KR100910764B1 - Surface-coating material for the car - Google Patents

Surface-coating material for the car Download PDF

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KR100910764B1
KR100910764B1 KR1020080105780A KR20080105780A KR100910764B1 KR 100910764 B1 KR100910764 B1 KR 100910764B1 KR 1020080105780 A KR1020080105780 A KR 1020080105780A KR 20080105780 A KR20080105780 A KR 20080105780A KR 100910764 B1 KR100910764 B1 KR 100910764B1
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coating
vehicle
liquid
present
weight
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KR20090013145A (en
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박향률
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박향률
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/14—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to metal, e.g. car bodies
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Catalysts (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

본 발명은 액상의 유기규소(Si) 40~70중량%, 산소반응촉매제 5~8.75중량%, 농도조절제 21.25~55중량%로 이루어진 차량 표면의 유리피막 코팅제를 제공하기 위한 것으로, 본 발명은 코팅성분(Si)이 고상(미세분말)이 아닌 액상으로 존재하므로 도포방식에 의한 코팅작업이 유용한 효과를 갖는 것이며, 코팅제를 액상(液狀)으로 도포함으로써 코팅제의 균일한 도포가 가능하게 되고, 반복코팅작업이 가능할 뿐만 아니라 숙련자가 아니더라도 코팅작업이 가능하게 되어 노동력과 작업시간, 작업비용을 절감시킬 수 있는 효과를 갖으며, 또한 본 발명은 액상으로 도포된 코팅제가 차량 피막 표면에 부착되면서 산소와 반응하여 유리막(실리카, 무기규소)을 형성함으로 차체 손상방지 및 오염방지, 세정, 장기간 광택효과 등을 기대할 수 있는 매우 유용한 발명인 것이다.The present invention is to provide a glass coating coating on the surface of the vehicle consisting of 40 to 70% by weight of the organic silicon (Si), 5 to 8.75% by weight of the oxygen reaction catalyst, 21.25 to 55% by weight of the concentration regulator, the present invention is a coating Since the component (Si) is present in the liquid phase rather than in the solid phase (fine powder), the coating method has a useful effect, and uniform coating of the coating agent is possible by applying the coating liquid in a liquid. Not only the coating work is possible but also the skilled workers can make the coating work, which has the effect of reducing labor, working time, and work cost. In addition, the present invention is a liquid coating agent is applied to the surface of the vehicle film and oxygen and It is a very useful invention that can anticipate damage to the body and prevent pollution, cleaning, long-term gloss effect by forming glass films (silica, inorganic silicon) by reaction. .

차량, 표면, 코팅제, 유리막 Vehicle, Surface, Coating, Glass Film

Description

차량 표면의 유리피막 코팅제{SURFACE-COATING MATERIAL FOR THE CAR}Glass coating on vehicle surface {SURFACE-COATING MATERIAL FOR THE CAR}

본 발명은 차량 표면의 유리피막 코팅제에 관한 것으로, 더욱 상세하게는 도색된 차량의 도장면을 보호하기 위한 코팅제를 차량의 도장면 표면에 도포할 수 있도록 하되 코팅제를 액상(液狀)으로 도포함으로써 코팅제의 균일한 도포는 물론 코팅작업의 편리함과 신속함을 도모할 수 있는 차량 도장면의 유리피막 코팅제에 관한 것이다.The present invention relates to a glass coating coating on a vehicle surface, and more particularly, by coating a coating agent for protecting the painted surface of the painted vehicle on the painted surface of the vehicle, but by applying the coating in a liquid state The present invention relates to a glass coating coating on the surface of a vehicle that can be uniformly applied as well as the convenience and speed of the coating operation.

일반적으로 소비자들은 차량의 도장면이 외부 오염물질(산성비나 화학적 스모그 등)에 의해 부식되는 것을 방지하고, 윤기있는 광택 및 색상을 갖도록 하며, 먼지나 이물질들이 달라 붙기 힘든 표면을 장기간 유지시켜 차량의 도장면을 보호하기 위해 다양한 종류의 차량용 왁스나 코팅제 등을 사용하고 있다.In general, consumers can prevent the painted surface from being corroded by external contaminants (such as acid rain or chemical smog), have a glossy luster and color, and maintain the surface of the vehicle for a long time to prevent dirt or foreign substances from sticking to it. To protect the painted surface, various types of vehicle waxes and coatings are used.

이에 따라 종래에는 10~100 나노크기로 분쇄된 실리카(SiO2; 무기규소) 2중량%와, 바인더 물질(결합물질) 98중량%로 구성된 고상(固相)의 코팅제를 사용하여 차량의 피막 표면을 코팅하고 있는 실정이다.Accordingly, the film surface of the vehicle is conventionally formed by using a solid coating composed of 2% by weight of silica (SiO 2 ; inorganic silicon) crushed to 10 to 100 nano-sizes and 98% by weight of a binder material (bonding material). It is a situation that the coating.

즉 미세한 분말상태의 실리카(SiO2)가 바인더에 의해 차량의 피막 표면에 코팅상태를 유지하게 되고, 결국 실리카(SiO2)에 의해 차량의 피막 표면이 오염물질(산성비나 화학적 스모그 등)에 의해 부식되는 것을 방지함과 동시에 광택을 장시간 유지하도록 하고 있다.That is, fine powder silica (SiO 2 ) is maintained on the coating surface of the vehicle by the binder, and eventually the surface of the vehicle coating by the silica (SiO 2 ) is caused by contaminants (acid ratio or chemical smog). It prevents corrosion and maintains gloss for a long time.

그러나 상기한 종래의 코팅제는 고체, 즉 분말상태인 실리카(SiO2)를 바인더 물질에 혼합하여 액상으로 제조되어 차량의 도장면에 도포되어질 때 유리막(SiO2) 성분의 농도가 높아질수록 기술적으로 작업성이 어려워져 현재 5% 이내가 현실입니다.However, the above-mentioned conventional coating agent is manufactured in a liquid state by mixing a solid, that is, powdered silica (SiO 2 ) with a binder material, and technically works as the concentration of the glass film (SiO 2 ) component increases when applied to the painted surface of the vehicle. As sex becomes more difficult, it is now less than 5%.

따라서 코팅제를 차량의 피막 표면에 코팅가능하게 하기 위해서는 유리막(SiO2)의 농도가 2% 정도이며, 농도가 낮은 관계로 3~5회 정도 반복시공을 해야 효과적이며, 이때 작업시에도 바인더 물질이 건조되면서 고형(미세분말)물질 등이 묻어나와 오히려 차량 피막에 스크래치를 만들기도 하며, 또 코팅제에 혼합된 유리막(SiO2)성분의 농도가 낮아 얇은 피막으로 차량 도장면의 보호효과나 얻고자 하는 상이한 목적에 부합하다는 것이다.Therefore, in order to be able to coat the coating on the surface of the vehicle, the concentration of glass film (SiO 2 ) is about 2%, and the concentration is low, so it needs to be repeated 3 ~ 5 times and it is effective. As it dries, solid (fine powder) substances are smeared on the surface, which makes scratches on the vehicle's film. Also, since the concentration of glass (SiO 2 ) component mixed with the coating is low, the thin film is used to protect the surface of the vehicle. It serves a different purpose.

또한 작업자의 수작업에 의해 코팅작업이 이루어짐으로써 균일한 코팅이 곤란하고, 숙련도를 필요로 할 뿐만 아니라, 작업이 힘들고 작업시간이 오래 걸려 작업자들이 작업을 기피하는 단점을 갖는 것이다. In addition, since the coating work is performed by the worker's manual work, it is difficult to uniformly coat the coating and require skill, but also has a disadvantage in that the worker avoids the work because the work is difficult and the work takes a long time.

따라서 본 발명은 상기와 같은 문제점을 해결하기 위해 안출된 것으로, 본 발명은 코팅성분을 액상(液狀)으로 도포할 수 있도록 하되 차량의 피막 표면에는 실리카(SiO2)가 형성될 수 있도록 함을 특징으로 한다.Therefore, the present invention has been made to solve the above problems, the present invention is to be able to apply the coating component in a liquid (液狀), but the silica (SiO 2 ) to be formed on the film surface of the vehicle It features.

이를 위해 본 발명은 종래의 방식인 고형의 미세분말 형태의 유리피막(SiO2) 성분이 아닌 액상의 유기규소(Si)를 차량의 피막 표면에 도포하되 상기 액상의 유기규소(Si)가 차량의 피막 표면에 도포되는 순간 공기 중의 산소와 반응하여 고형화, 즉 실리카(SiO2)가 될 수 있도록 상기 액상의 유기규소에 산소반응촉매를 혼합하여 도포함을 특징으로 한다.To this end, the present invention is a liquid organic silicon (Si) is applied to the surface of the vehicle film, not a solid glass powder (SiO 2 ) component of the conventional method, but the liquid organic silicon (Si) of the vehicle Molecular oxygen is reacted with oxygen in the air at the time of coating on the surface of the coating, that is, it is characterized by mixing the oxygen reaction catalyst in the liquid organosilicon so as to be silica (SiO 2 ).

이처럼 본 발명은 코팅성분(Si)이 고상(미세분말)이 아닌 액상으로 존재하므로 도포방식에 의한 코팅작업이 가능한 효과를 갖는 것이며, 코팅제를 액상(液狀)으로 도포함으로써 코팅제의 균일한 도포가 가능하게 되고, 반복코팅작업이 가능할 뿐만 아니라 숙련자가 아니더라도 코팅작업이 가능하게 되어 노동력과 작업시간, 작업비용을 절감시킬 수 있는 효과를 갖는다.As such, the present invention has the effect of coating by the coating method because the coating component (Si) is present in the liquid phase, not in the solid phase (fine powder), and uniform coating of the coating agent is achieved by applying the coating agent in the liquid phase. It becomes possible, and it is possible to repeat coating work as well as coating work is possible even if you are not skilled, it has the effect of reducing labor, work time, work cost.

또한 본 발명은 액상으로 도포된 코팅제가 차량 피막 표면에 부착되면서 산소와 반응하여 유리막(실리카)을 형성함으로 차체 손상방지 및 오염방지, 세정, 장기간 광택효과 등을 기대할 수 있는 매우 유용한 발명인 것이다.In addition, the present invention is a very useful invention that can be expected to prevent damage to the vehicle body and prevent contamination, cleaning, long-term gloss effect by forming a glass film (silica) by reacting with oxygen as the coating agent is applied to the liquid film surface of the vehicle film.

상기한 효과를 달성하기 위한 본 발명을 바람직한 실시예를 통해서 상세히 설명하면 다음과 같다.When explaining the present invention in detail through the preferred embodiment for achieving the above effects are as follows.

본 발명은 크게 액상의 유기규소(Si)와 산소반응촉매제, 농도조절제로 이루어지되, 상기 액상의 유기규소(Si)의 첨가량은 전체 중량%중 40~70중량%를 차지하며, 산소반응촉매제는 5 ~ 8.75중량%, 농도조절제로는 21.25~55중량%로 이루어짐이 바람직하다. The present invention largely consists of a liquid organosilicon (Si), an oxygen reaction catalyst, a concentration regulator, the amount of the organic silicon (Si) of the liquid addition accounts for 40 to 70% by weight of the total weight, the oxygen reaction catalyst 5 to 8.75% by weight, the concentration adjusting agent is preferably made of 21.25 to 55% by weight.

상기 액상의 규소와 산소반응촉매제의 가장 바람직한 혼합비는 중량비로 8:1이다. 이는 상기 산소반응촉매제의 양이 중량비로 1보다 미만인 경우에는 고형화 반응이 더디게 이루어지게 되고, 또는 1 이상인 경우에는 고형화 반응이 너무 빨리 이루어져 차량표면에 코팅막(유리막)을 형성하기 곤란하기 때문이다.The most preferable mixing ratio of the liquid silicon and the oxygen reaction catalyst is 8: 1 by weight. This is because when the amount of the oxygen reaction catalyst is less than 1 in weight ratio, the solidification reaction is slow, or when it is 1 or more, the solidification reaction is made so quickly that it is difficult to form a coating film (glass film) on the vehicle surface.

이때 상기 산소반응촉매제는 여러가지 성분이 존재할 수 있으나, 본 발명에서는 지르코늄(Zr) 또는 주석이 사용되었으며, 물론 상기 지르코늄(Zr)과 주석 같이 액상의 유기규소와 함께 함유되어 액상의 유기규소가 차량 피막 표면에 부착되 었을 때 산소와 반응시켜 실리카(SiO2)를 형성할 수 있다면 어떤 성분을 사용하더라도 무방할 것이다.In this case, the oxygen reaction catalyst may have various components, but in the present invention, zirconium (Zr) or tin was used, and of course, the zirconium (Zr) and tin are contained together with the liquid organic silicon such that the liquid organic silicon is a vehicle coating. Any component can be used as long as it can react with oxygen to form silica (SiO 2 ) when attached to the surface.

또한 농도조절제 역시 여러가지 성분을 사용할 수 있으나, 본 발명에서는 백등유(탄화수소)를 사용하였다. 상기 농도조절제 역시 액상의 유기규소가 산소와 반응하여 실리카(SiO2)를 형성하는데 문제되지만 않는다면 어떤 성분을 사용하더라도 무방하다.In addition, the concentration regulator may also use a variety of components, in the present invention, white kerosene (hydrocarbon) was used. The concentration regulator may also be used as long as the organic silicon in the liquid is not a problem to react with oxygen to form silica (SiO 2 ).

본 발명에서 사용되는 유기규소(Si)는 액상(液狀)이며, 본 발명에 있어서 실질적으로 코팅막(유리막)을 형성하는 물질이다. The organosilicon (Si) used in the present invention is a liquid phase, and is a substance which substantially forms a coating film (glass film) in the present invention.

상기 액상의 유기규소(Si)는 수세파쇄(水洗破碎)한 규석을 숯 또는 코크스로 전기로에서 환원시켜 제조한 규소 분말과, 증류 정제한 사염화규소를 고순도(高純度)의 아연으로 고온에서 환원시키는 뒤퐁법에 의해서 99.97% 정도의 순도로 제조한 규소 분말과, 대용융법(帶溶融法)이라 하는 정제법에 의해서 텐－나인의 순도(99.99999999%)를 갖도록 제도된 규소 분말에 메틸클로라이드(Methyl chloride)를 이용하여 통상적으로 순수한 액상의 유기규소(Si)를 추출하는 제법을 사용하도록 한다.The liquid organosilicon (Si) is a silicon powder produced by reducing the crushed silica (water) broken in a charcoal or coke with an electric furnace, and distilled purified silicon tetrachloride at high temperature (zinc) to reduce the zinc at high temperature Methyl chloride (Methyl) was prepared in silicon powder prepared by the DuPont method with a purity of about 99.97%, and silicon powder prepared to have ten-nine purity (99.99999999%) by a purification method called a high melting method. chloride) is used to extract the pure liquid organosilicon (Si).

즉 상기 액상의 유기규소(Si)는 규소 분말에 메틸클로라이드(염화메틸)를 반응시켜 아래와 같이 클로로실란(ChloroSilane) 혼합물로 제조하여 사용되는 것이다.That is, the liquid organosilicon (Si) is used to prepare a chlorosilane (ChloroSilane) mixture as shown below by reacting silicon chloride (methyl chloride) to the silicon powder.

Si(규소 분말) + 2CH3CL(염화메틸) → CH3 SiCL3, (CH3)2 SiCL2, (CH3)3 SiCL, SiCL4(사염화규소)Si (silicon powder) + 2CH 3 CL (methyl chloride) → CH 3 SiCL 3 , (CH 3 ) 2 SiCL 2 , (CH 3 ) 3 SiCL, SiCL 4 (silicon tetrachloride)

이때 상기 액상의 유기규소(Si)는 실온에 존재하는 공기 중의 산소와 축합반응하여 이산화규소(SiO2)를 산화는데, 본 발명에서는 차량의 도장면에 균일하게 도포한 상태에서 산소와 반응하여 고형화(유리화 또는 무기화)되어 진다.At this time, the liquid organic silicon (Si) is condensed with oxygen in the air present at room temperature to oxidize silicon dioxide (SiO 2 ), in the present invention is solidified by reacting with oxygen in a uniform coating state on the painted surface of the vehicle (Vitrified or inorganic).

이때 상기 고형화 반응을 촉진시키기 위해서 산소반응촉매제가 필요하게 되는데, 이러한 산소반응촉매제로는 지르코늄(Zr) 또는 주석이 사용되며, 상기 지르코늄(Zr) 또는 주석은 다양한 성분을 대상으로 오랫동안 실험한 결과 가장 바람직한 실험결과를 얻었기 때문이다.At this time, an oxygen reaction catalyst is required to promote the solidification reaction, and zirconium (Zr) or tin is used as the oxygen reaction catalyst, and the zirconium (Zr) or tin is the most preferable as a result of long experiments with various components. This is because the experimental results were obtained.

본 발명에서는 액상의 유기규소(Si)와 산소반응촉매제의 혼합중량%가 45중량% 이하인 경우에는 백등유의 중량%가 55중량%를 초과하게 되고, 따라서 차량표면에 코팅막을 형성하기 위한 규소성분이 너무 적게 함유되므로써 차량표면에 액상으로 존재하는 시간이 길어지게 되고, 이로 인해 규소가 고형화되기 전에 먼지나 이물질 등의 오염물질이 차량 피복의 표면에 부착되는 단점을 갖는다.In the present invention, when the mixed weight percent of the liquid organosilicon (Si) and the oxygen reaction catalyst is 45 wt% or less, the wt% of the white kerosene exceeds 55 wt%, and thus the silicon component for forming the coating film on the surface of the vehicle By containing too little, the time that the liquid phase is present on the surface of the vehicle becomes long, and this has the disadvantage that contaminants such as dust or foreign matter adhere to the surface of the vehicle coating before the silicon solidifies.

또 상기 액상의 규소(Si)와 산소반응촉매제의 혼합중량%가 78.75중량%를 초과한 경우에는 백등유의 중량%가 21.55중량% 미만이 되어 상기 백등유의 용제 역할을 기대하기 어렵고, 또 규소 성분이 너무 많이 함유되므로써 필요 이상으로 차량표면에 두꺼운 코팅막을 형성하는 문제점을 야기하게 되고 비용이 높아지는 단점을 갖게 된다. 따라서 본 발명에선 액상의 규소(Si)와 산소반응촉매제가 8:1의 질량비로 혼합된 45~78.75중량%에 대해 백등유는 21.25~55중량%로 이루어지는 것이 가장 바람직하다.In addition, when the mixed weight% of the liquid silicon (Si) and the oxygen reaction catalyst exceeds 78.75 wt%, the wt% of the white kerosene becomes less than 21.55 wt%, and it is difficult to expect the role of the solvent of the white kerosene. Too much content causes a problem of forming a thick coating film on the surface of the vehicle more than necessary, and has a disadvantage of high cost. Therefore, in the present invention, it is most preferable that the white kerosene is 21.25 to 55% by weight relative to 45 to 78.75% by weight of the liquid silicon (Si) and the oxygen reaction catalyst in a mass ratio of 8: 1.

이처럼 상기한 구성을 갖는 본 발명 차량 표면의 유리피막 코팅제는 일정량 함유된 액상의 유기규소와, 상기 액상의 유기규소를 공기 중의 산소와 반응시켜 차량 피복 표면에 고형화(유리화 또는 무기화)시키기 위한 산소반응촉매제와, 농도조절제로 사용되는 백등유로 이루어짐으로써 도포에 의한 코팅작업이 가능하고, 반복코팅이 가능하며, 숙련자가 아니더라도 쉽게 작업할 수 있으며, 신속하고 저렴한 코팅작업이 가능한 차량 피복 표면 코팅제를 제공할 수 있는 것이다.As described above, the glass coating agent on the surface of the vehicle having the above-described structure reacts with an organic silicon in a certain amount and liquid oxygen, and an oxygen reaction for solidifying (vitrifying or inorganicizing) the surface of the vehicle by reacting the liquid organic silicon with oxygen in the air. It consists of a catalyst and white kerosene used as a concentration regulator, which enables coating by coating, repetitive coating, easy operation even if not skilled, and can provide a vehicle coating surface coating that can be quickly and cheaply coated. It can be.

상기한 바와 같이 본 발명이 비록 한정된 실시예에 의해 설명되었으나, 본 발명은 이것에 의해 한정되지 않으며 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에 의해 본 발명의 기술사상과 아래에 기재될 특허청구범위의 균등범위 내에서 다양한 수정 및 변형이 가능하다 할 것이다.Although the present invention has been described by way of limited embodiments as described above, the present invention is not limited thereto and will be described below by the person skilled in the art and the technical spirit of the present invention. Various modifications and variations are possible within the scope of the claims.

Claims (3)

액상의 유기규소(Si) 화합물 40~70중량%, 지르코늄(Zr) 또는 주석 중 어느 하나를 선택적으로 사용하는 산소반응촉매제 5~8.75중량%, 농도조절제로 백등유 21.25~55중량%로 이루어짐을 특징으로 하는 차량 표면의 유리피막 코팅제.40 to 70% by weight of a liquid organosilicon (Si) compound, 5 to 8.75% by weight of an oxygen reaction catalyst using any one of zirconium (Zr) or tin, and 21.25 to 55% by weight of kerosene as a concentration regulator A glass film coating agent on the surface of a vehicle. 삭제delete 삭제delete
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR950002332B1 (en) * 1986-12-24 1995-03-16 필킹톤 피 엘 씨 Method of coating on glass
JPH1060374A (en) 1996-08-20 1998-03-03 Asahi Breweries Ltd Coating agent composition for glass container and glass container coated therewith
KR100198724B1 (en) 1995-06-14 1999-06-15 모리시따 요오이찌 Finishing agents and method using the same
US20060228566A1 (en) 2005-04-07 2006-10-12 Luten Henry A Hydrophobic coatings and methods

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR950002332B1 (en) * 1986-12-24 1995-03-16 필킹톤 피 엘 씨 Method of coating on glass
KR100198724B1 (en) 1995-06-14 1999-06-15 모리시따 요오이찌 Finishing agents and method using the same
JPH1060374A (en) 1996-08-20 1998-03-03 Asahi Breweries Ltd Coating agent composition for glass container and glass container coated therewith
US20060228566A1 (en) 2005-04-07 2006-10-12 Luten Henry A Hydrophobic coatings and methods

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