KR100768760B1 - Peel-off pack cosmetic composition containing starch or the derivatives thereof - Google Patents
Peel-off pack cosmetic composition containing starch or the derivatives thereof Download PDFInfo
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- KR100768760B1 KR100768760B1 KR1020050134645A KR20050134645A KR100768760B1 KR 100768760 B1 KR100768760 B1 KR 100768760B1 KR 1020050134645 A KR1020050134645 A KR 1020050134645A KR 20050134645 A KR20050134645 A KR 20050134645A KR 100768760 B1 KR100768760 B1 KR 100768760B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
본 발명은 필오프팩 화장료 조성물에 관한 것으로, 보다 상세하게는 필오프팩의 필름막 형성 주원료인 폴리비닐알콜(Polyvinyl Alcohol:PVA)에 전분(starch) 또는 그 유도체를 함유하여 필름막 조직강도의 변화로 팩 인장강도가 높아지고 건조시간이 빨라지게 하는 필오프 타입 팩 화장료 조성물에 관한 것이다.The present invention relates to a peel-off pack cosmetic composition, and more particularly, containing starch or a derivative thereof in polyvinyl alcohol (PVA), a film film-forming main ingredient of the peel-off pack, The present invention relates to a peel-off pack cosmetic composition for increasing pack tensile strength and speeding drying time.
필오프팩 * 폴리비닐알콜 * 전분 * 인장강도 * 건조시간 Peel-off Pack * Polyvinyl Alcohol * Starch * Tensile Strength * Drying Time
Description
본 발명은 필오프 팩 화장료 조성물에 관한 것으로, 보다 상세하게는 필오프 팩의 필름막 형성 주원료인 폴리비닐알콜(Polyvinyl Alcohol:PVA)에 전분(starch) 또는 그 유도체를 함유하여 필름막 조직강도의 변화로 팩 인장강도가 높아지고 건조시간이 빨라지게 하는 필오프 타입 팩 화장료 조성물에 관한 것이다.The present invention relates to a peel-off pack cosmetic composition, and more particularly, containing starch or a derivative thereof in polyvinyl alcohol (PVA), which is a film film-forming main ingredient of the peel-off pack, The present invention relates to a peel-off pack cosmetic composition for increasing pack tensile strength and speeding drying time.
팩이라 함은 진부한 물질과 죽은 상피세포 잔여물의 제거, 지방과 땀분비의 조절, 피부 혈색의 촉진, 체액의 조절, 피부 신장의 균일화 및 주름 형성의 감소를 목적으로 하는 미용제를 말하는 것으로 그 어원을 살펴보면 ‘Pack’이란 말은‘감싼다’,‘덮는다’는 뜻을 가지고 있으며 독일에서는 ‘Packung’또는 ‘Maske’, 불어권에서는 ‘Masque’, 이태리에서는 ‘Maschera’라 한다. 팩은 제형과 사용방법에 따라 건조된 필름을 제거하는 필오프 타입 팩, 팩제를 바른 후 물 세안으로 팩을 제거하는 워시오프 타입 팩, 티슈로 닦아내는 티슈오프 타입 팩 및 시트에 유액이 적셔 있는 시트 타입 팩으로 구분할 수 있다.Pack refers to cosmetics aimed at eliminating clichés and dead epithelial cell residues, controlling fat and sweat secretion, promoting skin coloration, regulating body fluids, equalizing skin elongation and reducing wrinkle formation. The word 'Pack' means 'to wrap' and 'cover'. In Germany, 'Packung' or 'Maske' is called 'Masque' in French and 'Maschera' in Italy. The pack is a peel-off type pack that removes the dried film according to the formulation and the method of use, a wash-off type pack that removes the pack with water wash after applying the pack agent, a tissue-off type pack that is wiped off with tissue, and the sheet is damp It can be divided into a sheet type pack.
그 중에서 필오프 타입 팩은 별도의 세안이 필요하지 않고 팩제를 바르고 마른 후 바로 팩을 떼어내므로 사용이 편리하고 모공 노폐물 제거 및 각질 케어 기능이 뛰어나 대표적으로 많이 사용하는 팩 제형의 하나이다. 그러나 필오프 팩은 피부와의 밀착력이 커서 팩을 떼어낼 때 피부에 자극을 줄 수 있어 민감한 피부에서는 사용이 어려우며, 팩 제거시에 팩의 일부가 그냥 끊어져 버려 깨끗하게 제거되지 못하고 피부에 남아있는 등의 문제가 있다.Among them, the peel-off type pack is one of the pack formulations that are commonly used because they do not require separate face-wash and apply the pack and remove the pack immediately after drying. However, peel-off packs have strong adhesion to the skin, which can irritate the skin when the pack is removed, making it difficult to use on sensitive skin, and when the pack is removed, some of the packs are simply broken off and remain on the skin. There is a problem.
상기와 같은 팩 제거가 용이하지 못한 문제를 해결하기 위해 필오프 팩의 점도를 높여주는 방법이 사용되는데, 첫번째 방법은 팩 성분 중 대표적인 필름 형성제인 폴리비닐알콜(PVA)의 함량을 높여 점도를 높이는 방법이 있으나, 폴리비닐알코올의 함량을 15% 이상 사용할 경우 점도가 높아져서 발림성이 떨어지고 건조시간이 길어지는 단점이 있다. 두번째 방법은 하이드록시에틸셀룰로즈, 카르복실메틸셀룰로즈, 폴리비닐피롤리돈, 잔탄검 등의 고분자 폴리머를 이용하여 제형의 점도를 높이는 방법이 있으나, 이 방법 또한 자체의 점도는 높이지만 발림성 저하 등의 문제를 가져오고 점도 상승 이외에 팩의 인장강도를 높여주는 기능은 약한 편이다.In order to solve such a problem that the pack removal is not easy, a method of increasing the viscosity of the peel-off pack is used. The first method is to increase the viscosity by increasing the content of polyvinyl alcohol (PVA), which is a representative film former, among the pack components. Although there is a method, when the content of polyvinyl alcohol is used more than 15%, there is a disadvantage in that the viscosity increases and the application time decreases and the drying time is long. The second method is to increase the viscosity of the formulation by using a polymer such as hydroxyethyl cellulose, carboxymethyl cellulose, polyvinylpyrrolidone, xanthan gum, etc., but this method also increases its viscosity but decreases application properties. In addition to causing problems and increasing viscosity, the ability to increase the pack's tensile strength is weak.
한편, 팩의 점도 상승으로 인장강도를 어느 정도 높여주어도 팩의 건조시간이 길어지는 부수적인 문제가 따라오게 되는데, 이를 해결하기 위하여 종래에는 필오프 팩에서 알코올을 사용하여 팩 건조시간을 단축하고 있으나, 알코올의 함량이 증가함에 따라 팩 건조시간은 줄어드나 피부 안전성은 크게 나빠지는 문제가 발생되어 건조시간 단축을 위해 팩 제형 내에 10% 이상의 알코올을 사용하는 것은 어렵다.On the other hand, even if the tensile strength is increased to some extent by increasing the viscosity of the pack, there is a side problem that the drying time of the pack is accompanied. To solve this problem, the pack drying time is shortened by using alcohol in the peel-off pack. As the alcohol content increases, the pack drying time decreases but the skin safety is significantly worsened. Therefore, it is difficult to use more than 10% alcohol in the pack formulation to shorten the drying time.
상기와 같이 필오프 팩 제형의 인장강도를 개선하고자 많은 연구가 진행되었지만 인장강도와 건조속도를 개선하여 팩 제거가 용이하도록 한 연구사례는 없었다.As described above, many studies have been conducted to improve the tensile strength of the peel-off pack formulation.
이에 본 발명자들은 상기와 같은 문제점을 해결하고자 예의연구한 결과, 폴리비닐알콜(PVA)을 주성분으로 하는 팩 제형에 전분 또는 그 유도체를 함유시킴으로써 팩의 인장강도와 건조속도를 높여 팩 제거가 용이하게 됨을 밝혀내여 본 발명을 완성하였다.Accordingly, the present inventors have studied diligently to solve the above problems, and as a result of containing starch or a derivative thereof in a pack formulation mainly containing polyvinyl alcohol (PVA), it is easy to remove the pack by increasing the tensile strength and drying speed of the pack. It was found that the present invention was completed.
따라서 본 발명의 목적은 인장강도와 건조속도를 개선하여 팩 제거가 용이한 필오프 팩 화장료 조성물을 제공하는 것이다.Therefore, an object of the present invention is to provide a peel-off pack cosmetic composition that is easy to remove the pack by improving the tensile strength and drying speed.
상기한 목적을 달성하기 위하여, 본 발명에 따른 필오프 팩 화장료 조성물은 필름 형성제로 폴리비닐알코올을 사용하고 인장강도 및 건조속도 개선을 위해 전분 또는 그 유도체를 더 함유하는 것을 특징으로 한다.In order to achieve the above object, the peel-off pack cosmetic composition according to the present invention is characterized in that it uses polyvinyl alcohol as a film forming agent and further contains starch or derivatives thereof for improving tensile strength and drying rate.
본 발명에 따른 필오프 팩 화장료 조성물은 조성물 전체 중량에 대하여 폴리비닐알코올을 5~20 중량% 함유하고, 전분 또는 그 유도체를 0.001~10 중량% 함유하는 것을 특징으로 한다.The peel-off pack cosmetic composition according to the present invention is characterized by containing 5 to 20% by weight of polyvinyl alcohol and 0.001 to 10% by weight of starch or derivatives thereof based on the total weight of the composition.
이하, 본 발명을 보다 상세히 설명하기로 한다. Hereinafter, the present invention will be described in more detail.
본 발명에 사용된 폴리비닐알코올은 화장품 원료로서 공지된 것으로 대표적인 필오프 타입 팩의 필름형성제로 수상에 용해되어 물이 날아가면서 가교되어 흡착 효과에 의해 피부에 부착한 오염이나 오래된 각질층을 제거하는 청정 효과도 겸비하고 있다. 상기 폴리비닐알코올은 팩의 용도, 성질에 맞추어 시판되는 것중에서 적당한 것을 사용할 수 있으며, 본 발명의 실시예에서는 분자량에 따라 일본 Kuraray사의 상품명 PVA217,205를 사용하였다.The polyvinyl alcohol used in the present invention is known as a raw material for cosmetics and is a film peeling agent of a typical peel-off type pack, which is dissolved in an aqueous phase and crosslinked with water as it flows, thereby removing dirt or dead skin layers attached to the skin by an adsorption effect. It also has an effect. As the polyvinyl alcohol, a suitable one can be used among commercially available ones according to the use and properties of the pack. In the examples of the present invention, the trade name PVA217,205, manufactured by Kuraray Japan, was used according to the molecular weight.
본 발명의 팩 화장료에 있어서, 상기 PVA의 함유량은 조성물 전체 중량에 대하여 5~20 중량%가 바람직하다. PVA의 함유량이 5중량% 미만이면 필름형성이 제대로 되지 않아 피막이 약하고 얇게 되어 필오프력이 떨어지게 되어 제품으로 사용이 어려우며, 20중량%를 초과하면 점도 상승으로 펴 발림성이 나빠지고 피부와 밀착력이 높아져 자극을 유발할 위험이 커진다.In the pack cosmetic of the present invention, the content of the PVA is preferably 5 to 20% by weight based on the total weight of the composition. If the content of PVA is less than 5% by weight, the film is not properly formed and the film is weak and thin, resulting in a peel-off force, making it difficult to use as a product.When it exceeds 20% by weight, the spreadability is worsened and the adhesion to skin is increased. The risk of causing irritation increases.
한편, 본 발명에 있어서 필오프 팩의 인장강도 상승 및 건조 속도 개선을 위해 사용되는 전분(Starch)은, 포도당이 그 기본 구조로 사용되어 있으며 긴 사슬 모양의 아밀로오즈와 가지처럼 연결된 아밀펙틴의 두 타입이 복합적으로 이루어져 있으며 식품, 섬유, 화장품 등에서 여러 가지 형태로 광범위하게 사용되고 있는 원료이다. 본 발명의 실시예에 사용된 전분은 National Starch사의 상품명 structure XL인 옥수수 전분에 하이드록시프로필화한 원료를 사용하였다.Meanwhile, in the present invention, starch, which is used to increase the tensile strength of the peel-off pack and improve the drying speed, is composed of amylopectin, in which glucose is used as its basic structure and connected with long-chain amylose. Combining both types, it is a raw material that is widely used in various forms in food, textiles, and cosmetics. The starch used in the examples of the present invention used a raw material which was hydroxypropylated on corn starch under the name of Structure XL of National Starch.
본 발명의 팩 화장료에 있어서, 상기 전분의 함유량은 조성물 전체 중량에 대하여 0.001~10 중량%가 바람직하다. 전분의 배합량이 0.001 중량% 미만에서는 필름의 인장강도, 건조 속도나 외관에 영향을 주지 못하고, 또한 함유량이10 중량%을 초과하면 점도가 과도하게 높아지기 때문에 사용 시 펴기가 어렵고 발림성이 나빠져서 제품화가 어려워지는 문제가 발생한다.In the pack cosmetic of the present invention, the content of the starch is preferably 0.001 to 10% by weight based on the total weight of the composition. If the amount of starch is less than 0.001% by weight, it does not affect the tensile strength, drying speed or appearance of the film, and if the content exceeds 10% by weight, the viscosity becomes excessively high, so it is difficult to unfold during use and the applicability becomes poor, making it difficult to commercialize. Losing problems occur.
본 발명의 팩 화장료의 조제에 있어서는, 상기 각 성분 외에, 통상 화장료에 사용되는 성분을 본 발명의 효과를 손상시키지 않는 범위에서 당업자가 적절하게 선정할 수 있다.In the preparation of the pack cosmetics of the present invention, those skilled in the art can appropriately select, in addition to the components described above, components that are usually used in cosmetics without impairing the effects of the present invention.
이하, 실시예, 시험예를 들어 본 발명을 보다 구체적으로 설명하지만,본 발명의 범위가 이들예에 한정되는 것은 아니다.Hereinafter, although an Example and a test example are given and this invention is demonstrated more concretely, the scope of the present invention is not limited to these examples.
[실시예 1-3 및 비교예 1-2][Example 1-3 and Comparative Example 1-2]
하기 표 1에 나타낸 조성을 사용하여 하기의 제법에 의해 실시예 1-3 및 비교예 1-2를 제조하였다. 실시예 1-3은 물파트를 75-80℃까지 가온한 후, 폴리비닐알코올을 천천히 혼합하여 용해시키고 Structure XL은 용해 후 바로 투입혼합하였다. 그 후 50℃까지 냉각시킨 후, 알코올 파트를 투입하고 30℃까지 냉각하였다. 비교예 1-2는 실시예 1-3과 같은 공정으로 실시하되 별도의 용기에 물을 일부 덜어 셀룰로오스 검을 미리 풀어 놓아 폴리비닐알코올 용해 이후 투입하였다.Using the compositions shown in Table 1 below, Example 1-3 and Comparative Example 1-2 were prepared by the following method. In Example 1-3, after warming the water part to 75-80 ° C., polyvinyl alcohol was slowly mixed to dissolve, and Structure XL was added and mixed immediately after dissolution. Then, after cooling to 50 degreeC, the alcohol part was thrown in and it cooled to 30 degreeC. Comparative Example 1-2 was carried out in the same manner as in Example 1-3, but by dissolving some of the water in a separate container in advance to release the cellulose gum was added after polyvinyl alcohol dissolved.
* 상품명 : PVA 217/205 (일본 Kuraray) * Product Name: PVA 217/205 (Japan Kuraray)
** 상품명 : Structure XL (미국 National Starch) ** Product Name: Structure XL (USA National Starch)
이상의 실시예 1-3 및 비교예 1-2에 대하여 인장강도, 건조시간에 대한 시험을 실시하였다.Tests for tensile strength and drying time were performed for Examples 1-3 and Comparative Examples 1-2.
필름의 인장 강도 측정Tensile Strength Measurement of Film
필오프 팩 필름의 인장 강도를 측정하기 위하여, 실시예1-3 및 비교예 1-2의 시료를 각각 0.1mm씩 일정한 두께가 되도록 도포한 후, 45℃ 항온조에서 팩이 완전히 마를 때까지 건조시키고 마른 팩을 1.5×1.5 (cm2)로 잘라 3mm/초의 속력으로 장력 시험을 실시하였다. 힘을 이기지 못하고 팩이 절단되는 시점을 인장강도로 정하고, 그 측정 결과를 하기 표 2에 나타내었다.In order to measure the tensile strength of the peel-off pack film, the samples of Example 1-3 and Comparative Example 1-2 were each applied in a constant thickness of 0.1 mm, and then dried in a 45 ° C. thermostat until the pack was completely dry. The dry pack was cut into 1.5 × 1.5 (cm 2 ) and subjected to a tension test at a speed of 3 mm / sec. The point at which the pack was cut without breaking the force was determined as the tensile strength, and the measurement results are shown in Table 2 below.
상기 표 2에서 알 수 있듯이 전분을 넣지 않은 비교예 1및 전분 대신 점증제를 넣은 비교예 2에 비하여 전분을 넣은 실시예 1-3의 경우가 인장 강도가 크게 나타나 전분을 함유함으로써 인장강도를 증가시키는데 도움을 주는 것을 알 수 있었다.As can be seen in Table 2, Comparative Examples 1, in which starch is added, and Comparative Examples 1, in which starch is added, instead of starch, are increased in tensile strength by increasing starch. It was found to help.
필름의 건조 속도 측정Measurement of Drying Speed of Film
필오프 팩 필름의 건조 속도를 측정하기 위하여, 실시예 1-3 및 비교예 1-2의 시료를 각각 1g씩 정확히 평량하여 측정 접시에 고르게 펴 바른 후, 수분 측정기 (MB45 Moisture Analyzer, Ohaus Co., USA)를 이용하여 50℃에서 수분을 증발시켜면서 무게 변화를 측정하고 더 이상 무게의 변화가 없는 지점을 증발 종료 시점으로 잡아 각 시료의 건조시간을 비교하였다.In order to measure the drying rate of the peel-off pack film, 1 g each of the samples of Example 1-3 and Comparative Example 1-2 were precisely weighed and evenly spread on a measuring plate, followed by a moisture meter (MB45 Moisture Analyzer, Ohaus Co. , USA) was used to measure the change in weight while evaporating moisture at 50 ° C., and the drying time of each sample was compared by taking the point where there was no change in weight as the end of evaporation.
전분을 넣지 않은 비교예 1및 비교예 2에 비하여 전분을 넣은 실시예 1-3의 경우가 필름의 건조속도가 빠른 것으로 나타났으며, 전분의 함유량이 1.0중량%인 경우 건조시간이 가장 짧게 나타났다. 따라서 폴리비닐알코올을 주성분으로 하는 필오프 팩에 전분을 첨가함에 따라 필름의 건조 속도가 빨라짐을 알 수 있었다.Compared with Comparative Example 1 and Comparative Example 2 without the starch, Examples 1-3 containing the starch showed a faster drying speed, and the drying time was shortest when the starch content was 1.0% by weight. . Therefore, it was found that the drying speed of the film was increased by adding starch to the peel-off pack mainly containing polyvinyl alcohol.
이상과 같이 본 발명에 따른 조성물은 폴리비닐알코올을 주원료로 하는 필오프 팩 제형에 전분을 함유함으로써 필름의 인장강도를 높여 팩 제거를 용이하게 하고 건조 시간을 단축시켜 팩 제형의 품질을 향상시키는데 효과가 있다.As described above, the composition according to the present invention contains starch in the peel-off pack formulation containing polyvinyl alcohol as the main ingredient, thereby increasing the tensile strength of the film, facilitating pack removal, and shortening the drying time, thereby improving the quality of the pack formulation. There is.
Claims (3)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160144836A (en) | 2015-06-09 | 2016-12-19 | (주)뷰티화장품 | Peel-off pack composition containing rice bran, kaolin and bentonite and method for preparing the same |
| KR20210027850A (en) | 2019-09-03 | 2021-03-11 | 주식회사 코스온 | Peel-off Pack coxmetic composition preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| FR2990348B1 (en) * | 2012-05-10 | 2016-07-01 | Lvmh Rech | COMPOSITION AND METHOD FOR COSMETIC CARE USING ELASTIC MIXTURE |
| KR101683833B1 (en) * | 2015-01-14 | 2016-12-09 | 주식회사 코스온 | Pill-off type osmetic composition improved the color and moisturizing of the lips and method for preparing the same |
| KR101667937B1 (en) * | 2016-01-05 | 2016-10-24 | 한국콜마주식회사 | Cosmetics composition of peel-off type pack and method preparing the same |
| KR20220121129A (en) | 2021-02-24 | 2022-08-31 | 최건우 | easy-to-open cone ice cream packaging |
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|---|---|---|---|---|
| JPS584707A (en) | 1981-06-29 | 1983-01-11 | Kanebo Ltd | Coating-type pack |
| JPS588006A (en) | 1981-07-02 | 1983-01-18 | Kanebo Ltd | Film type pack agent |
| KR970005275A (en) * | 1995-07-28 | 1997-02-19 | Self-image pack composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS584707A (en) | 1981-06-29 | 1983-01-11 | Kanebo Ltd | Coating-type pack |
| JPS588006A (en) | 1981-07-02 | 1983-01-18 | Kanebo Ltd | Film type pack agent |
| KR970005275A (en) * | 1995-07-28 | 1997-02-19 | Self-image pack composition |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160144836A (en) | 2015-06-09 | 2016-12-19 | (주)뷰티화장품 | Peel-off pack composition containing rice bran, kaolin and bentonite and method for preparing the same |
| KR20210027850A (en) | 2019-09-03 | 2021-03-11 | 주식회사 코스온 | Peel-off Pack coxmetic composition preparation method thereof |
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