ingredient Substances 0.000 description 4
- 238000007602 hot air drying Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 235000004347 Perilla Nutrition 0.000 description 2
- 244000124853 Perilla frutescens Species 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 235000020510 functional beverage Nutrition 0.000 description 2
- 235000013376 functional food Nutrition 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 229920001277 pectin Polymers 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000261585 Hadrobregmus pertinax Species 0.000 description 1
- 241000218657 Picea Species 0.000 description 1
- 244000184734 Pyrus japonica Species 0.000 description 1
- 238000010793 Steam injection (oil industry) Methods 0.000 description 1
- NBZANZVJRKXVBH-GYDPHNCVSA-N alpha-Cryptoxanthin Natural products O[C@H]1CC(C)(C)C(/C=C/C(=C\C=C\C(=C/C=C/C=C(\C=C\C=C(/C=C/[C@H]2C(C)=CCCC2(C)C)\C)/C)\C)/C)=C(C)C1 NBZANZVJRKXVBH-GYDPHNCVSA-N 0.000 description 1
- FSRZGYRCMPZNJF-UHFFFAOYSA-N beta-Cubebene Natural products C12C(C(C)C)CCC(C)C32C1C(=C)CC3 FSRZGYRCMPZNJF-UHFFFAOYSA-N 0.000 description 1
- FSRZGYRCMPZNJF-KHMAMNHCSA-N beta-cubebene Chemical compound CC(C)[C@@H]([C@H]12)CC[C@@H](C)[C@]32[C@@H]1C(=C)CC3 FSRZGYRCMPZNJF-KHMAMNHCSA-N 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/30—Foods, ingredients or supplements having a functional effect on health
- A23V2200/318—Foods, ingredients or supplements having a functional effect on health having an effect on skin health and hair or coat
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
Abstract
The present invention relates to a method for producing an extract of Hokkaido chinensis, which is capable of obtaining a high-quality product at a high yield by extracting it by a vacuum steam heating method and pulverizing it by a freeze-drying method. More particularly, the present invention relates to a method for manufacturing a wood-burning wood comprising: Adding purified water to the cut woods, heating the mixture at 100 to 160 ° C for 7 to 9 hours by a vacuum steam heating method, reheating it at a low temperature and naturally cooling it, And then filtering and concentrating the extract extracted in step (b) followed by lyophilization through freeze drying.
Description
More particularly, the present invention relates to a method for producing an extract of Hokkaido japonica with high yields by extracting by vacuum steam heating method and pulverizing by freeze drying method.
Dendropanax morbifera Lev. Is an evergreen broad-leaved arborescens in Araliaceae and Ogalli, native to Korea, which grows up to 15 meters high. The young branches are green and lustrous, the flowers bloom in June, and the fruit 7 to 19 mm long is black. It is a mature plant that grows in areas with a minimum temperature of minus 2 ℃ or more and an average annual temperature of 12 ~ 15 ℃. Hwangchil is a rare species that grows only inland in the southwestern part of the Korean peninsula, the coast, books, and Jeju Island. Currently, there are Shinan, Jindo, Wando and Jeju Island in the present area. There are small habitats in Haenam, Jangheung, Kangjin, Goheung, Seungju, Gwangyang and Yeosu. Hwangchil is also called golden gold because it is golden. The golden light of Huangchil becomes brighter when exposed in the sun. Unlike lacquer, which gives out black color, it has the characteristic of applying golden color to the product while preserving the pattern and color of the product. In addition, it has excellent painting ability for any material such as wood, metal, leather, and paper. In addition, furniture, upholstery, and soothbrush are applied to the burrs, cleanses the head and has the effect of comforting the mind and body.
In general, Huangchil is composed of 66.7% of non-volatile component, 10.8% of direction component, 8.1% of moisture and 14.4% of solid content, which is a paint component forming a golden color film. Especially, the direction component is mainly β- cubebene,? -cellinene,? -cadinene, and the like. The oriental ingredients contained in Huangchil have various pharmacological actions as well as value as a foot care which makes the mind and body clean and comfortable, and thus it is highly useful as perfume, cosmetics and functional food and beverage. However, there is still a lack of research on how to extract effective ingredients of Huangchil at high yield.
The present invention provides a method for producing an extract of Hokkaido tree which can obtain a high-quality product at a high yield.
The present invention relates to a method for producing a woody plant, Adding refined water to the cut woods, heating it at 100 to 160 ° C for 7 to 9 hours by vacuum steam heating method, reheating at low temperature and naturally cooling to extract the whitewash (step b); And a step (c) of filtering and concentrating the extract extracted in step b) followed by lyophilization (step c). The manufacturing method may further include drying the cut woods between step a and step b.
Washing and then cutting
Washing is a basic step for removing the impurities and extracting the original ingredients of the burnt grass at a later stage, and purified water can be used.
The cutting is carried out in order to widen the surface area of the perennial wood, so that the extraction can be easily carried out in the posternum extraction step. It is preferable to cut the washed woods to a size of 2 to 3 cm.
The manufacturing method may further include a straightening step before the cutting step after the washing. Jung-seon is carried out to remove foreign substances and obtain pure products. However, it does not use pesticides because it does not contain many foreign substances.
Drying of cut woodgrain
The step of drying the cut woods can be carried out by drying the cut woods so that the water content of the cut woods is 10% (w / w) or less. It is desirable to produce a high quality yellowish extract and to maintain the moisture content in the above range for safe storage and distribution of the yellowish. The drying process is carried out in order to prevent fungi or deterioration of the active ingredient when large quantities of woodweed are stored. In the past, natural drying methods were generally used, but in the case of natural drying, there was a problem in that the effective ingredient of the woody mildew between the bark and the wood penetrated into the wood, making extraction difficult. In the present invention, a rapid drying method is used to solve this problem. Rapid drying can be carried out by using a drier at 70 to 80 ° C for 7 to 9 hours, more preferably for 8 hours. When such a rapid drying method is used, there is an advantage that the extraction efficiency can be increased because the effective ingredient of the woody spruce does not penetrate into the wood during the drying process.
Step of preparing Hwangchu tree extract
The step of preparing the extract is carried out by adding purified water to the cut wood, heating it by a vacuum steam heating method, reheating it at a low temperature and cooling it naturally.
The amount of purified water to be applied to the perilla is preferably 3 to 5 times the weight of the perilla.
The heating by the vacuum steam heating method is carried out by heating at 100 to 160 ° C for 7 to 9 hours, more preferably for 8 hours by using an extractor of vacuum steam heating (heating by heating steam injection) can do. Conventionally, since the direct-burning method in which the heating container is heated by heating is used, there has been a problem that the woody wood contacted with the inner wall of the high-temperature extractor is burned or denatured.
The low temperature aging can be carried out by aging (leaving) at 50 to 70 DEG C for 22 to 26 hours, more preferably at 60 DEG C for 24 hours. Through the above-mentioned aging process, the volume of Hwigae-jinja can be expanded and the extraction can be facilitated.
Reheating can be carried out by heating at 90 to 110 ° C for 3 to 5 hours, more preferably at 98 ° C for 4 hours, and natural cooling for 3 to 5 hours, more preferably for 4 hours at room temperature Can be performed.
Filtration, concentration and powdering steps
This step can be performed by filtering and concentrating the extract extracted in step b, followed by lyophilization through freeze drying.
Through the filtration, starch, pectin, etc., which are polymeric substances, may be removed from the extract of step b to purify the pure yellowish component.
The concentration may be carried out by using a conventional concentrator in a concentration of 25 to 35 brix, more preferably 30 bricks. The concentration may be performed at 60 to 70 ° C for 5 to 6 hours. In the case of concentration in the above-mentioned concentration range, it is possible to maintain an appropriate solid content and obtain a fine powder in the subsequent pulverization step. Also, by concentrating within the above-mentioned period of time, breakage of the active ingredient can be minimized.
The freeze-drying can be performed by freezing at 80 to 90 ° C for 48 to 50 hours to remove moisture by sublimation to obtain a powder. In case of powdering by the above-mentioned method, it can be pulverized into particles of an appropriate size, which can be advantageous in terms of solubility, and powdery state can be obtained in a very clean state, so that a product of good quality can be obtained. In addition, it is possible to solve the problem that the active ingredient is destroyed by hot air drying.
According to the present invention, a high-quality product can be obtained at a high yield by extracting by a vacuum steam heating method and pulverizing by a freeze-drying method. More specifically, the present invention can solve the problem of extraction by the conventional direct method by extracting by the vacuum steam heating method. According to the flame-directing method, there is a problem that burnt wood contacted with the inner wall of the high-temperature extractor is burned or denatured, but the present invention does not cause such a problem. Also, by applying the pulverization method by freeze drying, not by hot air drying, the problem of destruction of the active ingredient by hot air drying can be solved. In addition, the extraction efficiency can be improved by applying the rapid drying method instead of the natural drying method in the drying step.
The extract of Wuchucho extract prepared according to the present invention can be applied to functional foods and beverages. In particular, Huangchil is safe for skin, excellent in moisturizing effect, inhibited melanin generation and skin whitening effect, and can also be used as a cosmetic composition.
Hereinafter, the present invention will be described in more detail with reference to Examples. The objects, features and advantages of the present invention will be readily understood through the following examples. The present invention is not limited to the embodiments described herein, but may be embodied in other forms. The embodiments described herein are provided to enable those skilled in the art to fully understand the spirit of the present invention. Therefore, the present invention should not be limited by the following examples.
EXAMPLES Example 1: Preparation of woodworm extract
500 kg of Hwangchujang were washed with water and then cut into 3 cm. The cut woods were dried at 75 ° C for 8 hours (dried at a yield of 500kg and weighed 250 kg), and then purified water of three times the weight of the woodchips was added to 250 kg of dried woodchips, and then heated at 120 ° C for 8 hours. (Left to stand) at 60 占 폚 for 24 hours at low temperature. After that, the extract was reheated at 98 ° C for 4 hours and then naturally cooled for 4 hours. The extract was filtered to remove starch, pectin and other macromolecular substances. The extract was concentrated for 5 to 6 hours with a conventional concentrator to obtain a concentration of 30 brix. After that, the mixture was freeze-dried at 80 to 90 ° C for 48 to 50 hours to prepare 25 kg of powdered Hwangchulchu extract (yield: 10%).
Comparative Example : Preparation of Hwangchulak Extract according to the conventional method
The extract was prepared by adding 3 times of purified water to 250 kg of the dried tree and heating at 90 to 98 ° C for 12 hours. The extract was filtered to prepare 10 kg of the extract (4% yield)
Claims (5)
Adding refined water to the cut woods, heating it at 100 to 160 ° C for 7 to 9 hours by vacuum steam heating, reheating at low temperature and naturally cooling to extract the whitewash (step b); And
(C) filtering and concentrating the extract extracted in step (b), followed by lyophilization through freeze drying,
Further comprising the step of drying the cut woods at 70 to 80 DEG C for 7 to 9 hours between the step a and the step b,
Wherein the vacuum steam heating method is performed by injecting heated steam and heating the vacuum steam heating method.
Wherein the low-temperature aging is carried out at 50 to 70 ° C for 22 to 26 hours, the reheating is carried out at 90 to 110 ° C for 3 to 5 hours, and the natural cooling is carried out for 3 to 5 hours. A method for producing a tree extract.
Wherein the concentration in step c is concentrated to a concentration of 25 to 35 brix.
Wherein the freeze-drying is carried out at 80 to 90 ° C for 48 to 50 hours in step c.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020150154598A KR101857430B1 (en) | 2015-11-04 | 2015-11-04 | Method for manufacturing the extract of dendropanax morbifera |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020150154598A KR101857430B1 (en) | 2015-11-04 | 2015-11-04 | Method for manufacturing the extract of dendropanax morbifera |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20170052303A KR20170052303A (en) | 2017-05-12 |
| KR101857430B1 true KR101857430B1 (en) | 2018-05-14 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020150154598A KR101857430B1 (en) | 2015-11-04 | 2015-11-04 | Method for manufacturing the extract of dendropanax morbifera |
Country Status (1)
| Country | Link |
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| KR (1) | KR101857430B1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20230075955A (en) | 2021-11-23 | 2023-05-31 | 경성대학교 산학협력단 | Parmaceutical composition comprising extract of Dendropanax morbiferus including chlorogenic acid with enhanced bioavailability as an effective componinet and preparation method thereof |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101961735B1 (en) | 2017-08-29 | 2019-03-25 | (주)비엔텍 | Method for manufacturing extract of dendropanax morbifera having increased amount of l-arginine and gaba |
| KR102010551B1 (en) * | 2018-01-30 | 2019-08-13 | 나봉주 | Method for producing Dendropanax morbifera powder with increased functionality using Dendropanax morbifera product produced year round by cultivation under structure |
| KR101875738B1 (en) * | 2018-04-30 | 2018-07-06 | 정수화 | extraction method for a lacquer liquid of lacquer tree's a leaf and seeds |
| KR102069542B1 (en) * | 2018-10-05 | 2020-02-24 | 박순애 | Meat bolide in plain water manufacturing method composition containing extract of dendropanax morbiferus |
| KR102402119B1 (en) * | 2019-12-12 | 2022-05-26 | 해미원 영어조합법인 | Abalone gimbap and manufacturing method for the same |
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2015
- 2015-11-04 KR KR1020150154598A patent/KR101857430B1/en active IP Right Grant
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20230075955A (en) | 2021-11-23 | 2023-05-31 | 경성대학교 산학협력단 | Parmaceutical composition comprising extract of Dendropanax morbiferus including chlorogenic acid with enhanced bioavailability as an effective componinet and preparation method thereof |
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| KR20170052303A (en) | 2017-05-12 |
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