KR100708409B1 - Rutin Extract Method from Buckwheat Bud and extracted rutin - Google Patents
Rutin Extract Method from Buckwheat Bud and extracted rutin Download PDFInfo
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Abstract
본 발명은 메밀싹 1 중량부에 대하여 물 2/3 중량부를 혼합하여 온도 70 ~ 95℃에서 40시간~50시간 동안 가열하는 제 1 가열단계(S10); 메밀싹을 건져내는 단계(S20); 및 메밀싹을 건져내고 남은 액체를 100℃에서 2시간 ~ 4시간 동안 가열하는 제 2 가열단계(S30);를 포함하는 것을 특징으로 하는 메밀싹으로부터 루틴 추출 방법을 제공한다. 본 발명에 따른 메밀싹으로부터 루틴 추출 방법은 건강에 해로운 알코올 또는 아세톤을 사용하지 않고 물을 용매로 루틴을 손쉽게 추출하여 안전하고 공정이 간이한 효과 및 높은 추출 효율로 높은 농도의 루틴을 추출할 수 있는 효과를 달성하게 한다.The present invention is a first heating step (S10) for heating for 40 hours to 50 hours at a temperature of 70 ~ 95 ℃ by mixing 2/3 parts by weight of water with respect to 1 part by weight of buckwheat sprout; Harvesting buckwheat sprout (S20); And a second heating step (S30) of extracting the buckwheat sprout and heating the remaining liquid at 100 ° C. for 2 hours to 4 hours. The routine extraction method from the buckwheat sprout according to the present invention can be easily extracted with water as a solvent without using unhealthy alcohol or acetone to extract a high concentration of routine with a safe and simple process and high extraction efficiency. To achieve the effect.
루틴, 메밀싹, 물, 추출, 가열 Rutin, Buckwheat Sprout, Water, Extraction, Heating
Description
본 발명은 메밀싹으로부터 루틴을 추출하는 방법에 관한 것으로, 보다 상세하게는 물과 메밀싹을 가열하여 메밀싹으로부터 루틴을 추출하는 방법에 관한 것이다.The present invention relates to a method of extracting rutin from buckwheat sprout, and more particularly, to a method of extracting rutin from buckwheat sprout by heating water and buckwheat sprout.
루틴(rutin, C27H30O16)은 일명 비타민 P로도 알려져 있으며, 비타민 C의 작용을 강화시키고, 모세혈관을 강화하고 모세혈관의 투과성을 조절하며, 혈압과 콜레스트롤을 낮추고, 신장 질환을 개선하며, 피부 노화를 방지하고, 비만을 방지하는 효능이 있는 것으로 알려져 있다. Rutin (C 27 H 30 O 16 ), also known as vitamin P, enhances the action of vitamin C, strengthens capillaries, regulates capillary permeability, lowers blood pressure and cholesterol, and improves kidney disease It is known to be effective in preventing skin aging and preventing obesity.
루틴은 메밀, 감자, 아스파라거스, 살구, 앵두, 토마토, 무화과, 감귤류, 팥 등 일상적으로 먹고 있는 야채, 과일뿐만 아니라 꿀, 녹차 등에도 함유되어 있다. 이 중 메밀에 특히 많은 루틴이 함유되어 있으며, 특히 메밀싹의 경우 루틴을 메밀 종실보다 다량 함유한 것으로 알려지고 있다.Rutin is found in buckwheat, potatoes, asparagus, apricots, cherry, tomatoes, figs, citrus fruits, and red beans, as well as honey and green tea. Among them, buckwheat contains a lot of rutin, and especially buckwheat sprout is known to contain a larger amount of rutin than buckwheat seeds.
메밀로부터 루틴을 추출하는 방법에 대하여는, 대한민국 특허공개 제1997-88 호, 대한민국 특허공개 제2002-15805호 및 대한민국 특허공개 제2005-7463호 등에 기재되어 있다. 상기 방법들은 메밀싹 또는 메밀 전초로부터 알코올 또는 아세톤을 용매로 하여 루틴을 추출하였다. 이러한 방법을 사용하는 경우 용매로 사용되는 이소프로판올, 메탄올, 에탄올(또는 주정), 아세톤 등은 건강에 해로우며, 추출액으로부터 이러한 알코올 또는 아세톤을 제거하기 위한 추가적인 공정이 필요하다.A method for extracting a routine from buckwheat is described in Korean Patent Publication No. 1997-88, Korean Patent Publication No. 2002-15805, and Korean Patent Publication No. 2005-7463. The methods extracted rutin with alcohol or acetone as solvents from buckwheat sprouts or buckwheat outposts. When using this method, isopropanol, methanol, ethanol (or spirits), acetone, and the like, which are used as solvents, are harmful to health and require an additional process for removing such alcohol or acetone from the extract.
이에 본 발명은 상기와 같은 문제점을 해결하기 위하여 안출된 것으로서, 본 발명의 제 1 목적은, 메밀싹에 함유된 다량의 루틴을 물을 용매로 하여 추출하는 것을 특징으로 하는 메밀싹으로부터 루틴 추출 방법을 제공하는 것이다. Accordingly, the present invention has been made to solve the above problems, the first object of the present invention is a routine extraction method from buckwheat sprout, characterized in that the extraction of a large amount of rutin contained in the buckwheat sprout with water as a solvent. To provide.
본 발명의 제 2 목적은, 높은 추출 효율과 높은 농도를 가지는 루틴 추출물을 추출할 수 있는 메밀싹으로부터 루틴 추출 방법을 목적으로 한다.A second object of the present invention is to provide a routine extraction method from buckwheat sprouts capable of extracting a routine extract having a high extraction efficiency and a high concentration.
본 발명의 그 밖의 목적, 특정한 장점들 및 신규한 특징들은 첨부 도면들과 관련되어 설명되는 이하의 상세한 설명과 바람직한 실시예들로부터 더욱 명확해질 것이다.Other objects, specific advantages and novel features of the invention will become more apparent from the following detailed description and the preferred embodiments described in conjunction with the accompanying drawings.
상기와 같은 본 발명의 목적들은, 메밀싹 1 중량부에 대하여 물 2/3 중량부를 혼합하여 온도 70 ~ 95℃에서 40시간 ~ 50시간 동안 가열하는 제 1 가열단계(S10); Objects of the present invention as described above, the first heating step (S10) for heating for 40 hours to 50 hours at a temperature of 70 ~ 95 ℃ by mixing 2/3 parts by weight of water with respect to 1 part by weight of buckwheat sprout;
상기 메밀싹을 건져내는 단계(S20); 및Harvesting the buckwheat sprout (S20); And
상기 메밀싹을 건져내고 남은 액체를 100℃에서 2시간 ~ 4시간 동안 가열하 는 제 2 가열단계(S30);를 포함하는 것을 특징으로 하는 메밀싹으로부터 루틴 추출 방법에 의해 달성될 수 있다.The buckwheat sprout can be achieved by a routine extraction method from the buckwheat sprout, characterized in that it comprises a; a second heating step (S30) for heating the remaining liquid at 100 ℃ for 2 hours to 4 hours.
제 1 가열단계(S10)는 약 48 시간인 것이 바람직하다.The first heating step S10 is preferably about 48 hours.
그리고, 제 2 가열단계(S30)는 약 3 시간인 것이 더욱 바람직하다.Further, the second heating step S30 is more preferably about 3 hours.
이하에서는 본 발명에 따른 메밀싹으로부터 루틴 추출 방법에 관하여 각 단계별로 더욱 상세하게 설명한다.Hereinafter, the routine extraction method from the buckwheat sprout according to the present invention will be described in more detail in each step.
우선, 본 발명의 실시예에서 사용하는 메밀싹을 준비한다. 메밀싹은 공지의 발아조건속에 발아된 메밀싹을 준비하며, 메밀싹을 발아시킨다. 메밀보다 메밀싹을 준비하는 이유는 발아과정에서 영양분의 변화로 인해 메밀싹이 메밀보다 루틴의 추출 함량이 높기 때문이다. First, buckwheat sprouts used in the embodiment of the present invention are prepared. Buckwheat sprout prepares the buckwheat sprout germinated under known germination conditions, and germinates the buckwheat sprout. The reason for preparing buckwheat sprouts rather than buckwheat is because buckwheat sprouts have a higher content of rutin than buckwheat due to changes in nutrients during germination.
그 다음, 준비된 메밀싹과 물의 중량비가 3 : 2 가 되도록 혼합된다. 본 실시예에서는 메밀싹 3 Kg에 대해 물 2 Kg을 혼합하였다.Then, the prepared buckwheat sprout and water are mixed so that the weight ratio is 3: 2. In this example, 2 Kg of water was mixed with 3 Kg of buckwheat sprout.
그 다음, 혼합된 메밀싹 및 물은 온도 70℃ ~ 95℃에서 48시간 동안 가열을 한다(1차 가열공정, S10). 만약 1차 가열온도가 95 ℃ 이상이 되면 물이 끓기 시작하기 때문에 메밀싹으로부터 루틴이 추출되기 보다 메밀싹 자체가 익어버리게 된다. 그리고, 1차 가열온도가 70 ℃ 이하가 되면, 48시간보다 더 오랫동안 가열하여야 하기 때문에 시간과 연료비 등의 부담이 증가하게 된다. 상기 온도 조건에서 48 시간 미만으로 가열할 경우 메밀싹으로부터 루틴이 충분하게 추출되지 않는다.Then, the mixed buckwheat sprout and water is heated for 48 hours at a temperature of 70 ℃ ~ 95 ℃ (primary heating step, S10). If the primary heating temperature is above 95 ℃, the water begins to boil, so the buckwheat sprout itself ripens rather than the routine extracted from the buckwheat sprout. When the primary heating temperature is 70 ° C. or less, the heating time is longer than 48 hours, and the burden of time and fuel cost is increased. When heated to less than 48 hours at the above temperature conditions, rutin is not sufficiently extracted from buckwheat sprout.
1차 가열단계후, 가열된 혼합물로부터 메밀싹을 건져낸다(S20). 이는 메밀싹으로부터 루틴이 충분히 빠져 나온 상태임으로 메밀싹을 건져내고 액체상태만으로 다음 공정을 진행하기 위함이다. After the first heating step, the buckwheat sprouts from the heated mixture (S20). This is to remove the buckwheat sprouts from the buckwheat sprouts and to proceed to the next process only in the liquid state.
그 다음, 메밀싹을 건져내고 남은 액체를 온도 100 ℃에서 3시간 동안 가열한다(2차 가열공정, S30). 2차 가열온도인 100 ℃는 액체를 끓이기 위한 온도이고 100 ℃ 이상으로 가열하는 경우 루틴 함량이 감소한다. 3시간 동안 가열함은 루틴과 기타 물질의 충분한 농축이 이루어지도록 하기 위함이다. 3시간 미만으로 가열할 경우 액체의 체적이 많고 농도가 낮아 추가적인 농축공정을 필요로 하고, 3시간 보다 오래 가열할 경우 용액이 지나치게 고농축화(엑기스화)되어 진뜩진뜩해지는 현상이 발생한다. Then, the buckwheat sprout is taken out and the remaining liquid is heated at a temperature of 100 ° C. for 3 hours (secondary heating step, S30). The secondary heating temperature of 100 ° C. is the temperature for boiling the liquid and the rutin content decreases when heated above 100 ° C. Heating for 3 hours is intended to allow sufficient concentration of the routine and other materials. If the heating time is less than 3 hours, the liquid volume is high and the concentration is low, so an additional concentration step is required, and if the heating time is longer than 3 hours, the solution is excessively concentrated (extracted), and the phenomenon of dulling occurs.
이와 같은 2차 가열단계를 거친 최종 액체는 갈색(커피색)이고 다량의 루틴으로 인해 미끈거리며, 시간이 지남에 따라 추출된 루틴이 액체의 윗부분에 부유하게 된다. 본 실시예와 같은 실험조건에 의할 경우 루틴 함량은 약 46 %이다. The final liquid undergoing this second heating step is brown (coffee) and slippery due to the large amount of routine, and over time the extracted routine becomes suspended in the upper portion of the liquid. According to the experimental conditions as in the present embodiment, the routine content is about 46%.
비록, 본 발명의 실시예에서는 1차 가열단계의 조건과 2차 가열단계의 조건에 관하여 구체적인 온도와 시간조건을 개시하고 있으나, 이는 본 발명의 기술사상 내에서 일예에 불과한 것으로, 본 명세서를 숙지한 당업자라면 다양한 공정조건으로 변형하여 실시할 수 있을 것이고, 이 역시 본 발명의 권리범위내에 속하는 것으로 해석되어야 할 것이다. Although the embodiment of the present invention discloses specific temperature and time conditions with respect to the conditions of the first heating step and the conditions of the second heating step, this is only one example within the spirit of the present invention, it is to be understood the present specification. One skilled in the art will be able to implement a variety of process conditions, which should also be construed as falling within the scope of the invention.
본 발명에 따른 메밀싹으로부터 루틴 추출 방법은 건강에 해로운 알코올 또는 아세톤을 사용하지 않고 단지 물만을 용매로 사용하였기 때문에 루틴을 손쉽게 추출할 수 있고, 이를 식품에 사용하여도 안전할 뿐만 아니라 제조공정이 간단하여 높은 경제성을 갖추고 있다. 또한, 높은 추출 효율로 고농도의 루틴을 추출할 수 있다.The routine extraction method from the buckwheat sprout according to the present invention can easily extract the routine because only water is used as a solvent without using unhealthy alcohol or acetone. It is simple and has high economic feasibility. In addition, it is possible to extract a high concentration of the routine with a high extraction efficiency.
본 발명의 요지와 범위로부터 벗어남이 없이 다양한 수정이나 변형을 하는 것이 당업자에게 가능하다. 따라서 첨부된 특허청구의 범위는 본 발명의 요지에서 속하는 이러한 수정이나 변형을 포함할 것이다.Various modifications and variations are possible to those skilled in the art without departing from the spirit and scope of the invention. Accordingly, the appended claims will cover such modifications and variations as fall within the spirit of the invention.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR19980020507A (en) * | 1996-09-09 | 1998-06-25 | 김진봉 | Method of manufacturing buckwheat processed foods reinforced with rutin |
| KR0154582B1 (en) * | 1995-06-10 | 1998-10-01 | 권태봉 | Method for preparing sprout buckwheat essence |
| KR20020015805A (en) * | 2000-08-23 | 2002-03-02 | 한수길 | Extracting process of highly purified natural rutin from buckwheat |
| KR20050007463A (en) * | 2002-04-30 | 2005-01-18 | 유승삼 | Method of extracting rutin from buck wheat growed by hydroponics |
-
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- 2005-09-27 KR KR1020050089646A patent/KR100708409B1/en not_active IP Right Cessation
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR0154582B1 (en) * | 1995-06-10 | 1998-10-01 | 권태봉 | Method for preparing sprout buckwheat essence |
| KR19980020507A (en) * | 1996-09-09 | 1998-06-25 | 김진봉 | Method of manufacturing buckwheat processed foods reinforced with rutin |
| KR20020015805A (en) * | 2000-08-23 | 2002-03-02 | 한수길 | Extracting process of highly purified natural rutin from buckwheat |
| KR20050007463A (en) * | 2002-04-30 | 2005-01-18 | 유승삼 | Method of extracting rutin from buck wheat growed by hydroponics |
Non-Patent Citations (4)
| Title |
|---|
| 1001545820000 |
| 1019980020507 |
| 1020020015805 |
| 1020050007463 |
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| Publication number | Publication date |
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| KR20070039408A (en) | 2007-04-12 |
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