KR101515239B1 - Heat treatment apparatus for oxidation of carbon fiber with protective shielding means - Google Patents

Heat treatment apparatus for oxidation of carbon fiber with protective shielding means Download PDF

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KR101515239B1
KR101515239B1 KR1020090135000A KR20090135000A KR101515239B1 KR 101515239 B1 KR101515239 B1 KR 101515239B1 KR 1020090135000 A KR1020090135000 A KR 1020090135000A KR 20090135000 A KR20090135000 A KR 20090135000A KR 101515239 B1 KR101515239 B1 KR 101515239B1
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heat treatment
treatment chamber
carbon fiber
shielding means
hot air
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KR20110078243A (en
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성문규
방윤혁
김성룡
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주식회사 효성
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/32Apparatus therefor
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • D01D10/02Heat treatment
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/07Addition of substances to the spinning solution or to the melt for making fire- or flame-proof filaments
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/20Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
    • D01F9/21Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F9/22Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B9/00Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity
    • F27B9/28Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity for treating continuous lengths of work
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2101/00Inorganic fibres
    • D10B2101/10Inorganic fibres based on non-oxides other than metals
    • D10B2101/12Carbon; Pitch
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/04Heat-responsive characteristics
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Electrochemistry (AREA)
  • Inorganic Fibers (AREA)

Abstract

본 발명은 열풍공급수단, 상기 열풍공급수단에 의하여 상측에서 수직열풍이 유입되어 프리커서 섬유를 산화하는 열처리실 및 상기 프리커서 섬유를 상기 열처리실에 유입 또는 유출하는 폴딩롤러를 포함하는 탄소섬유용 산화 열처리장치에 있어서, 각각의 폴딩롤러에 의하여 프리커서 섬유가 열처리실로 유입 또는 유출되는 열처리실 측벽 외부에 보호차폐수단을 구비함으로써 열처리실 내부에 공정문제가 발생할 경우 상기 보호차폐수단을 통하여 열처리실 내부로 접근 또는 관찰가능한 것을 특징으로 하는 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치를 제공한다. The present invention relates to a method for producing a carbon fiber including a hot air supply means, a heat treatment chamber for introducing vertical hot air from above by the hot air supply means to oxidize precursor fibers, and a folding roller for introducing or discharging the precursor fibers into the heat treatment chamber In the oxidation heat treatment apparatus, since protective curtain means is provided outside the side wall of the heat treatment chamber where the precursor fibers flow into or out of the heat treatment chamber by the respective folding rollers, if a process problem occurs in the heat treatment chamber, The present invention provides an oxidation heat treatment apparatus for a carbon fiber having a protection shielding means which is accessible or observable inside.

본 발명에 의하면, 조업에 지장이 없으며 현장상황을 바로 체크할 수 있으므로 조업자를 폭주반응에 의한 화재로부터 보호할 수 있으며, 조업을 원할하게 할 수 있다는 장점이 있다. According to the present invention, there is no impediment to the operation and the situation can be checked immediately, so that the operator can be protected from the fire caused by the runaway reaction, and the operation can be made easy.

탄소섬유, 산화 열처리장치, 보호차폐, Carbon fiber, oxidation heat treatment device, protective shield,

Description

보호차폐수단을 구비한 탄소섬유용 산화 열처리장치{Heat treatment apparatus for oxidation of carbon fiber with protective shielding means}TECHNICAL FIELD [0001] The present invention relates to a heat treatment apparatus for oxidation of carbon fiber,

본 발명은 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치에 관한 것으로서, 더욱 상세하게는 각각의 폴딩롤러에 의하여 프리커서 섬유가 열처리실로 유입 또는 유출되는 출입구에 보호차폐수단을 구비함으로써 열처리실 내부로 접근 또는 관찰가능하여 폭주반응시 조업자의 안전을 보호할 수 있는 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치에 관한 것이다.The present invention relates to an oxidizing heat treatment apparatus for carbon fiber having a protective shielding means, and more particularly, to an oxidation heat treatment apparatus for carbon fiber having protective shielding means, The present invention relates to an oxidation heat treatment apparatus for a carbon fiber having a protection shielding means capable of protecting the safety of an operator during a runaway reaction.

아크릴로니트릴(acrylonitrile)계 중합체로부터 제조되는 탄소섬유, 소위 PAN(Polyacrylonitrile)계 탄소섬유는 강도가 매우 우수하여, 탄소섬유의 원료로서 많이 사용되고 있다. 최근에는 전체 탄소섬유의 90%이상이 PAN계 탄소섬유이다. 또한, PAN계 탄소섬유는 2차전지용 탄소 전극 재료 및 탄소 필름 등에도 적용가능성이 있기 때문에, 이에 대한 연구개발도 활발하게 진행되고 있다. BACKGROUND ART Carbon fibers, so-called PAN (polyacrylonitrile) -based carbon fibers, produced from acrylonitrile-based polymers are very strong and widely used as raw materials for carbon fibers. More recently, more than 90% of the total carbon fibers are PAN-based carbon fibers. In addition, since PAN-based carbon fibers are also applicable to carbon electrode materials for secondary batteries and carbon films, research and development thereof have also been actively conducted.

아크릴로니트릴계 중합체로부터 탄소섬유를 제조하는 경우에는 아크릴로니트 릴계 중합체를 방사하여 얻어진 아크릴 섬유, 즉 탄소섬유용 전구체를 산화 분위기에서 200~400℃로 내염화 처리를 실시하는데, 이렇게 제조된 섬유를 내염화섬유라고 한다. 이렇게 얻어진 내염화섬유를 불활성가스 분위기에서 800~2000℃로 탄화처리하여 탄소섬유를 제조한다. 또한, 이렇게 얻어진 탄소섬유를 더욱 고온의 불활성가스 중에서 처리하는 경우도 있는데, 이렇게 얻어진 섬유를 흑연섬유라고 한다.In the case of producing a carbon fiber from an acrylonitrile-based polymer, acrylic fiber obtained by spinning an acrylonitrile-based polymer, that is, a precursor for a carbon fiber is subjected to chlorination treatment at 200 to 400 ° C in an oxidizing atmosphere. Is called chlorinated fiber. The chlorinated fibers thus obtained are carbonized at 800 to 2000 占 폚 in an inert gas atmosphere to produce carbon fibers. The carbon fiber thus obtained may be treated in an inert gas at a higher temperature. The thus obtained fiber is referred to as graphite fiber.

상기 내염화섬유를 얻기 위한 산화공정은 화학반응이 진행되는 과정에서 그 반응을 제어하기 어려운 폭주반응이 일어날 가능성이 높아 폭주반응에 대응하는 기술이 중요하게 인식되고 있다. 특히 폭주반응이 일어나면 화재가 발생할 가능성이 높고 그에 따른 인명피해가 발생할 가능성이 있으므로 신속한 억제가 필요하다.The oxidation process for obtaining the chlorinated fibers has a high possibility of a congestion reaction which is difficult to control the reaction during the progress of the chemical reaction, and therefore, a technology corresponding to the congestion reaction has been recognized as important. Especially, when a runaway reaction occurs, there is a high possibility that a fire is likely to occur, and there is a possibility of causing personal injury, so rapid restraint is needed.

그러나 폭주반응을 억제하기 위한 대책으로 소화설비의 설치정도가 전부이다. 지금까지 폭주반응은 제어할 수 없기 때문에 열처리온도와 공정속도를 낮추어 폭주반응이 발생하기 않게 조절하여 왔지만 생산성 향상을 위해 공정속도를 높임에 따라 폭주반응이 일어나기 쉬운 공정조건에서 작업을 하게 되고, 이에 따라 화재로 이어지기 쉽게 되어 조업자의 안전을 위한 설비가 요구되고 있는 실정이다. However, as a countermeasure to suppress the runaway reaction, the degree of installation of fire extinguishing facilities is all. Since the congestion reaction can not be controlled until now, the heat treatment temperature and the process speed have been lowered to control the runoff reaction. However, in order to improve the productivity, the process speed is increased and the work is carried out under process conditions where runaway reaction is likely to occur. Accordingly, it is easy to lead to a fire, and facilities for the safety of the operator are required.

본 발명은 상기와 같은 문제점을 해결하기 위하여 안출된 것으로서, 각각의 폴딩롤러에 의하여 프리커서 섬유가 열처리실로 유입 또는 유출되는 출입구에 보호차폐수단을 구비함으로써 열처리실 내부로 접근 또는 관찰가능하여 폭주반응시 조업자의 안전을 보호할 수 있는 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치를 제공함에 그 목적이 있다.SUMMARY OF THE INVENTION The present invention has been conceived to solve the problems described above, and it is an object of the present invention to provide a protective shielding means at an entrance where inlet and outlet of precursor fibers flow into or out of a heat treatment chamber by respective folding rollers, And an object of the present invention is to provide an oxidation heat treatment apparatus for carbon fibers having protective shielding means capable of protecting the safety of a pilot operator.

상술한 바와 같은 목적을 구현하기 위한 본 발명의 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치는 열풍공급수단, 상기 열풍공급수단에 의하여 상측에서 수직열풍이 유입되어 프리커서 섬유를 산화하는 열처리실 및 상기 프리커서 섬유를 상기 열처리실에 유입 또는 유출하는 폴딩롤러를 포함하는 탄소섬유용 산화 열처리장치에 있어서, 각각의 폴딩롤러에 의하여 프리커서 섬유가 열처리실로 유입 또는 유출되는 열처리실 측벽 외부에 보호차폐수단을 구비함으로써 열처리실 내부에 공정문제가 발생할 경우 상기 보호차폐수단을 통하여 열처리실 내부로 접근 또는 관찰가능한 것을 특징으로 한다. In order to accomplish the above object, according to the present invention, there is provided an oxidizing heat treatment apparatus for carbon fiber having a protective shielding means, comprising a hot air supply means, a heat treatment chamber for oxidizing precursor fibers, And a folding roller for introducing or discharging the precursor fibers into or out of the heat treatment chamber, wherein the precursor fibers are introduced into or out of the heat treatment chamber by the respective folding rollers, The shielding means is provided so as to be able to approach or observe the inside of the heat treatment chamber through the protective shielding means when a process problem occurs in the heat treatment chamber.

또는 상기 보호차폐수단의 재질은 내열성의 투명한 내열강화유리인 것을 특징으로 한다. Or the material of the protective shielding means is heat-resistant transparent heat-resistant tempered glass.

또는 상기 보호차폐수단은 여닫이 문, 미닫이 문, 여닫이 창 및 미닫이 창 중 어느 하나의 형태로 이루어진 것을 특징으로 한다.Alternatively, the protective shielding means may be formed in any one of a hinged door, a sliding door, a casement window, and a sliding window.

본 발명에 따른 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치에 의하면, 각각의 폴딩롤러에 의하여 프리커서 섬유가 열처리실로 유입 또는 유출되는 출입구에 보호차폐수단을 구비하여 조업에 지장이 없으며 현장상황을 바로 체크할 수 있으므로 조업자를 폭주반응에 의한 화재로부터 보호할 수 있으며, 조업을 원할하게 할 수 있다는 장점이 있다. According to the oxidation heat treatment apparatus for carbon fiber having the protective shielding means according to the present invention, it is possible to provide a protective shielding means at the entrance where the precursor fibers enter or exit the heat treatment chamber by the respective folding rollers, It is possible to protect the operator from the fire caused by the runaway reaction, and it is advantageous that the operation can be made easy.

이하 첨부한 도면을 참조하여 본 발명의 바람직한 실시예에 대한 구성 및 작용을 상세히 설명하면 다음과 같다. 여기서, 종래와 동일한 구성요소에 대해서는 동일한 도면부호를 사용하기로 한다.DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings. Here, the same reference numerals are used for the same constituent elements as those in the prior art.

도 1은 본 발명에 따른 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치의 구성도이다. 1 is a configuration diagram of an oxidation heat treatment apparatus for carbon fibers having a protective shielding unit according to the present invention.

도 1에서 보는 바와 같이, 산화 열처리장치(100)는 열처리실(60) 내부에는 다수개의 패스를 형성하여 프리커서 섬유(10)가 주행하고 있으며, 상기 프리커서 섬유(10)는 열처리실(60) 외부에 설치된 소정 세트의 폴딩롤러(20)에 의해 폴딩되 어 측벽(50)에 형성된 다수개의 슬릿(30)을 통하여 열처리실(60)에 반복 공급된다. 1, in the oxidation heat treatment apparatus 100, precursor fibers 10 are formed by forming a plurality of passes in a heat treatment chamber 60, and the precursor fibers 10 are passed through a heat treatment chamber 60 Is folded by a predetermined set of folding rollers 20 installed outside and is repeatedly supplied to the heat treatment chamber 60 through a plurality of slits 30 formed in the side wall 50. [

여기서 상기 프리커서 섬유(10)를 산화열처리하기 위한 열풍발생공급수단(도시하지는 않음)은 열처리실 외부에 설치되는 히터에 의하여 발생된 열풍이 상방열풍유로를 따라 상기 열처리실(60) 상측으로부터 상부통기판을 통하여 열처리실(60) 내부로 유입되어 하부통기판을 통하여 배출되며 배출된 열풍은 하방열풍유로를 따라 히터로 순환된다. 산화열처리 장치에서의 열풍발생공급수단은 해당기술의 통상의 지식을 갖는 자에게는 자명한 사항이므로 자세한 설명은 생략한다.Here, hot air generating and supplying means (not shown) for oxidizing and annealing the precursor fibers 10 is constructed such that hot air generated by a heater provided outside the heat treatment chamber flows from the upper side of the heat treatment chamber 60 to the upper side The heated air flows into the heat treatment chamber (60) through the tubular substrate, is discharged through the lower tubular substrate, and the discharged hot air is circulated to the heater along the downward hot air flow path. The hot air generating and supplying means in the oxidation heat treatment apparatus is obvious to those having ordinary skill in the art, so a detailed description thereof will be omitted.

열처리실(60)의 측벽(50)에는 프리커서 섬유(10)가 열처리실 내부로 유입하는 통로인 다수의 슬릿(30)이 형성되어 있으며, 상기 측벽(50) 외부에는 상기 프리커서 섬유(10)를 폴딩하여 구동력을 전달하는 다수개의 폴딩롤러(20)가 구비되어 있다. A plurality of slits 30 are formed in the sidewall 50 of the heat treatment chamber 60 as a passage through which the precursor fibers 10 flow into the heat treatment chamber. And a plurality of folding rollers 20 for folding and transmitting the driving force.

보호차폐수단(40a,40b)은 각각의 폴딩롤러(20)에 의하여 프리커서 섬유(10)가 열처리실(60)로 유입 또는 유출되는 출입구 즉 열처리실 측벽(50) 외부에 구비된다. 상기 보호차폐수단(40a,40b)은 조업에 지장이 없으며, 열처리실 내부상황을 바로 접근 및 관찰할 수 있으며 조업자를 폭주반응에 의한 화재로부터 보호하는 기능을 한다. The protective shielding means 40a and 40b are provided at the entrance or outside of the heat treatment chamber side wall 50 through which the precursor fibers 10 are introduced into or out of the heat treatment chamber 60 by the respective folding rollers 20. The protection shielding means (40a, 40b) are free from any obstacles to operation, and can easily access and observe the inside of the heat treatment chamber and protect the operator from fire caused by the runaway reaction.

따라서 상기 보호차폐수단(40a,40b)은 열처리실 내부상황을 바로 접근 및 관찰할 수 있도록 내열성의 투명한 재질인 내열강화유리를 사용함이 바람직하다. 또한 사절등의 공정문제가 발생하였을 경우 문 또는 창을 열고 작업하고, 평소에는 문 또는 창을 닫고 공정을 관찰할 수 있도록 여닫이 문, 미닫이 문, 여닫이 창 및 미닫이 창 중 어느 하나의 형태로 이루어짐이 바람직하다. Therefore, it is preferable that the protective shielding means 40a and 40b use a heat-resistant tempered glass which is a heat resistant transparent material so that the inside of the heat treatment chamber can be immediately accessed and observed. In addition, if a process problem such as embroidering occurs, the door or window is opened and operated. Normally, the door or window is closed so that the process can be observed. The door is a door, a sliding door, a casement window and a sliding window. desirable.

본 발명은 상기 실시예에 한정되지 않고 본 발명의 기술적 요지를 벗어나지 아니하는 범위 내에서 다양하게 수정·변형되어 실시될 수 있음은 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에 있어서 자명한 것이다.It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit and scope of the invention will be.

도 1은 본 발명에 따른 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치의 구성도이다. 1 is a configuration diagram of an oxidation heat treatment apparatus for carbon fibers having a protective shielding unit according to the present invention.

<도면의 주요 부분에 대한 부호의 설명>Description of the Related Art

10:프리커서 섬유 20:폴딩롤러10: precursor fiber 20: folding roller

30:슬릿 40a,40b:보호차폐수단30: slit 40a, 40b: protective shielding means

50:측벽 60:열처리실50: side wall 60: heat treatment chamber

100:산화 열처리장치100: Oxidation heat treatment apparatus

Claims (3)

열풍공급수단, 상기 열풍공급수단에 의하여 상측에서 수직열풍이 유입되어 프리커서 섬유를 산화하는 열처리실 및 상기 프리커서 섬유를 상기 열처리실에 유입 또는 유출하는 폴딩롤러를 포함하는 탄소섬유용 산화 열처리 장치에 있어서, And a folding roller for introducing or discharging the precursor fibers into or out of the heat treatment chamber, wherein the hot air supply means comprises: a heat treatment chamber for introducing vertical hot air from the upper side by the hot air supply means to oxidize precursor fibers, In this case, 각각의 폴딩롤러에 의하여 프리커서 섬유가 열처리실로 유입 또는 유출되는 열처리실 측벽 외부에 열처리실 내부상황에 따라 접근 및 관찰이 가능하고, 내열성의 투명한 내열강화유리로 된 보호차폐수단을 구비한 것을 특징으로 하는 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치.A protective shielding means made of heat-resistant transparent heat-resistant tempered glass capable of approaching and observing outside the side wall of the heat treatment chamber through which the precursor fibers flow into or out of the heat treatment chamber by the respective folding rollers, And a protective shielding means for protecting the carbon fiber. 삭제delete 제 1항에 있어서,The method according to claim 1, 상기 보호차폐수단은 여닫이 문, 미닫이 문, 여닫이 창 및 미닫이 창 중 어느 하나의 형태로 이루어진 것을 특징으로 하는 보호차폐수단을 구비한 탄소섬유용 산화 열처리장치.Wherein the protection shielding means is formed in any one of a hinged door, a sliding door, a casement window, and a sliding window.
KR1020090135000A 2009-12-30 2009-12-30 Heat treatment apparatus for oxidation of carbon fiber with protective shielding means KR101515239B1 (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004124310A (en) 2002-10-03 2004-04-22 Toray Ind Inc Flameproofing furnace
JP2007217835A (en) * 2006-02-17 2007-08-30 Toho Tenax Co Ltd Flameproofing treatment oven
JP2008138325A (en) 2006-12-04 2008-06-19 Toray Ind Inc Flame resistant furnace and method for producing flame resistant fiber bundle, and method for producing carbon fiber bundle
JP2008231610A (en) 2007-03-20 2008-10-02 Mitsubishi Rayon Co Ltd Flame-resistance treatment oven and flame resistance treatment method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004124310A (en) 2002-10-03 2004-04-22 Toray Ind Inc Flameproofing furnace
JP2007217835A (en) * 2006-02-17 2007-08-30 Toho Tenax Co Ltd Flameproofing treatment oven
JP2008138325A (en) 2006-12-04 2008-06-19 Toray Ind Inc Flame resistant furnace and method for producing flame resistant fiber bundle, and method for producing carbon fiber bundle
JP2008231610A (en) 2007-03-20 2008-10-02 Mitsubishi Rayon Co Ltd Flame-resistance treatment oven and flame resistance treatment method

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