KR100620786B1 - A spray for indoor air cleaning - Google Patents

A spray for indoor air cleaning Download PDF

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KR100620786B1
KR100620786B1 KR1020050014877A KR20050014877A KR100620786B1 KR 100620786 B1 KR100620786 B1 KR 100620786B1 KR 1020050014877 A KR1020050014877 A KR 1020050014877A KR 20050014877 A KR20050014877 A KR 20050014877A KR 100620786 B1 KR100620786 B1 KR 100620786B1
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extract
antimicrobial
cinnamon
herbs
ginger
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KR20060094169A (en
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양기해
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(주)세기종합환경
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/14Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

Abstract

본 발명은 실내 공기 정화용 스프레이 액에 관한 것으로, 더욱 상세히 설명하면 올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아, 허브에서 추출한 천연 항균 물질을 연소시켜 독한 향과 끈적임을 제거하고 추출하여 완성한 실내공기 정화용 스프레이 액에 관한 것이다. 상기 발명에 의하여 공기 중의 세균을 즉시 제거하며, 인체에 무해하고, 방향성이 우수한 공기정화용 스프레이액이 제조된다. The present invention relates to a spray liquid for indoor air purification, and more specifically, to burn a natural antibacterial material extracted from olives, cinnamon, ginger, pine, algae, spearmint, sweetened oil, tansy chrysanthemum, salvia, herbs, strong flavor and stickiness The present invention relates to a spray liquid for purifying indoor air that has been removed and extracted. According to the present invention, the air purifying spray liquid is immediately removed, harmless to the human body, and excellent in directionality.

정화, 방향성, 스프레이액. Cleansing, fragrances, sprays.

Description

실내 공기 정화용 스프레이액{A SPRAY FOR INDOOR AIR CLEANING} Spray liquid for indoor air purification {A SPRAY FOR INDOOR AIR CLEANING}

본 발명은 실내 공기 정화용 스프레이 액에 관한 것으로, 더욱 상세히 설명하면 올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아, 허브에서 추출한 천연 항균 물질을 연소시켜 독한 향과 끈적임을 제거하고 추출하여 완성한 실내공기 정화용 스프레이 액에 관한 것이다. The present invention relates to a spray liquid for indoor air purification, and more specifically, to burn a natural antibacterial material extracted from olives, cinnamon, ginger, pine, algae, spearmint, sweetened oil, tansy chrysanthemum, salvia, herbs, strong flavor and stickiness The present invention relates to a spray liquid for purifying indoor air that has been removed and extracted.

근래 대기 오염의 심화로 도심지역에서는 가정, 공공장소를 불문하고 기계식 공기정화기를 설치하고 있는 추세이다. 공기정화기는 실내 공기 중에 기도로 흡수되어 호흡기 질환을 유발시킬 수 있는 미세 입자를 제거하기 위한 것으로, 수미크론 이하의 유해균을 제거할 수는 없다. 또한 항균 필터를 사용하여 상기와 같은 유해균 해결하고 있다고 하나 그 효과가 미미하여 실내 항균 및 유해균 제거는 여전히 방향제 혹은 스프레이제를 사용하여 행하고 있다. 이중 방향제는 장기에 걸쳐 서서히 균일한 공기 정화효과를 보기위한 것이나, 스프레이제는 실내 오염이 심할 경우 오염물질에 직접적으로 강력히 대응하기 위한 수단으로서 사용되고 있다. Recently, due to the deepening of air pollution, mechanical air purifiers are being installed in urban areas regardless of homes or public places. An air purifier is used to remove fine particles that can be absorbed into the airways into the airways and cause respiratory diseases. It cannot remove harmful bacteria below several microns. In addition, antibacterial filter is used to solve the above harmful bacteria, but the effect is insignificant, and indoor antibacterial and harmful bacteria removal is still performed using a fragrance or spray agent. Dual fragrances are used to achieve a uniform air purification effect over a long period of time, but spray agents are used as a means to respond directly to the pollutants when the indoor pollution is severe.

상기의 스프레이제와 관련하여 현재 시중에 생산, 판매되고 있는 대부분의 물질은 단순한 방향성분을 첨가하기 위한 것이 대부분으로 실상은 방향제 이상의 큰 효과를 내지 못하며, 공기정화 효과도 미흡한 것이 사실이다.With regard to the above spraying agent, most of the materials currently produced and sold on the market are mainly for adding simple fragrance components, and in fact, they do not have a greater effect than the fragrance, and the air purification effect is also insufficient.

본 발명에서는 상기의 문제점을 극복하기 위한 방편으로 천연항균 물질로 올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아, 허브를 이용하였다. 상기 수종중 올리브,계피,생강,소나무,이질풀의 추출물은 각각 대장균, 장티프스균등 광범위한 세균에 대하여 강한 살균력을 보이며 스피어민트, 감송유, 쑥국화, 샐비아, 허브는 전자의 수종보다 살균력은 조금 떨어지나 휘발성이 강하여 본 발명의 휘발성 항균제 제조에 적합하다. 전술한 우수한 성능에 불구하고 상기 수종에서 추출한 액상 물질들은 점도가 높고 끈적임이 심하여 바로 항균용 스프레이 액으로 제조하기 힘들다. 따라서 급속히 고온연소 시켜 상기의 고 점도 성분을 제거하여 항균성분만 이용하였다.In the present invention, as a means for overcoming the above problems, olive, cinnamon, ginger, pine, algae, spearmint, persimmon oil, tansy chrysanthemum, salvia, herbs as a natural antibacterial material. Extracts of olives, cinnamon, ginger, pine and dysentery among the species show strong bactericidal activity against a wide range of bacteria, such as Escherichia coli and typhoid bacteria, respectively. It is strong and suitable for producing the volatile antimicrobial agent of the present invention. Despite the excellent performance described above, the liquid materials extracted from the species are high in viscosity and sticky, and thus hard to be prepared as an antibacterial spray liquid. Therefore, the high temperature component was rapidly burned to remove the high viscosity component, and only the antibacterial component was used.

본 발명은 상기와 같은 종래의 문제점을 해결하기 위한 것으로서, 본 발명의 목적은 방향효과와 아울러 실내의 유해균을 신속히 제거하기 위한 실내 공기정화용 천연 항균 스프레이제를 제공하는 데 있다. The present invention is to solve the above-mentioned conventional problems, an object of the present invention to provide a natural antibacterial spray for indoor air purification to quickly remove harmful bacteria in the room as well as aroma effect.

이하 본 발명을 상세히 설명한다. Hereinafter, the present invention will be described in detail.

본 발명의 스프레이의 제조방법은 다음과 같다.The manufacturing method of the spray of this invention is as follows.

올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아, 허브 를 수처리에 의해 세척하여 이물질을 제거하고;Olives, cinnamon, ginger, pine, algae, spearmint, sauerkraut, tansy, salvia and herbs by water treatment to remove debris;

상기 세척된 항균 수종을 열풍 건조하고;Hot air drying the washed antibacterial species;

상기 열풍 건조된 올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아를 고온에서 급속히 연소시키고;Rapidly burning the hot air dried olives, cinnamon, ginger, pine, algae, spearmint, persimmon oil, tansy, and salvia at high temperature;

상기 연소된 항균수종과 허브를 일정크기로 절단하고 에탄올을 첨가하여 일정기간 숙성시키고;Cutting the burned antimicrobial species and herbs to a certain size and aging for a certain period by adding ethanol;

상기 숙성된 항균추출물을 원심분리하여 하층부의 항균추출물을 채취하고;Centrifuging the aged antimicrobial extract to obtain an antimicrobial extract in the lower layer;

상기 채취된 항균추출물을 액체 컬럼 크로마토그래피에서 시클로헥산(Cyclohexane,pH 7.5)을 용리액으로 하여 분리추출하고;Separating and extracting the collected antimicrobial extract by using cyclohexane (Cyclohexane, pH 7.5) as an eluent in liquid column chromatography;

상기 분리추출액을 원심분리하여 하층부의 항균추출물을 분리하고;Centrifuging the separated extract to separate the antimicrobial extract from the lower layer;

상기 분리된 항균추출물에 5~15% 농도의 에탄올 수용액과 분사용 가스를 혼합하여 공기정화용 스프레이제를 완성한다.5 to 15% concentration of the ethanol aqueous solution and the injection gas to the separated antimicrobial extract to complete the air purification spray agent.

상기 항균 수종의 연소는 특유의 독한 향과 끈적임을 유발하는 성분을 제거하기 위한 것으로 유요성분이 파괴되지 않도록 탄화가 일어나기 직전까지만 연소하여야 한다. 따라서 실험에 의하면 연소 온도는 500~700℃, 연소시간은 10~20분 사이가 최적이다.Combustion of the antimicrobial species is to remove the components causing the unique strong flavor and stickiness should be burned only until just before the carbonization occurs so that the active ingredients are not destroyed. Therefore, according to the experiment, the combustion temperature is optimal between 500 ~ 700 ℃ and the combustion time is 10 ~ 20 minutes.

상기 항균수종의 에탄올 추출에 있어서 에탄올은 30~60%의 것을 사용하며 실험에 의하면 이때 효율이 최대가 되는 것으로 나타났다. 상기 에탄올에 의한 숙성은 30~50일 사이로 한다. 30일 이하이면 숙성이 미진하며, 50일이면 숙성이 거의 마무리되어 기간을 연장 한다고 해도 수율의 향상을 기대할 수 없다.In the ethanol extraction of the antimicrobial species, ethanol is used in 30 ~ 60% of the experiments showed that the efficiency is the maximum at this time. Maturation with the ethanol is made between 30 to 50 days. If it is 30 days or less, the aging is insufficient, and if it is 50 days, the aging is almost finished, and even if the period is extended, the yield cannot be improved.

상기 원심분리는 2000G~3000G 사이가 적당하다. 2000G 이하이면 분리가 미진하고, 3000G 이상에서는 분리도의 별다른 변화가 없는 것으로 나타났다.The centrifugation is suitably between 2000G and 3000G. If it is less than 2000G, separation is inadequate, and if it is more than 3000G, there is no change in separation degree.

이하 실시예를 설명한다. Examples will be described below.

실시예. 1Example. One

올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아, 허브를 물 고압 분사하여 이물질을 제거하고 열풍 건조시킨후 노에서 700℃의 온도에서 10분간 연소시켰다. 상기 연소된 항균추출물과 허브를 50% 에탄올 용액에 담그고, 50일간 숙성하였다. 상기 숙성액을 3000G로 1시간 동안 원심분리하여 하층액을 분리하고 고성능액체크로마토그래피에 알루미나를 충전하고 pH 7.5의 시클로헥산을 용리액으로 하여 상기 항균추출물을 정제하였다. 상기 정제액을 2.500G에서 1시간 동안 다시 원심분리하여 하층액을 분리하였다. 상기 분리된 하층액 500g에 50%에탄올 5g을 첨가하고 LPG 개스 10g을 첨가하여 스프레이액을 완성하였다.Olives, cinnamon, ginger, pine, algae grass, spearmint, sweetened oil, tansy, sage, and herbs were sprayed with water under high pressure to remove foreign matters and hot-air dried, and then burned in a furnace at a temperature of 700 ° C. for 10 minutes. The burned antibacterial extract and herbs were soaked in 50% ethanol solution and aged for 50 days. The antimicrobial extract was purified by centrifuging the aging solution at 3000G for 1 hour to separate the lower layer solution, filling high-performance liquid chromatography with alumina, and using a pH 7.5 cyclohexane as an eluent. The purified solution was centrifuged again at 2.500 G for 1 hour to separate the lower layer solution. To 500 g of the separated lower layer solution, 5 g of 50% ethanol was added, and 10 g of LPG gas was added to complete the spray solution.

상술한 바와 같이 본 발명에 따른 스프레이액은 공기 중의 세균을 즉시 제거하며, 인체에 무해하고, 방향성이 우수한 공기정화용 스프레이액이다. As described above, the spray liquid according to the present invention is an air purifying spray liquid that immediately removes bacteria in the air, is harmless to the human body, and has excellent directionality.

Claims (1)

올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아, 허브를 수처리에 의해 세척하여 이물질을 제거하고; Olives, cinnamon, ginger, pine, algae, spearmint, condensed oil, tansy, sage, and herbs by water treatment to remove foreign substances; 상기 세척된 항균 수종을 열풍 건조하고;  Hot air drying the washed antibacterial species; 상기 열풍 건조된 올리브, 계피, 생강, 소나무, 이질풀, 스피어민트, 감송유, 쑥국화, 샐비아를 500~700℃에서 10~20분간 연소시키고;  Burning the hot air dried olives, cinnamon, ginger, pine, algae, spearmint, persimmon oil, tansy, salvia for 10-20 minutes at 500 ~ 700 ℃; 상기 연소된 항균수종과 허브를 일정크기로 절단하고 30~60%의 에탄올 수용액을 첨가하여 30~50일간 숙성시키고;  Cutting the burned antimicrobial species and herbs to a certain size and aged for 30 to 50 days by adding 30-60% ethanol aqueous solution; 상기 숙성된 항균추출물을 2,000~3,000G 로 원심분리하여 하층부의 항균추출물을 채취하고;  Centrifuging the aged antimicrobial extract at 2,000-3,000 G to collect the antimicrobial extract at the bottom; 상기 채취된 항균추출물을 액체 컬럼크로마토그래피에서 시클로헥산(pH 7.5)을 용리액으로 하여 휘발성항균성분을 분리추출하고;  Extracting the volatile antimicrobial component from the collected antibacterial extract by using cyclohexane (pH 7.5) as an eluent in liquid column chromatography; 상기 분리추출액을 2,000~3,000G 로 원심분리하여 하층부의 항균추출물을 분리하고;  Centrifuging the separated extract at 2,000-3,000 G to separate the antimicrobial extract from the lower layer; 상기 분리된 항균추출물에 5~15% 농도의 에탄올 수용액과 분사용 가스를 혼합하여 제조되는 것을 특징으로 하는 공기정화용 스프레이액.  Spraying for air purification, characterized in that the prepared antibacterial extract by mixing a 5 to 15% concentration of ethanol aqueous solution and the injection gas.
KR1020050014877A 2005-02-23 2005-02-23 A spray for indoor air cleaning KR100620786B1 (en)

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