KR101434873B1 - Preparation method of Cudrania Tricupspidate Bureau extract using seawater and Cudrania Tricupspidate Bureau extract thereby - Google Patents

Abstract

The present invention relates to a method for producing cucurbitan extract using deep sea water and a method for preparing the cucurbitan extract, which comprises a first step of blending deep seawater and cucurbitaceous material into a deep sea water, And a third step of adding the sweetener to the fermented material to ferment and aging the fermented material, and a third step of adding the fermented aged raw material and the desalted deep sea water to the extractor and extracting the extract from the extractor. The present invention provides a method for preparing a cucumber extract using deep sea water and a cucumber extract prepared thereby. Thus, the functional ingredients of the deep sea water are further reinforced to the active ingredient of the cucumber japon by producing the cucumber extract using the deep sea water, thereby providing the cucurbitan extract having improved functionality.

Description

Preparation method of Cucumis japonica extract using deep seawater and preparation of Cucumis japonica extract using seawater and Cudrania tricupspidate Bureau extract thereby,

The present invention relates to a process for producing cucurbitan extract using deep sea water and a method for preparing the cucurbit species extract, wherein the functional ingredients of the deep seawater are supplemented to the active ingredient of cucurbit The present invention also relates to a method for producing cucurbitan extract using deep sea water having improved functionality and a cucumber extract thereof.

Generally, Cucumisporon is a native native to Korea. It can be used for various purposes such as roots, stems and leaves. Stems and roots can be used as medicines or leaves and fruits as food.

It is well known that cucurbitan has a high anticancer effect, and it is known to be effective for relieving hangover, diabetes and hypertension. Therefore, there have been a lot of studies to apply these effective ingredients to various industrial fields in recent years.

Particularly, most of the active ingredients of cucurbitan are added to foods. In case of using red pepper paste or soybean paste, we can use water, or add cucumber extract to beverages or alcoholic beverages, or to prevent obesity, antioxidant, Research in various fields is active.

One of these techniques is the Korean Patent Registration No. 0975754, which is prepared by boiling soybeans in an extract that extracts the twigs and leaves of cedarwood wood, and making distilled liquor by using cucumber powder and red pepper or blue pepper Which is mixed with meju and aged for aging to prepare soybean paste doenjang.

On the other hand, deep seawater in the sea is located in a deep seafloor with depth of 200m or more, which does not reach sunlight, so there are few organic matter and pathogens, and it maintains a low temperature stable throughout the year. It is rich in various nutrients essential for the growth of marine plants, Is a useful seawater resource.

In other words, deep ocean water is a useful marine resource with characteristics such as low temperature water, cleanliness, stability, eutrophication, and aging, and research on industrialization using it has been actively conducted in the USA and Japan from early on, Research is being actively conducted to utilize deep seawater in various industrial fields.

Korean Patent Application No. 2006-0056135 discloses a technology using this deep sea water. This is a method in which plants such as vegetables, wild plants, and fruits are fermented and aged using mineral components extracted from brown sugar and deep seawater so that plant extracts containing a large amount of mineral components The pH of the solution is adjusted to 3 to 4 by the addition of an organic acid, fermentation is performed at 32 to 38 ° C for 7 to 10 days, and the filtrate separated from the solid matter is subjected to high-pressure constant- And sterilization treatment to produce plant extracts.

As described above, in the prior art, since cucumispolon is simply used in purified water and the like, water is not properly extracted from the active ingredients of cucurbitan and there is a lack of minerals.

Accordingly, the present invention provides a method for preparing a coconut water extract using deep sea water, which comprises extracting a large amount of active ingredients of coconut water using mineral-rich deep sea water and further increasing the efficacy of coconut water and including minerals, .

In order to accomplish the above object, the present invention provides a method for producing a marine deodorized water, comprising the steps of: mixing marine deep seawater and coconut water; And a third step of putting fermented aged cobbing material and desalted deep seawater into an extractor and extracting a cryoprotectant extract from the extractor. The method for producing cocoon extract of the deep sea water according to claim 1, As a technical point.

In addition, it is preferable to use raw water as the deep seawater of the first step.

It is preferable that the first-step curing material is cut for 1 hour to 6 hours or less, and it is preferable to use one or more of the fruits, leaves, stem, and roots mixed and washed.

Meanwhile, after the first step, it is preferable that the water is sprayed on the cicophyll material that has been dipped in the deep seawater, followed by drying and crushing, and the crushed cobblin material is added to the tumbler to perform the tumbling operation. Is in the range of 14 to 20 degrees, and the amount of the alcohol to be sprayed is preferably 0.3 to 0.5 parts by weight per 100 parts by weight of the raw material.

In the second step, it is preferable to mix 10 to 200 parts by weight of a sweetener with respect to 100 parts by weight of the raw material, and fermentation is aged for 30 days or more. The sweetener may be selected from sugar, honey, syrup, rice syrup and malt syrup It is preferable to use one or two or more of them in combination.

In the third step, the desalted deep sea water preferably has a hardness of 100 to 300.

The desalted deep seawater is preferably added to the extractor in an amount of 100 to 2000 parts by weight based on 100 parts by weight of the fermented raw material in the third step.

In addition, in the third step, extraction is carried out at 30 ° C to 50 ° C for 12 hours to 36 hours while maintaining the vacuum state, and the fermented aged deep-sea water mixture and the demineralized deep-sea water mixture are boiled, .

As a result, the functional ingredients of the deep sea water are further reinforced to the active ingredients of cucurbitan so that the cucurbit flavor extract using the deep sea water having improved functionality can be manufactured.

In the present invention, the process of blending raw materials with deep seawater is to remove the effective ingredient of the raw material from the deep seawater into the deep seawater and to remove the characteristic bitterness and unique toxicity in the raw material itself, , And has the effect of neutralizing.

Thus, when the extract containing the active ingredient of Cjizipon is obtained by using the rich deep sea water, its functionality is further added, and the efficacy of the cilippon is further increased.

FIG. 1 is a flow chart of a method for producing an extract of Curcuma longa by using deep sea water according to the present invention.

The present invention relates to a method for preparing a cucumber extract using deep sea water and a method for producing the cucumber extract. The extract of Cucumis japonica is prepared by using deep sea water, The functional ingredients in the deep seawater are reinforced, thereby making it possible to produce a coconut extract having improved functionality.

Hereinafter, the present invention will be described in detail with reference to the accompanying drawings. FIG. 1 is a flowchart illustrating a method for preparing an extract of Ciliaceae using deep sea water according to the present invention.

As shown in the figure, the present invention provides a method for producing a fermented matured seaweed, comprising the following steps: a first step of blending deep sea water and coconut water into a raw material, a second step of adding a sweetener to the coconut- And a third step of adding the deodorized material and the deionized deep sea water to the extractor and extracting the extract from the extractor.

The deep seawater according to the present invention preferably uses raw water, and it is used in deep seawater taken at about 300 to 1300 m, specifically about 500 to 1100 m from the east coast, the west coast or the south coast of Korea, Specific examples thereof include deep pool water (605m) or wterbis (1032m) of Gangwon, and inorganic compounds having anticancer activity such as selenium (Se) and zinc as well as sodium, calcium, magnesium and potash, Ions and other minerals.

Such deep seawater can be desalinated through a desalting treatment process well known in the art. Specifically, the deep seawater can be subjected to a desalting treatment process using a cationic or an anionic ion exchange resin, It is possible to carry out desalination through a process such as desalting by carrying out an electrolysis process for decomposing the sodium chloride component through a two-tank electrolytic device or desalting by a membrane filtration process.

Meanwhile, the raw material according to the present invention can be used by mixing any one or two or more of fruits, leaves, stems, and roots, and the leaves, stems, and roots of the roots can be collected to peel off the roots, It is dried and prepared, and the fruit is cleaned and dried.

The first step is to use the deep-sea water for 1 hour to 6 hours. When the above-mentioned deep seawater is pickled, if it does not last for 1 hour, the pickle will not be completely pickled. If it is longer than 6 hours, the salt will be excessively seeped into the pickle.

In the process of blending cocoon ingredients and deep seawater, the effective ingredients of the cocoon ingredients are extracted into the deep seawater by deep seawater, and the peculiar bitterness and unique toxicity of the cocoon ingredients are removed, It will act to neutralize.

It is preferable that the alcohol be sprayed to the deep seawater soaked in the deep sea water, dried and crushed, and the crushed coconut material is put into a tumbling machine to further perform a tumbling operation. , And the amount of the squeeze sprayed to 100 parts by weight of the raw material is preferably 0.3 to 0.5 parts by weight.

Here, after spraying alcohol on the shredded raw material, the inner temperature of the tumbler rotates at a low speed of 40 to 50 rpm at a temperature of 70 ° C to 100 ° C, and when the intrinsic flavor of the material starts to evaporate, the tumbler The inner temperature of the tumbler is sealed so that it does not exceed 120 ℃ ~ 200 ℃ and it is rotated at a high speed of 200 ~ 250rpm to perform the tumbling operation. Sprayed wine can be used for fermentation such as sake or distillate such as shochu have.

This is a process to maximize the nutrients and flavor of the noodles and to obtain the extracts with the flavor of the coodinates kept at the maximum.

In the second step, the sweetener is added to the deep-sea water so that the sweet potato is fermented and aged. The sweet potato is mixed with 10 to 200 parts by weight of 100 parts by weight of the raw material, I will. Specifically, the raw materials and the sweetener are mixed at a weight ratio of about 1: 2 and fermented for more than 100 days. More specifically, the raw materials and sweeteners can be mixed at a weight ratio of about 1: 1 and fermented for 100 to 300 days.

Examples of the sweetening agent include, but are not limited to, sugar, honey, starch syrup, rice syrup and malt syrup.

Next, as the third step of the present invention, the fermentation-aged raw material and the desalted deep sea water are put into an extractor, and the extract is extracted from the extractor.

The hardness of the desalted deep sea water is preferably 100 to 300, and the hardness indicates the degree of mineral dissolved in the water. The higher the value, the more the mineral is contained.

Specifically, hardness means the content (ppm) of Ca ions and Mg ions converted to calcium carbonate in ppm, and Ca (ppm) x2.5 + Mg (ppm) x4.1 = US hardness (ppm).

In addition, in the present invention, the fermentation-aged raw material and the de-ionized deep sea water used in the extractor are used in an amount of 100 to 2000 parts by weight per 100 parts by weight of desalted deep seawater. Specifically, 100 to 1000 parts by weight of desalted deep seawater based on 100 parts by weight of the raw material, more specifically 200 to 1,000 parts by weight with respect to 100 parts by weight of the raw material, more specifically, 500 To 1000 parts by weight, more particularly about 1000 parts by weight of deep sea water per 100 parts by weight of the raw material.

In addition, in the third step, the extract may be extracted at 30 to 50 ° C for 12 to 36 hours, or may be extracted for 18 to 30 hours. In the vacuum state, the fermented aged seaweed material and the desalted deep sea water The mixture may be boiled to perform the distillation and concentration processes simultaneously.

The thus-prepared cucurbitan extract can be formulated into a liquid, a gel, a pill or a granule according to the purpose of use.

Hereinafter, a method for manufacturing the bean sprouts according to the present invention will be described in detail.

≪ Example 1 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water. Then, the above-prepared cornflakes and sugar were mixed in a weight ratio of 1: 1, the lid was sealed, and the fermentation was aged for 100 days in a shaded place where the air was well ventilated. 10% by weight of deionized deep sea water having a hardness of 100 and fermentation aging for 100 days was added to the extractor, and the extractor was extracted at 30 ° C to 50 ° C for 3 hours and then transferred to a concentrator. The extract was extracted. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

≪ Example 2 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the salt and foreign matter were removed, and the cured jongpobong was harvested for 3 hours in a barrel filled with deep sea water. Then, the above-prepared cornflakes and sugar were mixed in a weight ratio of 1: 1, and the lid was sealed, followed by fermentation for 200 days in a shaded place with good air circulation. Then, 200 g of fermented aged deep-seated deep-seated deep-seated deep-sea water with a hardness of 100 was added to the extractor at a ratio of 1 wt%: 10 wt%, the extractor was extracted at 30 ° C to 50 ° C for 3 hours, Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

≪ Example 3 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water. Then, the above-prepared cornflakes and sugar were mixed in a weight ratio of 1: 1, the lid was sealed, and the fermentation was aged for 300 days in a shaded place where air was well-flowed. Then, 300 g of fermented aged cornflakes and 100 deep desalted deep sea water were added to the extractor at a ratio of 1 wt%: 10 wt%, and the extractor was extracted at 30 ° C to 50 ° C for 3 hours and then transferred to a concentrator Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

<Example 4>

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water. Then, 1: 1 weight ratio of bamboo shoots and sugar was mixed, and the lid was sealed, followed by 100 days of fermentation in a shaded place with good air circulation. Then, 100% of fermented aged deep-seated deep-seated deep-seated water and 200 mature desalted deep seawater were added to the extractor at a ratio of 1 wt%: 10 wt%, and the extractor was extracted at 30 ° C to 50 ° C for 3 hours and then transferred to a concentrator Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

&Lt; Example 5 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water. Then, 1: 1 by weight of sugar was mixed with the above-prepared cucumber, and the lid was sealed, followed by fermentation for 200 days in a shaded place with good air circulation. Then, 200 g of fermented aged cornflakes and 200 deep desalted deep seawater were added to the extractor at a ratio of 1 wt%: 10 wt%, and the extractor was extracted at 30 ° C to 50 ° C for 3 hours and then transferred to a concentrator Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

&Lt; Example 6 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water. Then, the above-prepared cornflakes and sugar were mixed at a ratio of 1: 1 by weight, respectively, and the lid was sealed. Then, the fermentation was aged for 300 days in a shaded place with good air circulation. Then, 300 g of fermented aged cornflakes and 200 deep desalted deep seawater were added to the extractor at a ratio of 1 wt%: 10 wt%, and the extractor was extracted at 30 ° C to 50 ° C for 3 hours and then transferred to a concentrator Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

&Lt; Example 7 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). In addition, we removed the bitter taste of the cucumber which had been removed from the stones and foreign matter by cutting it for 3 hours. Then, the above-prepared cornflakes and sugar were mixed in a weight ratio of 1: 1, and the lid was sealed, followed by fermentation for 100 days in a shaded place with good air circulation. Then, 100% of fermented aged corn deep-fried and deep-seated deep sea water having a hardness of 300 was added to the extractor at a ratio of 1 wt%: 10 wt%, the extractor was extracted at 30 ° C to 50 ° C for 3 hours, Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

&Lt; Example 8 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water. Then, the above-prepared cornflakes and sugar were mixed in a weight ratio of 1: 1, and the lid was sealed, followed by fermentation for 100 days in a shaded place with good air circulation. Then, 100% of the deep-seaweed deionized water having a hardness of 100 and fermented for 100 days was added to the extractor at a ratio of 1 wt%: 10 wt% and the extractor was heated at 85 ° C for 24 hours to extract the extract. Then, the extract of Curcuma longa extract extracted from the extractor was introduced into a concentrator, and the concentrate was heated at 100 ° C. for 12 to 24 hours to extract a gel-like extract of Cucurbitaceae. Thereafter, the gel-form condiment concentrate extracted from the concentrator was cooled and sterilized, and the sterilized gel-form concentrate was packed in a wrapping paper.

&Lt; Example 9 >

First, we picked the cucumber from the Goseong area of Gangwon province, and removed the stones and foreign matter by putting the collected cucumber in the seaweed (not in the city). Then, the cured jugulpon which had been removed from the stones and the foreign matter was cut for 3 hours in a barrel filled with deep sea water.

0.4 parts by weight of sake, which was 0.4 parts by weight of alcohol, and 14 parts by weight of alcohol was sprayed to 100 parts by weight of the above-prepared coconut oil, dried, crushed and put into a kneading machine.

When the internal temperature of the kneader is 80 ° C, the kneading operation is performed at a low speed of 40-50 rpm. When the inherent flavor of the kneaded material begins to vaporize, the kneading machine is sealed, And rotated at a speed of 250 rpm at a high speed.

Then, the above-prepared cucumber and sugar were mixed in a weight ratio of 1: 1, the lid was sealed, and then fermented for 300 days in a shaded place with good air circulation. Then, 300 g of fermented aged cornflakes and 100 deep desalted deep sea water were added to the extractor at a ratio of 1 wt%: 10 wt%, and the extractor was extracted at 30 ° C to 50 ° C for 3 hours and then transferred to a concentrator Extracts were extracted from. Then, the extract of Cjuripong extracted from the extractor was cooled and sterilized, and the sterilized cugypolum extract was packed in a wrapping paper.

<Experimental Example 1. Sensory Test>

(Hereinafter referred to as &quot; Comparative Example &quot;) prepared by using a conventional method without using deep sea water and stored at a refrigeration temperature for 24 hours, The sensory evaluation was carried out on 20 sensory test workers and the results of Examples 1, 2, 3 and 4 are shown in Table 1 below. The sensory test items were evaluated for taste, flavor and overall acceptability. The score was recorded by the testee using the 5-point scale method and the mean value of the scores was recorded.

5: Very good

4: Good

3: Usually

2: It is not good to be bad

1: Very bad

flavor incense Likelihood Comparative Example 2.0 3.8 2.3 Example 1 4.2 4.2 4.3 Example 2 4.3 4.5 4.4 Example 3 4.4 4.7 4.6 Example 4 4.5 4.6 4.7 Example 5 4.3 4.5 4.5

As a result of extracting the common cranberry extract and the functional cranberry extract using the deep sea water of the present invention, the functional cranberry extract of the present invention obtained a high sensory score in taste and flavor. Tastes and aromas were superior to the comparative examples, especially due to the antioxidant components contained in the deep ocean water and the optimized process conditions of the present invention. As a result, the functional extract of Coleoptera using the deep sea water of the present invention was superior to the Comparative Example in overall acceptability.

&Lt; Preparation Example 1: Production of liquid &

- 10 mg of CJP extract, 10,000 mg of isomerization, 5,000 mg of mannitol,

Dissolving the above components in purified water according to a usual liquid preparation method, adding an appropriate fragrance, filling the bottle and sterilizing it.

&Lt; Preparation Example 2: Preparation of granules &

- Cucumber extract 10mg, soybean extract 50mg, glucose 200mg, starch 500mg

After mixing the above components, 100 mL of 30% ethanol is added and the mixture is dried at 60 ° C to form granules, which are filled in a capsule to prepare granules.

&Lt; Preparation Example 3: Preparation of pellets >

- Cucumber extract 20mg, lactose 1,500mg, glycerin 1,500mg, starch 980mg

After mixing the above components, the mixture is prepared to be 4 g per one ring according to a conventional method for producing a pellet.

The present invention relates to a method for producing a cucumber extract using deep sea water and a method for producing the cucumber extract. The present invention is applicable to a fusion type production industry combined with a local agricultural product, cucumber, utilizing deep sea water.

Claims (12)

A first step of blending the deep seawater and the coconut material into a raw material;
A second step of adding a sweetener into the deep-sea water to make a fermented material;
And a third step of introducing the fermented aged raw materials and the desalted deep seawater into an extractor and extracting the extract from the extract of Coleoptera japonica extract. The method according to claim 1, wherein the deep seawater in the first stage is raw water. The method according to claim 1, wherein the first step of ripening is performed for 1 hour to 6 hours. The method according to claim 1, wherein the first-
A method for preparing a coconut water extract using deep-sea deep-sea water, characterized in that one or two or more of coconut fruit, leaf, stem, and root are mixed and washed. 2. The method of claim 1, further comprising, after the first step,
The method of the present invention is characterized by spraying alcohol with a degree of alcohol of 14 to 20 degrees to a cobbled material in the deep seawater, drying and crushing the crushed material, &Lt; / RTI &gt; [Claim 6] The method according to claim 5, wherein the alcohol content of the alcohol is 14 to 20 degrees and the amount of the alcohol to be sprayed is 100 to 0.3 part by weight. 2. The method according to claim 1,
Wherein the sweetener is mixed in an amount of 10 to 200 parts by weight with respect to 100 parts by weight of the raw material, and fermentation is aged for 30 to 300 days. 2. The method according to claim 1, wherein, in the second step,
Wherein the sweetener is a mixture of one or more of sugar, honey, syrup, rice syrup and malt syrup. 2. The method according to claim 1, wherein in the third step,
Wherein the desalted deep sea water has a hardness of 100 to 300. 6. The method of claim 1, The method according to claim 1, wherein the desalted deep seawater is added to the extractor in an amount of 100 to 2000 parts by weight per 100 parts by weight of the fermented raw material in the third step. The method according to claim 1, wherein in the third step, the extraction is performed at 30 to 50 ° C for 12 to 36 hours during the extraction, wherein the vacuum state is maintained to boil the fermented aged and deionized deep sea water mixture, Wherein the concentrate is simultaneously subjected to a concentration process. 11. A cranberry extract which is produced by the method of any one of claims 1 to 11.

Images