KR100858663B1 - The device of manufacturing the bio-diesel with waste edible-oil - Google Patents
The device of manufacturing the bio-diesel with waste edible-oil Download PDFInfo
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- KR100858663B1 KR100858663B1 KR1020080012753A KR20080012753A KR100858663B1 KR 100858663 B1 KR100858663 B1 KR 100858663B1 KR 1020080012753 A KR1020080012753 A KR 1020080012753A KR 20080012753 A KR20080012753 A KR 20080012753A KR 100858663 B1 KR100858663 B1 KR 100858663B1
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
- C10G3/42—Catalytic treatment
- C10G3/44—Catalytic treatment characterised by the catalyst used
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/32—Liquid carbonaceous fuels consisting of coal-oil suspensions or aqueous emulsions or oil emulsions
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
- C10L2290/24—Mixing, stirring of fuel components
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
- C10L2290/52—Hoppers
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
- C10L2290/58—Control or regulation of the fuel preparation of upgrading process
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
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- Oil, Petroleum & Natural Gas (AREA)
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- Liquid Carbonaceous Fuels (AREA)
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Abstract
Description
본 발명은 폐식용유를 이용한 바이오 디젤의 제조장치에 관한 것으로서, 메탄올과 알칼리 촉매제를 첨가하여 에스테르 교환방식의 화학반응을 이용하여 정제하고, 이후 연료로서의 품질을 향상시키기 위해 세정, 탈수 공정을 거쳐 경유 성상과 동일한 바이오 디젤의 제조를 완료하게 되는 폐식용유를 이용한 바이오 디젤의 제조장치에 관한 것이다.The present invention relates to an apparatus for producing biodiesel using waste cooking oil, wherein methanol and alkali catalyst are added to purify using a transesterification chemical reaction, and thereafter, diesel is washed and dehydrated to improve quality as a fuel. The present invention relates to a biodiesel manufacturing apparatus using waste cooking oil, which completes the production of biodiesel having the same properties.
종래의 경우, 일반 가정이나 식당 및 식품가공회사에서 사용한 후 대량으로 배출되는 식물성 폐식용유는 하수도로 그냥 배출하거나 폐기물 처리하여 방치하는 경우가 대부분이었고, 이로 인해 심각한 환경오염의 주범이 되기도 하였다.In the conventional case, vegetable waste cooking oil discharged in large quantities after being used at homes, restaurants, and food processing companies is usually discharged to sewage or disposed of by waste treatment, which is a major culprit of serious environmental pollution.
또한, 가정이나 산업현장 등에서 대표적으로 사용되는 석유와 경유는 그 의존도가 점점 높아지면서 점차 자원고갈로 인해, 그 가격이 계속 상승하는 추세이고 이러한 유가상승 부담에 따라 대체연료를 개발하려는 시도가 계속 이루어지고 있는 실정이다.In addition, oil and diesel, which are typically used in homes and industrial sites, are increasingly dependent on the depletion of resources, and their prices continue to rise, and attempts to develop alternative fuels have been made in response to the burden of rising oil prices. It is losing.
따라서 이를 해소하기 위하여 폐식용유를 수거하고 약품처리를 통해 바이오 디젤화 하는 방법이 소개되어 있기도 하나, 실용화되어 사용하기에는 불편함이 있었고 그 제조단가가 높은 단점이 있었다.Therefore, in order to solve this problem, a method of collecting waste cooking oil and biodiesel through chemical treatment is introduced, but it is inconvenient to be used for practical use, and its manufacturing cost is high.
본 발명은 종래의 제반 문제점을 감안하여 안출된 것으로서, 보다 안전하고 용이하게 사용할 수 있도록 장치를 제공하고, 상기 장치를 통해 수거되는 폐식용유를 에스테르 교환방식을 통해 정제하여 석유, 경유 등의 원료를 대체하는 바이오디젤의 제조장치를 제공하는 데 목적이 있는 것이다.The present invention has been made in view of the conventional problems, to provide a device for safer and easier use, and to refine the waste cooking oil collected through the device through a transesterification method to raw materials such as petroleum, diesel It is an object of the present invention to provide an apparatus for manufacturing a biodiesel to be replaced.
본 발명의 목적을 달성하기 위하여, 가정이나, 식당 또는 대형 공장 등에서 수거된 폐식용유를 교반탱크에 충진하고, 충진된 폐식용유에 메탄올과 촉매제 1, 2군을 투여하는 공정을 거쳐,In order to achieve the object of the present invention, the waste cooking oil collected from a home, a restaurant, a large factory, etc. is filled in a stirring tank, and through the process of administering methanol and a catalyst group 1 and 2 to the filled waste cooking oil,
스크류 및 구동모터 그리고 히터가 장치되는 교반탱크와, 이들을 제어하는 제어반을 통해 일정 데이타에 따라 일정한 시간동안 열을 가하고 교반하여 정제된 바이오디젤을 추출하는 장치를 그 기본구성으로 제공한다.A stirring tank equipped with a screw, a driving motor and a heater, and a control panel for controlling them provide a device for extracting purified biodiesel by applying heat and stirring for a predetermined time according to predetermined data.
본 발명은 폐식용유를 수거하고 이를 정제하여 바이오 디젤을 추출함에 있어서, 그 찌꺼기로 나온 글리세린 제조용은 유류연소용 연료와 혼합해서 사용할 수 있으며, 또한, 가축의 분뇨와 혼합하여 사용하면 토양의 박테리아와 잘 결합하여 발효효과가 향상되어 토양의 질을 개선, 향상시키며, 폐식용유에서 정제한 바이오디젤을 사용함으로써 연소시 발생하는 Co2 등의 공해성분을 줄여 환경오염을 방지하고 석유 및 경유의 대체연료로서 사용하는 효과를 갖는 것이다.In the present invention, the waste cooking oil is collected and purified to extract biodiesel. For the production of glycerin, the residues can be used in combination with fuel for fuel combustion, and when used in combination with livestock manure, It combines well and improves fermentation effect, improving and improving soil quality. By using biodiesel purified from waste cooking oil, it reduces pollution of Co2, etc. generated during combustion, to prevent environmental pollution, and as alternative fuel for petroleum and diesel. It is to have an effect to use.
본 발명에서 식물성 폐식용유는 점도가 높기 때문에 점도를 낮추는 처리가 필요하고, 이를 위해서는 알콜과 산이 산 촉매 하에서 에스텔기와 물을 생성시키는 반 에스테르화 교환방식을 이용하여 혼합하고, 이를 세정 탈수 공정을 거치면서 바이오디젤을 추출하는 것을 특징으로 하는 바이오 디젤의 제조장치에 관한 것이다.In the present invention, the vegetable waste cooking oil has a high viscosity and thus requires a treatment for lowering the viscosity, and for this, alcohol and acid are mixed using a semi-esterification exchange method in which an ester and a water are produced under an acid catalyst, followed by a washing and dehydration process. While the present invention relates to a biodiesel manufacturing apparatus characterized by extracting biodiesel.
본 발명에서 사용되는 식물성 폐식용유는 가정, 식당 또는 식품가공 공장에서 사용한 후 배출되는 폐식용유로서 옥수수유, 대두유, 채종유, 미강유, 아마인유 또는 이들의 혼합유를 포함한다.The vegetable waste cooking oil used in the present invention includes corn oil, soybean oil, rapeseed oil, rice bran oil, linseed oil or mixed oils thereof as waste cooking oil discharged after use in homes, restaurants or food processing plants.
이러한 폐식용유를 수거하여 음식물 등의 찌꺼기를 제거하고 교반탱크에 충진하여, 설정된 공정을 거쳐 바이오 디젤을 얻게 되는 것이다.The waste cooking oil is collected to remove food waste and the like, and filled in a stirring tank to obtain biodiesel through a set process.
본 발명에 따른 바이오디젤은 기존 석유 연료에 비하여 독성이 적고 매연과 같은 공해물질이 적기 때문에 청정연료로서, 폐식용유에 의해 발생할 수 있는 환경 오염을 방지하고 재활용할 수 있다.Biodiesel according to the present invention is a clean fuel because it is less toxic than conventional petroleum fuel and less pollutants such as smoke, it is possible to prevent and recycle the environmental pollution that may be caused by waste cooking oil.
따라서 본 발명의 바이오디젤은 산업발전 시설 및 보일러 연료인 등유, 경유, 대체연료로 유효하게 사용할 수 있는 것이다.Therefore, the biodiesel of the present invention can be effectively used as kerosene, diesel, and alternative fuel which is an industrial power plant and a boiler fuel.
이하, 실시예에 의거하여 본 발명을 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail with reference to Examples.
(실시예 1)(Example 1)
폐식용유를 수거하여 탈수작업을 거쳐 수분을 제거하고 불순물을 여과시켜 찌꺼기를 제거하여 준비한다.The waste cooking oil is collected and dehydrated to remove moisture, and impurities are filtered to prepare the residue.
(실시예 2)(Example 2)
실시예 1과 같이 하여 마련된 정제 폐식용유를 교반탱크(10)에 충진한다.The refined waste cooking oil prepared as in Example 1 is filled into the stirring
(실시예 3)(Example 3)
상기 정제 폐식용유 100중량%에 대하여, 메탄올 20중량%, 나트륨계열의 촉매제1군 2%중량, 엽산 촉매제2군 0.1%중량을 투입하여 60℃의 열로써 60분 동안 교반탱크(10)에서 혼합한다.To 100% by weight of the refined waste cooking oil, 20% by weight of methanol, 2% by weight of sodium-based catalyst group 1, and 0.1% by weight of folate catalyst group 2 were mixed and mixed in the stirring
(실시예 4)(Example 4)
상기 실시예 3을 완료하고, 30분간 대기하면 응고된 침전물이 발생 되는데, 이를 분리 배출한다.After completing Example 3, waiting 30 minutes to generate a solidified precipitate, which is separated and discharged.
(실시예 5)(Example 5)
상기 침전물을 배출하고, 남은 정제 폐식용유 100% 중량에 대하여 물 20%중량과 엽산 촉매제 2군 0.1중량%를 투여하여 60℃ 온도하에서 30∼50분 가량 교반 혼합한다.The precipitate was discharged, 20% by weight of water and 0.1% by weight of folic acid catalyst group 2 were administered to 100% by weight of the remaining refined waste cooking oil, followed by stirring for 30 to 50 minutes at a temperature of 60 ° C.
(실시예 6)(Example 6)
상기 실시예 4와 같이 교반장치 동작을 멈추고 30분간 대기상태에 있게 되면 응고되는 침전물이 발생하고 이를 분리 배출한다.When the stirring apparatus stops as in Example 4 and remains in the standby state for 30 minutes, a solidified precipitate is generated and discharged separately.
상기와 같은 공정을 거쳐 투명한 오렌지 색상의 부유액을 추출하여 바이오디젤이 얻어졌다.Biodiesel was obtained by extracting the suspension of the transparent orange color through the above process.
상기에서 얻어진 본 발명의 바이오디젤을 일반 디젤과 비교하면 다음과 같다.The biodiesel of the present invention obtained above is compared with general diesel as follows.
비 교 표Comparison table
상기 비교표를 통해 알 수 있듯이 인화점이 경유와 비교하여 약 2배가량 높기 때문에 취급 저장에 있어서 안전성이 높다.As can be seen from the comparison table, since the flash point is about twice as high as that of diesel, the safety in handling and storage is high.
또한, SOx의 발생원인이 되는 유황분이 현저하게 낮기 때문에 사용시에 대기를 오염시키지 않게 된다.In addition, since sulfur content, which causes SOx, is significantly low, the air is not polluted during use.
상기 공정에 따른 본 발명의 장치의 동작은 다음과 같다.The operation of the apparatus of the present invention according to the above process is as follows.
도 1에서 보는 바와 같이 교반탱크(10)는 원통형 호퍼 형태로 제작되어 지며, 지상에 설치될 수 있도록 지주체(13)가 4개소 이상 설치되어 있다.As shown in FIG. 1, the
상기 호퍼 형태의 교반탱크(10) 하부에는 선택에 의해 개방 또는 폐쇄되는 배출구(115)가 형성된다.A discharge port 115 is formed at the lower portion of the hopper-
상기 교반탱크(10) 내부에는 외부전원의 인가에 의해 동작되는 히터선(미도시함)이 내장되어 있고, 그리고 구동모터(21)에 의해 동작되는 스크류(23)는 회전축(22)을 매개로 결합형성된다.The
상기 히터와 구동모터(21)는 전기적으로 연결된 제어반(12)에 의해 작동제어가 가능한 것이다.The heater and the driving
상기와 같이 구성되어 진 교반탱크(10) 내부에 폐식용유와 메탄올 그리고 첨가제 1,2군을 투입하고, 제어반을 통해 일정한 온도(60℃ 구동모터(21)의 동작시간을 설정하고 동작시키게 되면,When the waste cooking oil, methanol and additives 1,2 are added to the stirring
구동모터(21)의 동작으로 회전축(22)과 연결된 스크류(23)는 회전하면서 교반탱크(10) 내부의 폐식용유를 강제로 혼합하게 된다.The
이는 원심분리기의 원리를 이용하여 충진된 액체의 성분을 에스테르화 하는 반응을 갖게 한다.This allows the reaction of esterifying the components of the filled liquid using the principle of centrifuge.
이때 히터선에도 전원이 인가되므로 설정한 온도의 열이 인가되면서 혼합공정이 이루어 지게 되는 것이다.In this case, since power is also applied to the heater wire, the mixing process is performed while heat of the set temperature is applied.
이어서, 설정된 시간동안 작동이 완료된 상태에서 교반탱크(10)에서 일정시간 대기하게 되면, 응고된 액상의 침전물이 탱크(10) 하부에 가라앉게 되고 이를 배출구(15)를 통해 배출하고 탱크(10) 상부의 액상의 부유물은 성상의 정제 폐식용유는 상기의 방법대로 재차 2-3회 정도의 교반공정을 거쳐 투명한 오렌지 색상의 바이오디젤을 얻게 되는 것이다.Subsequently, when waiting for a predetermined time in the stirring
이상과 같이 설명된 본 발명은 한정된 실시예를 참고하여 설명하였으나, 본 발명은 상기한 실시예에 한정되지 아니하며, 본 발명의 바이오디젤을 추출하기 위한 에스테르 교환반응 및 교반공정을 이용하여 본 발명 요지를 벗어나지 않는 범위 내에서 당해 발명이 속하는 기술 분야의 통상적 지식을 가진 자에 의하여 다양한 변경과 수정이 이루어질 수 있는 것이며, 이는 본 발명의 권리범위에 속하는 것은 당연한 것이다.The present invention described above has been described with reference to a limited embodiment, but the present invention is not limited to the above embodiment, the present invention using the transesterification reaction and agitation process for extracting the biodiesel of the present invention Various changes and modifications may be made by those skilled in the art to which the present invention pertains without departing from the scope of the present invention, which naturally belongs to the scope of the present invention.
도 1은 본 발명의 구조를 보여주기 위한 사시도1 is a perspective view showing the structure of the present invention
도 2는 본 발명의 공정을 나타내기 위한 공정순서도2 is a process flow chart showing the process of the present invention
(도면의 주요부분에 대한 부호의 설명)(Explanation of symbols for the main parts of the drawing)
10...교반탱크 11...폐식용유 투입구10 ... Stirring tank
12...제어반 13...지주체12 ...
14...잔량표시구 15...배출구14 ... Remaining
21...구동모터 22...회전축21
23...스크류23 ... screw
Claims (3)
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KR1020080012753A KR100858663B1 (en) | 2008-02-12 | 2008-02-12 | The device of manufacturing the bio-diesel with waste edible-oil |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019098556A1 (en) * | 2017-11-20 | 2019-05-23 | 김경화 | Apparatus and method for production of biodiesel |
KR20210061083A (en) | 2019-11-19 | 2021-05-27 | 무진기공주식회사 | Assembly apparatus of the Bio-diesel reactor |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH07197047A (en) * | 1993-12-30 | 1995-08-01 | Someya Shoten:Kk | Diesel fuel and its production |
US5514820A (en) * | 1989-09-29 | 1996-05-07 | Henkel Kommanditgesellschaft Auf Aktien | Continuous process for the production of lower alkyl esters |
KR100495425B1 (en) * | 1998-02-24 | 2005-09-15 | 삼성전자주식회사 | Oil detection device and automatic oil supply device using laser |
-
2008
- 2008-02-12 KR KR1020080012753A patent/KR100858663B1/en not_active IP Right Cessation
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5514820A (en) * | 1989-09-29 | 1996-05-07 | Henkel Kommanditgesellschaft Auf Aktien | Continuous process for the production of lower alkyl esters |
JPH07197047A (en) * | 1993-12-30 | 1995-08-01 | Someya Shoten:Kk | Diesel fuel and its production |
KR100495425B1 (en) * | 1998-02-24 | 2005-09-15 | 삼성전자주식회사 | Oil detection device and automatic oil supply device using laser |
Non-Patent Citations (1)
Title |
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논문;한국신재생에너지학회 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019098556A1 (en) * | 2017-11-20 | 2019-05-23 | 김경화 | Apparatus and method for production of biodiesel |
KR20210061083A (en) | 2019-11-19 | 2021-05-27 | 무진기공주식회사 | Assembly apparatus of the Bio-diesel reactor |
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