KR101793973B1 - Apparatus for continuous process electric radiation using spiral needle and system for producting nano fiber - Google Patents

Apparatus for continuous process electric radiation using spiral needle and system for producting nano fiber Download PDF

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Publication number
KR101793973B1
KR101793973B1 KR1020160009865A KR20160009865A KR101793973B1 KR 101793973 B1 KR101793973 B1 KR 101793973B1 KR 1020160009865 A KR1020160009865 A KR 1020160009865A KR 20160009865 A KR20160009865 A KR 20160009865A KR 101793973 B1 KR101793973 B1 KR 101793973B1
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South Korea
Prior art keywords
probe
probes
electrospinning
predetermined
liquid
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KR1020160009865A
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Korean (ko)
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KR20170089532A (en
Inventor
이경진
길만재
문성준
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충남대학교 산학협력단
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning
    • D01D5/0061Electro-spinning characterised by the electro-spinning apparatus
    • D01D5/0069Electro-spinning characterised by the electro-spinning apparatus characterised by the spinning section, e.g. capillary tube, protrusion or pin
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning
    • D01D5/0015Electro-spinning characterised by the initial state of the material
    • D01D5/003Electro-spinning characterised by the initial state of the material the material being a polymer solution or dispersion
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning
    • D01D5/0061Electro-spinning characterised by the electro-spinning apparatus
    • D01D5/0076Electro-spinning characterised by the electro-spinning apparatus characterised by the collecting device, e.g. drum, wheel, endless belt, plate or grid
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning
    • D01D5/0061Electro-spinning characterised by the electro-spinning apparatus
    • D01D5/0092Electro-spinning characterised by the electro-spinning apparatus characterised by the electrical field, e.g. combined with a magnetic fields, using biased or alternating fields
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/70Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
    • D04H1/72Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
    • D04H1/728Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by electro-spinning
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures

Abstract

The present invention relates to a continuous process electrospinning apparatus using a spiral probe and a polymer nanofiber production system using the same.
More specifically, according to an embodiment of the present invention, a continuous process electrospinning device using a helical probe includes at least one probe for performing electrospinning by spraying a polymer material in liquid form, and a probe capable of rotating 360 degrees at a predetermined speed, Wherein the one or more probes are spaced apart from one another by a predetermined distance and the spacing of each of the one or more probes may be helical.

Description

TECHNICAL FIELD [0001] The present invention relates to a continuous process electrospinning apparatus using a spiral probe, and a polymer nanofiber production system using the same. [0002]

The present invention relates to a continuous process electrospinning apparatus using a spiral probe and a polymer nanofiber production system using the same, and more particularly, to a method of manufacturing a polymer nanofiber production system using at least one of the probes, And a polymer nanofiber production system using the same.

Since the industrialization of modern society, there has been a remarkable development of nano-biotechnology. Therefore, attempts to extend these nano-biotechnologies to the high-tech industries have been actively carried out.

The electrospinning fiber produced according to the above electrospinning process has a very large surface area per unit volume and is applied to various physical properties depending on the applied polymer material. And it is widely used in the production of special fibers such as nanofibers.

On the other hand, since the electrospinning process is very simple and uses an electric field, there is an advantage that nano-sized fibers that can not be produced in a general spinning process can be produced.

Accordingly, attempts have been made to increase the number of probes of the probe used in the electrospinning process to several but not one, in order to produce the nano-sized fibers. However, the probe of the probe used in the electrospinning process In the case of a plurality of electrodes, generally, one or more probes are arranged in a straight line at predetermined intervals.

However, in such a case, there is a problem that the electric interaction between the electric fields induced in each of the probes causes the efficiency of electrospinning to be lowered. Accordingly, a large number of probes are disposed in the probe at one time to produce nano- There is an additional problem that it is difficult to do so.

In addition, in a need-less electrospinning process, radiation is generally performed from above to below, that is, in a vertical direction. In this vertical process, in order to overcome gravity, about 30 to 60 Kv (Kilovolts) of high voltage. Therefore, there is a problem that the electrospinning is performed at a relatively high voltage, which may cause an excessive cost to the process.

Accordingly, a method for solving the above problems is required.

Korean Registered Patent No. 10-2008-7000423 (published on Jan. 17, 2008)

SUMMARY OF THE INVENTION It is an object of the present invention to provide a probe for use in an electric spiral in which a probe is spirally attached so as to continuously produce a large amount of nanofibers by reducing electrical interaction between probes.

It is another object of the present invention to provide an electric disposable probe capable of producing a large amount of nanofibers even at a low voltage by generating a centrifugal force by raising the ground at a predetermined angle and improving the rotation speed of the probe.

It is a further object of the present invention to provide an electric room application probe that provides separate conduction to minimize voltage loss and increase electrical efficiency.

The technical problems to be solved by the present invention are not limited to the technical problems and other technical problems which are not mentioned can be understood by those skilled in the art from the following description.

According to an aspect of the present invention, there is provided a continuous process electrospinning device using a spiral probe, including: at least one probe for injecting a liquid polymer material to perform electrospinning; Wherein the one or more probes are spaced apart from each other by a predetermined distance and the spacing of each of the one or more probes may be helical.

A continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention includes a conductive line connected to each of the at least one probe and controlling a voltage applied to the electrospinning apparatus to be guided to each of the at least one probe .

In the continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention, the probe rod is connected to a solution storage unit containing a liquid polymer material, and the liquid polymer material is connected to the probe Can be delivered in a drop form and used for the electrospinning.

In a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention, the probe may be configured to support a voltage required for the electrospinning on a liquid polymer material in the solution reservoir and supply a predetermined voltage And can be supplied from a power supply unit.

In a continuous process electrospinning apparatus using a helical probe according to an embodiment of the present invention, the injection of the liquid polymeric material, which the at least one probe performs for electrospinning, is performed while the probe is rotating 360 degrees And each time the one or more probes included in the probe are positioned at a predetermined injection point.

In the continuous process electrospinning apparatus using the spiral probe according to an embodiment of the present invention, the predetermined injection point may be inclined by a predetermined angle range with respect to the vertical direction of the probe.

In the continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention, the predetermined angle range may be 45 degrees to 60 degrees.

In a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention, the liquid type polymer material injected from the at least one probe is collected by a conductive conveyor belt rotating at a constant speed, and the conductive conveyor belt May be inclined by the predetermined angle range with respect to the vertical direction of the probe.

In a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention, the probe may be non-conductive.

According to an aspect of the present invention, there is provided a polymer nanofiber production system including a continuous process electrospinning device using a spiral probe, comprising: a solution reservoir containing a liquid polymer material; A probe which is mounted on the inside of the solution storing part and pulls up the liquid type polymeric material contained in the solution storing part in a droplet form, a power supply part which is supported on the liquid type polymer material in the storing part and supplies a voltage of a predetermined size, At least one probe coupled to the probe and injecting the polymeric material in liquid form to conduct electrospinning and a conductive conveyor belt for collecting the polymeric material injected from the at least one probe to produce nanofibers, Wherein each of the one or more probes has a predetermined distance Wherein the spacing of each of the one or more probes is in the form of a spiral and the injection of the polymeric material in liquid form carried out by the one or more probes for electrospinning is performed while the probe is rotating 360 degrees And each time the one or more probes included in the probe are positioned at a predetermined injection point.

According to the present invention as described above, the following effects can be obtained. However, effects obtained through the present invention are not limited thereto.

First, according to the present invention, since an electric room probe having a spiral probe is provided, the electrical interaction between the probes is reduced, so that a large amount of nanofibers can be continuously produced.

Secondly, according to the present invention, since the ground is rotated at a predetermined angle and the rotating speed of the probe is improved, the nanofiber can be manufactured even at a low voltage due to the centrifugal force of the probe.

Thirdly, according to the present invention, since the electrosynthetic probe forming a separate conduction is provided, the voltage loss of the rotating probe can be minimized, and the electrical efficiency of the probe can be increased.

The effects obtained by the present invention are not limited to the above-mentioned effects, and other effects not mentioned can be clearly understood by those skilled in the art from the following description will be.

1 is a view for explaining electrospinning results of an electrospinning apparatus including a needle in a probe.
Fig. 2 is a view for explaining electrospinning results of an electrospinning apparatus including two needles in a probe. Fig.
3 is a view for explaining electrospinning results of an electrospinning apparatus including three needles in a probe.
4 is a view for explaining a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention.
5 is a diagram illustrating a probe of a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention.
6 is a view for explaining electrospinning results of a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention.

Hereinafter, preferred embodiments according to the present invention will be described in detail with reference to the accompanying drawings. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The following detailed description, together with the accompanying drawings, is intended to illustrate exemplary embodiments of the invention and is not intended to represent the only embodiments in which the invention may be practiced.

It is to be understood that both the foregoing general description and the following detailed description of the present invention are exemplary and explanatory and are intended to provide further explanation of the invention as claimed. Only.

In some instances, well-known structures and devices may be omitted or may be shown in block diagram form, centering on the core functionality of each structure and device, to avoid obscuring the concepts of the present invention. In the following description, the same components are denoted by the same reference numerals throughout the specification.

Throughout the specification, when an element is referred to as "comprising" or " including ", it is meant that the element does not exclude other elements, do.

Also, the term "part" in the description means a unit for processing at least one function or operation, which may be implemented by hardware, software, or a combination of hardware and software. Furthermore, the terms " a or an, "" one," and similar related terms, unless the context clearly dictates otherwise or clearly contradicted by context, As used herein.

In addition, specific terms used in embodiments of the present invention are provided to facilitate understanding of the present invention. Unless otherwise defined, all terms used herein, including technical or scientific terms, And have the same meaning as commonly understood by those of ordinary skill in the art. The use of such a specific term may be changed to other forms without departing from the spirit of the present invention.

Hereinafter, preferred embodiments according to the present invention will be described in detail with reference to the accompanying drawings. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The following detailed description, together with the accompanying drawings, is intended to illustrate exemplary embodiments of the invention and is not intended to represent the only embodiments in which the invention may be practiced.

Figs. 1 to 3 are diagrams for explaining electrospinning results of an electrospinning apparatus including one to three probes in a probe, respectively. Fig.

The electrospinning device to be described below includes a probe, a probe coupled to the probe, a solution reservoir for supplying a polymer material for electrospinning to the probe, a power supply for supplying a voltage required for the electrospinning, And a collecting part for collecting the fibers radiated as the probe sprays the polymer material.

1 (a) showing a structure of a probe including one probe, and FIG. 1 (b) showing a result of performing electrospinning using the probe. FIG. 1 c) shows a screen of the result of electrospinning using a probe including the probe, which is observed with a microscope.

As shown in FIG. 1 (b), when electrospinning is performed using a probe (FIG. 1 (a)) including one probe, it can be confirmed that the radiation is concentrated in a specific region only, As shown in FIG. 1 (c), when observed under a microscope, the morphologies of the spun fibers are not aggregated but collected in a separated state.

Next, referring to FIG. 2, a structure of a probe including two probes is shown in FIG. 2 (a), and FIG. 2 (b) is a result of performing electrospinning using the probe. FIG. 2 (c) is a view of a result of electrospinning using a probe including the two probes, which is observed with a microscope.

Here, referring to FIG. 2 (b), when compared with FIG. 2 (b) showing the result of electrospinning using a probe including one probe, the radiation is not concentrated in a specific region, It can be confirmed that it is divided into a plurality of regions, and in addition, it can be confirmed that some lumps are included in the radiated region. 2 (c), it can be confirmed that the morphologies of the radiated fibers are collected in a state where they are partially gathered with each other. Thus, in a form different from that shown in FIG. 1 (c) You can see what is being captured.

3 (a) shows the structure of a probe including three probes, FIG. 3 (b) shows a result of performing electrospinning using the probe, and FIG. 3 3 (c) shows the result of the electrospinning using a probe including the three probes, which is observed with a microscope.

Referring to FIG. 3 (b), when compared with the result of electrospinning using a probe including one or two probes as shown in FIGS. 1 (b) and 2 (b) (C) or FIG. 2 (c), in which the morphology of the fiber has one characteristic and is consistently collected, (c), it can be confirmed that some of the fibers are collected separately, and they are collected even in a state where they are bundled together. Thus, it can be confirmed that the fibers are collected in various forms inconsistently.

1 through 3, the results of the electrospinning using a probe including one to three probes showed that the smaller the number of probes in the probe, the narrower the emission was And furthermore, it can be confirmed that the more the number of probes in the probe, the more the collection of fibers becomes clumped or distorted.

The reason why the shape of the fibers is changed according to the number of probes included in the probes is that the electrical interaction between the electric fields induced in each of the probes causes the efficiency of electrospinning to deteriorate.

More specifically, when one to three probes are included in the probe, it is general that the probes are arranged in the forward direction. Accordingly, when an electric current for electrospinning flows to the probe bar made of a conductive material and an electric field is induced for each probe, the electric fields induced in the respective probes cause electric interaction and affect each other. And only the probe at both ends of the probe will emit radiation, affecting the electrospinning performed by each probe.

Therefore, if the number of probes included in one probe increases, the distance between the probes in the probe must be reduced, and the distance between the probes becomes closer to each other. As a result, if a large number of probes are included in one of the probes, there is a problem that the efficiency of electrospinning by the probes is greatly reduced because the influence due to the electrical interaction between the probes is very large. .

Accordingly, in order to solve the above-mentioned problem, the present invention is to describe a probe for use in an electric furnace with a probe attached spirally so as to reduce the electrical interaction between the probes and continuously produce a large amount of nanofibers. Hereinafter, a detailed description will be given with reference to FIG. 4 and FIG.

FIG. 4 is a view for explaining a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention. FIG. 5 is a cross-sectional view of a probe of a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention. Fig.

4, a continuous process electrospinning device using a spiral probe according to an embodiment of the present invention includes a probe 1 including at least one probe, a probe 1 for supplying a voltage required for electrospinning of the electrospinning device A solution reservoir (3) for supplying a polymeric material for electrospinning to the probe, and a controller connected between the power supply and the solution reservoir for supplying a voltage supplied from the power supply to the solution reservoir A conductive bar for collecting the fibers radiated as the probe sprays the polymer material, and a rotating bar for guiding the rotation of the conductive conveyor belt. (5, 6).

4, the continuous process electrospinning apparatus using the spiral probe according to an embodiment of the present invention may further include other configurations other than the configurations described above, and some of the configurations described above may be omitted .

Referring again to FIG. 4, the probe 1 may comprise one or more probes. Hereinafter, for convenience of explanation, it is assumed that the probe includes a plurality of probes 8 as shown in FIG. 5. However, according to an embodiment of the present invention, . ≪ / RTI >

At this time, the probe bar 1 may have a part of the structure supported on the solution storage part 3 containing the liquid polymeric material, Of the polymeric material. At this time, the liquid polymer material may be pulled up by the probe 1 in a droplet form, thereby inducing Taylor Cone formation.

The probe 1 may include a plurality of probes. The probes may be formed by injecting the high-character material drawn from the solution reservoir 3 in the form of droplets by the probe 1, Radiation can be performed.

In addition, in order to solve the above-mentioned problems, the continuous process electrospinning apparatus using the spiral probe according to an embodiment of the present invention has a configuration in which each of the multiple probes 8 has a predetermined distance And the spacing of each of the multiple probes 8 may be helical.

In this way, when the predetermined number of the probes 8 are spaced apart from each other in a spiral shape, the electrical interaction between the probes 8 can be reduced, As more probes can be included in the probe, more probes can be used to produce more efficient nanofibers because more efficient electrospinning can be achieved as the number of probes increases.

Also, in the case of conventional probes or conventional needless electrospinning, it is common that the material of the probe or rotating rod is made of a conductor such as metal, so that the voltage of the probe or rotating rod There is a problem that efficiency of electrospinning is somewhat deteriorated due to loss.

However, in the case of the continuous process electrospinning apparatus using the spiral probe according to an embodiment of the present invention, the probe may be made of non-conductive material, and each of the multiple probes 8 included in the probe rod 1 May be connected to a conductive line (9).

At this time, the conductive line 9 may be connected to each of the plurality of probes 8 to control the voltage applied to the electrospinning device to be induced in each of the plurality of probes 8 have.

When the plurality of probes 8 are connected through the conductive line 9, the voltage applied to the probe 1 can be concentrated on each of the probes 8, The efficiency of the continuous process electrospinning apparatus using the spiral probe according to one embodiment can be further increased.

Referring again to FIG. 4, the probe may perform electrospinning by spraying the high-character material drawn from the solution reservoir 3 in a droplet form, as described above .

At this time, the probe 1 can rotate 360 degrees at a predetermined speed, and each of the probes of the multiple probes included in the probe 1 while the probe is rotating 360 degrees is rotated at a predetermined injection point The liquid type polymer material is injected every moment it is positioned to perform the electrospinning.

According to an embodiment of the present invention, the predetermined injection point may be inclined by a predetermined angle range with respect to a vertical direction of the probe, and the predetermined angle range may be a vertical direction of the probe It can be from 45 degrees to 60 degrees as a standard.

At this time, the liquid type polymer material ejected from the predetermined number of ejection points from the multiple number of probes is transferred to the conductive conveyor belt 7, which rotates at a constant speed by the rotation bar 6, And the conductive conveyor belt may be inclined by an angle range of 45 ° to 60 ° with respect to the vertical direction of the probe bar.

For example, when each of the plurality of probes injects the polymer material in the form of liquid to perform the electrospinning, the injection point is in an angle range of 45 degrees with respect to the vertical direction of the probe, May be positioned in an angular range of 45 degrees with respect to a vertical direction of the probe, which is an angle range in which the injection is performed.

That is, in the case of a conventional needleless electrospinning device, since the direction of electrospinning is vertical (from top to bottom), electrospinning is performed using a high voltage of about 30 to 60 kV (kilovolts) And thus there is a problem that a high voltage is required for electrospinning.

However, in the case of the electrospinning device according to an embodiment of the present invention, at a specific point inclined by 45 to 60 degrees with respect to the vertical direction of the probe, The electrospinning can be performed at a lower voltage (about 15 to 18 kV) due to the centrifugal force induced by the rotation of the probe bar 1, since the liquid type polymer material is injected to perform the electrospinning. Therefore, it becomes possible to perform electrospinning at a relatively low voltage, so that a larger amount of nanofibers can be produced at the same voltage, thereby increasing the efficiency of the electrospinning process and reducing the cost of the electrospinning process There is an effect that can be done.

6 is a view for explaining electrospinning results of a continuous process electrospinning apparatus using a spiral probe according to an embodiment of the present invention.

6 (a), poly (methyl methacrylate) (PMMA) polymer produced according to electrospinning performed by using a probe having a plurality of probes arranged in a straight line in a positive direction FIG. 6 (b) is a graph showing the results of a microscopic observation of a plurality of probes according to an embodiment of the present invention, and FIG. 6 And a microscopic observation of the resulting polymethacrylate (PMMA) polymer is shown.

The PMMA polymer shown in FIG. 6 (a) and the PMMA polymer shown in FIG. 6 (b) are different from each other only in the arrangement of the probe included in the probe, 10% THF (tetrahydrofuran) solvent) are assumed to be the same.

6 (a), when a plurality of probes are arranged in a line in a positive direction and a current for electrospinning flows through the probe, the electric fields induced in the respective probes are electrically The fibers shown in Fig. 6 (a) are formed to have a coherent or distorted shape because they interact with each other and affect each other and influence the electrospinning performed by each probe according to such influence .

6 (a), an electrospinning device according to an embodiment of the present invention, that is, a plurality of probes arranged in a helical shape spaced apart from each other by a predetermined distance, And that the fibers shown in Fig. 6 (b) are well separated from each other without being clumped or distorted.

As described above, when a plurality of the probes are spaced apart from each other in a spiral manner, the electrical interaction between the probes can be reduced, And the quality of the fiber can be further improved.

 It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims. Therefore, the disclosed methods should be considered in an illustrative rather than a restrictive sense. It is intended that the present invention cover the modifications and variations of this invention provided they come within the scope of the appended claims and their equivalents.

The continuous process electrospinning apparatus using the spiral probe of the present invention and the polymer nanofiber production system using the same can be applied to various apparatuses for performing electrospinning and various systems for producing polymer nanofibers.

1: probe 2: power supply
3: solution storage part 4: conductor
5: grounding rod 6: rotating rod
7: Conductive conveyor belt 8: Multiple probe
9: Conductive line

Claims (10)

A continuous process electrospinning apparatus using a spiral probe,
A plurality of probes for ejecting a polymer material in liquid form to perform electrospinning; And
And a probe including a plurality of probes rotatable 360 degrees at a predetermined speed,
Wherein the probe is nonconductive,
Wherein each of the plurality of probes is spaced apart from each other by a predetermined distance and the spacing of each of the plurality of probes is in the form of a spiral.
The method according to claim 1,
Further comprising a conductive line connected to each of the plurality of probes to control a voltage applied to the electrospinning device to be guided to each of the plurality of probes.
The method according to claim 1,
Wherein the probe is connected to a solution reservoir containing a liquid polymeric material,
Wherein the polymeric material in liquid form is delivered to the probe in a drop form and used for the electrospinning.
The method of claim 3,
Wherein the probe is supplied with a voltage required for the electrospinning from a power supply unit that supports a liquid type polymer material in the solution reservoir and supplies a predetermined voltage.
The method of claim 1, wherein
Wherein the injection of the liquid polymeric material performed by the plurality of probes for electrospinning is performed at a moment when each of the plurality of probes included in the probe rod is located at a predetermined injection point while the probe is rotating 360 degrees Wherein the first electrode and the second electrode are electrically connected to each other.
6. The method of claim 5,
Wherein the predetermined injection point is inclined by a predetermined angle range with respect to a vertical direction of the probe.
The method according to claim 6,
Wherein the predetermined angular range is from 45 degrees to 60 degrees.
8. The method of claim 7,
The liquid polymer material injected from the plurality of probes is collected by the conductive conveyor belt rotating at a constant speed,
Wherein the conductive conveyor belt is inclined by the predetermined angle range with respect to a vertical direction of the probe bar.
delete 1. A production system for polymer nanofibers comprising a continuous process electrospinning device using a spiral probe,
A solution reservoir containing a liquid polymeric material;
A power supply unit which is supported by the liquid polymer material in the solution reservoir and supplies a voltage of a predetermined magnitude; And
A probe attached to the inside of the solution storage part to pull up the liquid type polymer material contained in the solution storage part in a droplet form;
A plurality of probes coupled to the probe and injecting the polymeric material in liquid form to conduct electrospinning; And
And a conductive conveyor belt for collecting the polymer material injected from the plurality of probes to produce nanofibers,
Wherein each of the plurality of probes is spaced apart from each other by a predetermined distance, the spacing of each of the plurality of probes is in the form of a spiral,
Wherein the injection of the liquid polymeric material for the plurality of probes for electrospinning is performed at a moment when each of the plurality of probes included in the probe rod is located at a predetermined injection point while the probe is rotating 360 degrees Respectively,
Wherein the probe is a nonconductor.
KR1020160009865A 2016-01-27 2016-01-27 Apparatus for continuous process electric radiation using spiral needle and system for producting nano fiber KR101793973B1 (en)

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US20110311671A1 (en) 2008-10-17 2011-12-22 Tong Lin Electrostatic spinning assembly

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US20110311671A1 (en) 2008-10-17 2011-12-22 Tong Lin Electrostatic spinning assembly

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