KR101703162B1 - A Batch Reactor for Improving Mixing Capability - Google Patents

A Batch Reactor for Improving Mixing Capability Download PDF

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KR101703162B1
KR101703162B1 KR1020140048271A KR20140048271A KR101703162B1 KR 101703162 B1 KR101703162 B1 KR 101703162B1 KR 1020140048271 A KR1020140048271 A KR 1020140048271A KR 20140048271 A KR20140048271 A KR 20140048271A KR 101703162 B1 KR101703162 B1 KR 101703162B1
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reactor
baffle
batch reactor
present
batch
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KR20150121978A (en
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예원경
홍유식
송영수
임예훈
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주식회사 엘지화학
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00029—Batch processes

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  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

본 발명은 반응기 내의 하부에 설치되어 반응기 내부의 반응액을 교반시키는 교반기; 및 반응기 내의 벽면을 따라서 나선형을 이루며 설치된 배플(Baffle);을 포함하는 회분식(Batch) 반응기에 관한 것이다.The present invention relates to a process for producing a polymer electrolyte membrane, comprising: a stirrer provided at a lower portion of a reactor for stirring a reaction solution inside a reactor; And a baffle provided in a spiral shape along the wall surface in the reactor.

Description

혼합 능력이 개선된 회분식 반응기{A Batch Reactor for Improving Mixing Capability}[0001] The present invention relates to a batch reactor having improved mixing ability,

본 발명은 혼합 능력이 개선된 회분식 반응기에 관한 것이다.The present invention relates to a batch reactor with improved mixing capability.

회분식 반응기는 배치형 반응기(Batch Reactor)로도 불리며, 소규모 운전이나 새로운 공정의 시험, 고가의 생성물 제조 및 연속 공정으로 전화하기 어려운 공정들에 대하여 사용되고 있다.Batch reactors are also referred to as batch reactors and are used for processes that are difficult to call by small operation or testing of new processes, production of expensive products and continuous processes.

이러한 회분식 반응기는 교반을 통하여 반응물들을 혼합하는데, 원심력 등에 의하여 반응기의 내부와 외부의 혼합이 어렵다는 문제가 있다.Such a batch reactor mixes the reactants through stirring, and there is a problem that it is difficult to mix the inside and the outside of the reactor by centrifugal force or the like.

이러한 문제점을 해결하기 위하여, 종래에는 배플(Baffle)을 반응기의 벽면과 수직인 방향으로 판형 형태로 설치하여, Vortex형성을 완화하고, 내부 혼합 증대를 꾀하였으나, 혼합능력의 개선이 미미하다는 문제점이 있었다.In order to solve such a problem, conventionally, a baffle is provided in a plate shape in a direction perpendicular to the wall surface of the reactor to alleviate the formation of the vortex and to increase the internal mixing. However, there was.

이에, 회분식 반응기의 내부에 설치되는 배플을 이용하여 종래 기술의 배플에 비하여 반응액의 내부 혼합능력이 더욱 개선된 새로운 회분식 반응기에 대한 연구가 필요한 실정이다.
Therefore, it is necessary to study a new batch reactor in which the internal mixing ability of the reaction liquid is further improved as compared with the baffles of the prior art by using the baffles installed inside the batch reactor.

US 4276262US 4276262

상기와 같은 종래기술의 문제점을 해결하고자, In order to solve the above problems of the prior art,

본 발명은 회분식 반응기의 내부에 설치되는 배플을 이용하여 반응액의 혼합능력이 더욱 개선된 새로운 회분식 반응기를 제공하는 것을 목적으로 한다.
The present invention aims to provide a new batch reactor in which the mixing ability of a reaction solution is further improved by using a baffle installed inside the batch reactor.

상기의 목적을 달성하기 위하여, In order to achieve the above object,

본 발명은 반응기 내의 하부에 설치되어 반응기 내부의 반응액을 교반시키는 교반기; 및 반응기 내의 벽면을 따라서 나선형을 이루며 설치된 배플(Baffle);을 포함하는 회분식(Batch) 반응기를 제공한다.
The present invention relates to a process for producing a polymer electrolyte membrane, comprising: a stirrer provided at a lower portion of a reactor for stirring a reaction solution inside a reactor; And a baffle provided in a spiral shape along a wall surface in the reactor.

본 발명의 회분식(Batch) 반응기에 따르면, According to the batch reactor of the present invention,

회분식 반응기의 내부에 설치되는 배플이 반응기 내의 벽면을 따라서 일정한 각도의 나선형을 이루며 설치되기 때문에 반응액의 혼합능력이 더욱 개선되어 반응기 내의 물질의 혼합시간을 40% 이상 단축할 수 있다는 장점이 있다.
Since the baffle provided inside the batch reactor is installed in a spiral shape at a certain angle along the wall surface in the reactor, the mixing ability of the reaction solution is further improved, and the mixing time of the substances in the reactor can be shortened by 40% or more.

도 1은 본 발명의 회분식 반응기를 나타낸 그림이다.
도 2는 본 발명의 회분식 반응기의 피치와 직경의 관계를 나타낸 그림이다.
도 3은 본 발명의 회분식 반응기의 상부에서 본 평면도이다.
도 4는 본 발명의 회분식 반응기의 측면에서 본 측면도이다.
도 5는 본 발명의 실시예와 비교예의 회분식 반응기에 따른 혼합 능력의 차이를 나타낸 그래프이다.1 is a view showing the batch reactor of the present invention.
FIG. 2 is a view showing the relationship between the pitch and the diameter of the batch reactor of the present invention. FIG.
3 is a top plan view of the batch reactor of the present invention.
Figure 4 is a side view from the side of the batch reactor of the present invention.
FIG. 5 is a graph showing the difference in mixing ability according to the batch reactor of the embodiment of the present invention and the comparative example.

이하 본 발명의 회분식(Batch) 반응기에 대하여 상세하게 설명한다.
Hereinafter, the batch reactor of the present invention will be described in detail.

본 발명은 도 1과 같이, 반응기 내의 하부에 설치되어 반응기 내부의 반응액을 교반하는 교반기; 및 반응기 내의 벽면을 따라서 나선형을 이루며 설치된 배플(Baffle)을 포함하는 회분식(Batch) 반응기를 제공한다. 종래의 기술에서는 배플(Baffle)이 반응기의 벽면과 수직인 방향으로 판형 형태로 존재했으나, 본 발명의 회분식 반응기는 도 1에서와 같이, 배플이 반응기 내의 벽면을 따라서 나선형을 이루며 설치되어 있기 때문에, 교반기에 의하여 반응액을 교반 시킬 때, 반응액이 나선형의 배플을 따라 상승 또는 하강하기 때문에, 그 혼합능력을 개선할 수 있다.
As shown in FIG. 1, the present invention relates to an apparatus for separating and purifying a reaction mixture, comprising: a stirrer provided at a lower portion of the reactor for stirring a reaction solution inside the reactor; And a baffle provided in a spiral shape along a wall surface in the reactor. In the prior art, the baffle was present in a plate shape in a direction perpendicular to the wall surface of the reactor. However, since the baffle of the present invention is installed in a spiral shape along the wall surface in the reactor as in Fig. 1, When the reaction liquid is stirred by the stirrer, the reaction liquid is raised or lowered along the spiral baffle, so that the mixing ability can be improved.

본 발명의 회분식(Batch) 반응기에 있어서, 상기 배플은 일정한 각도의 나선형을 이루며 설치될 수 있다. 또한, 상기 배플은 도 2에서와 같이 배플간의 거리 및 반응기의 직경을 정의하는 경우, 배플간의 거리(pitch)가 반응기의 직경 대비 1/2 내지 3/4를 만족할 때, 그 혼합능력이 더욱 개선될 수 있다.
In the batch reactor of the present invention, the baffle can be installed in a spiral shape at a certain angle. Further, when the baffle defines the distance between the baffles and the diameter of the reactor as in Fig. 2, when the pitch between the baffles satisfies 1/2 to 3/4 of the diameter of the reactor, .

본 발명의 회분식(Batch) 반응기에 있어서, 상기 교반기는 반응기 내의 하부에 설치되어 반응기 내부의 반응액을 교반하는 것으로, 회분식 반응기에 일반적으로 사용되는 것이라면 특별한 제한은 없으나, 임펠러(Impeller)를 사용하는 것이 바람직하다.
In the batch reactor of the present invention, the stirrer is installed at a lower portion of the reactor to stir the reaction solution inside the reactor. The stirrer is not particularly limited as long as it is generally used in a batch reactor, but an impeller .

본 발명의 회분식(Batch) 반응기에 있어서, 상기 배플은 반응기 내의 벽면을 따라서 일정한 각도의 나선형을 이루며 설치된다. 상기 일정한 각도란 반응기 내의 벽면의 수평에 대하여 배플이 이루고 있는 각도를 말하며, 사용자의 의도에 따라서 다양하게 조절될 수 있다.
In the batch reactor of the present invention, the baffle is installed in a spiral shape at an angle along the wall surface in the reactor. The constant angle refers to the angle formed by the baffle with respect to the horizontal plane of the wall in the reactor, and can be variously adjusted according to the user's intention.

본 발명의 회분식(Batch) 반응기에 있어서, 상기 반응기는 특별한 제한이 있는 것은 아니나, 바람직하게는 원형일 수 있다. 반응기가 원형인 경우, 반응기 내의 벽면의 수평에 대하여 배플이 이루고 있는 각도가 일정하게 될 수 있으며, 반응기 내의 전체 반응액의 혼합능력이 더욱 개선될 수 있다.
In the batch reactor of the present invention, the reactor is not particularly limited, but may be preferably circular. When the reactor is circular, the angle formed by the baffle with respect to the horizontal plane of the wall in the reactor can be made constant, and the mixing ability of the entire reaction liquid in the reactor can be further improved.

본 발명의 회분식(Batch) 반응기에 있어서, 상기 배플의 너비는 도 3에서와 같이 나타낼 수 있으며, 상기 배플의 너비는 사용자의 의도에 따라서 다양하게 조절될 수 있으나, 바람직하게는 반응기 직경의 1/8 내지 1/6인 것을 사용할 수 있다.
In the batch reactor of the present invention, the width of the baffle may be as shown in FIG. 3, and the width of the baffle may be variously adjusted according to the user's intention, 8 to 1/6 can be used.

본 발명의 회분식(Batch) 반응기에 있어서, 상기 배플은 도 4에서와 같이, 반응기 내의 벽면을 따라서 나선형으로 회전을 하여 이루어지는데, 상기 배플의 회전수는 사용자의 의도에 따라서 다양하게 조절될 수 있다.
In the batch reactor of the present invention, as shown in FIG. 4, the baffle is spirally rotated along the wall surface in the reactor, and the number of revolutions of the baffle can be variously adjusted according to a user's intention .

이하 본 발명의 이해를 돕기 위하여 바람직한 실시예를 제시하나, 하기 실시예는 본 발명을 예시하는 것일 뿐 본 발명의 범주 및 기술사상 범위 내에서 다양한 변경 및 수정이 가능함은 당업자에게 있어서 명백한 것이며, 이러한 변경 및 수정이 첨부된 특허청구범위에 속하는 것도 당연한 것이다.
It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the scope and spirit of the invention as disclosed in the accompanying claims. Changes and modifications may fall within the scope of the appended claims.

실시예Example

[실시예 1] [Example 1]

반경이 1.8m 이고, 높이가 4.5m 인 회분식 반응기의 내부에 배플을 나선형으로 설치하였다. 상기 배플의 너비는 0.5m이고, Pitch는 2.66m이었다.A baffle was spirally installed inside a batch reactor having a radius of 1.8 m and a height of 4.5 m. The width of the baffle was 0.5 m and the pitch was 2.66 m.

상기 회분식 반응기 내에 반응액으로 물을 넣은 후, 반응기 내의 임팰러를 작동시켜 혼합하였다. After the reaction liquid was poured into the batch reactor, the impeller in the reactor was operated to mix.

[비교예 1] [Comparative Example 1]

반경이 1.8m 이고, 높이가 4.5m 인 회분식 반응기의 내부에 배플을 반응기의 벽면과 수직인 방향으로 판형 형태로 설치하였다. 상기 배플의 너비는 0.5m 이었다.A baffle was installed in a plate shape in the direction perpendicular to the wall surface of the reactor in a batch reactor having a radius of 1.8 m and a height of 4.5 m. The width of the baffle was 0.5 m.

상기 회분식 반응기 내에 반응액으로 물을 넣은 후, 반응기 내의 임팰러를 작동시켜 혼합하였다.
After the reaction liquid was poured into the batch reactor, the impeller in the reactor was operated to mix.

실험예Experimental Example

상기 실시예 및 비교예의 반응기 내의 온도를 측정하여, 혼합시간에 따른 CoV(Coefficient of Variation)의 값을 측정하여, 그 값이 0.01에 도달한 시점을 비교하여 도 5에 나타내었다.
The temperature in the reactors of the Examples and Comparative Examples was measured, and the value of CoV (Coefficient of Variation) according to the mixing time was measured. When the value of CoV reached 0.01, the results are shown in FIG.

도 5에 나타난 바와 같이, 본 발명의 회분식 반응기를 사용하는 경우, CoV 값이 0.01에 도달하는 시간이 약 8초로서, 종래의 회분식 반응기를 사용하는 경우의 13초에 비하여, 40% 이상 빨라지는 것을 알 수 있었다. As shown in FIG. 5, when the batch reactor of the present invention is used, the time required for the CoV value to reach 0.01 is about 8 seconds, which is 40% faster than that of the conventional batch reactor using 13 seconds .

따라서, 본 발명의 실시예에 따른 회분식 반응기에 의하면 반응액의 혼합 시간을 현저하게 줄일 수 있다는 것을 확인할 수 있었다.
Therefore, it was confirmed that the batch time of the reaction solution can be remarkably reduced by the batch reactor according to the embodiment of the present invention.

Claims (6)

반응기 내의 하부에 설치되어 반응기 내부의 반응액을 교반시키는 교반기; 및
반응기 내의 벽면을 따라서 일정한 각도의 나선형을 이루며 설치된 배플(Baffle);을 포함하고,
상기 배플은 배플간의 거리(pitch)가 직경 대비 1/2 내지 3/4로 이루어진 것이고,
상기 배플의 너비는 반응기 반경의 1/8 내지 1/6인 것을 특징으로 하는 회분식(Batch) 반응기.A stirrer installed at a lower portion of the reactor to stir the reaction solution inside the reactor; And
And a baffle provided at a predetermined angle in a spiral shape along a wall surface in the reactor,
The baffle has a pitch of 1/2 to 3/4 of the diameter of the baffles,
Wherein the width of the baffle is 1/8 to 1/6 the radius of the reactor. 삭제delete 삭제delete 청구항 1에 있어서,
상기 교반기는 임펠러(Impeller)인 것을 특징으로 하는 회분식(Batch) 반응기.The method according to claim 1,
Wherein the agitator is an impeller. 청구항 1에 있어서,
상기 반응기는 원형인 것을 특징으로 하는 회분식(Batch) 반응기.The method according to claim 1,
Wherein the reactor is circular. 삭제delete
KR1020140048271A 2014-04-22 2014-04-22 A Batch Reactor for Improving Mixing Capability KR101703162B1 (en)

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KR101195892B1 (en) 2011-06-07 2012-10-30 경상대학교산학협력단 Mixing containers with baffles parallel to the primary rotational flow and an agitator using the same

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KR101195892B1 (en) 2011-06-07 2012-10-30 경상대학교산학협력단 Mixing containers with baffles parallel to the primary rotational flow and an agitator using the same

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