KR100512880B1 - Appartus for producing a dyes from a leaf and method of the same - Google Patents
Appartus for producing a dyes from a leaf and method of the same Download PDFInfo
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- KR100512880B1 KR100512880B1 KR10-2003-0022072A KR20030022072A KR100512880B1 KR 100512880 B1 KR100512880 B1 KR 100512880B1 KR 20030022072 A KR20030022072 A KR 20030022072A KR 100512880 B1 KR100512880 B1 KR 100512880B1
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- extract
- plant
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- leaves
- dye
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- 239000000975 dye Substances 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title abstract description 25
- 241000196324 Embryophyta Species 0.000 claims abstract description 49
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 41
- 239000000284 extract Substances 0.000 claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 claims abstract description 23
- 239000000835 fiber Substances 0.000 claims abstract description 21
- 239000000463 material Substances 0.000 claims abstract description 17
- 238000002156 mixing Methods 0.000 claims abstract description 17
- 239000000126 substance Substances 0.000 claims abstract description 15
- 229930182559 Natural dye Natural products 0.000 claims abstract description 13
- 239000000978 natural dye Substances 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 10
- 230000000144 pharmacologic effect Effects 0.000 claims abstract description 10
- 238000001179 sorption measurement Methods 0.000 claims abstract description 10
- 239000010419 fine particle Substances 0.000 claims abstract description 8
- 239000002245 particle Substances 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 5
- 239000000419 plant extract Substances 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000003086 colorant Substances 0.000 claims abstract description 3
- 238000003825 pressing Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims 1
- 238000010298 pulverizing process Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 238000004043 dyeing Methods 0.000 abstract description 19
- 239000004744 fabric Substances 0.000 abstract description 4
- 238000009835 boiling Methods 0.000 abstract description 2
- 239000012530 fluid Substances 0.000 description 5
- 240000006891 Artemisia vulgaris Species 0.000 description 4
- 235000003261 Artemisia vulgaris Nutrition 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000009792 diffusion process Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000002351 wastewater Substances 0.000 description 4
- 239000002131 composite material Substances 0.000 description 2
- 239000002781 deodorant agent Substances 0.000 description 2
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 description 1
- 235000003097 Artemisia absinthium Nutrition 0.000 description 1
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 description 1
- 235000011201 Ginkgo Nutrition 0.000 description 1
- 235000008100 Ginkgo biloba Nutrition 0.000 description 1
- 244000194101 Ginkgo biloba Species 0.000 description 1
- 235000010643 Leucaena leucocephala Nutrition 0.000 description 1
- 240000007472 Leucaena leucocephala Species 0.000 description 1
- 241000218206 Ranunculus Species 0.000 description 1
- 239000002156 adsorbate Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000001138 artemisia absinthium Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
본 발명은 식물잎을 이용한 섬유 염료 제조장치 및 그 방법에 관한 것으로, 식물의 고유 약리기능을 유지하면서, 그 염색 색상을 자유롭게 선택할 수 있도록 식물잎의 액기스에서 투명 추출액을 취출하고, 다양한 염료를 배합하여 소망하는 색상으로 직물을 염색할 수 있게 한 식물잎을 이용한 섬유 염료 제조장치 및 그 방법을 제공함에 그 목적이 있다. The present invention relates to a fiber dye manufacturing apparatus and method using the plant leaves, while maintaining the inherent pharmacological function of the plant, extracting the transparent extract from the extract of the plant leaves to freely select the dyeing color, and mixes various dyes It is an object of the present invention to provide a fiber dye production apparatus and method using the plant leaves that can dye the fabric in the desired color.
본 발명은 채취한 식물의 잎을 깨끗하게 세정하고, 물에 데쳐서 최소 입도로 분쇄하는 과정과; 분쇄물질을 제 1 가압펌프에 인입시키고 가압하여 액상의 추출액을 추출하는 과정과; 추출액을 80 mesh로 이루어진 제 1 여과기를 통과시켜 여과하는 과정과; 미립자로 여과된 추출액을 반응탱크에 인입시켜 활성탄의 흡착작용에 의해 천연염료를 제거하는 과정과; 반응탱크를 통과한 물질을 제 2 가압펌프에 투입하여 2차 가압하는 과정과; 상기 가압펌프를 통과한 물질을 120 mesh로 이루어진 제 2 여과기에 투입하여 2차 여과하는 과정과; 2차 여과된 물질을 1㎛의 제 3 여과기에 투입하여 3차 여과하는 과정과; 얻어진 투명 식물 추출액과 화학안료를 혼합 탱크에 각각 투입하여 혼합 교반시키는 과정으로 이루어진 것을 특징으로 한다.The present invention cleans the leaves of the harvested plant, the process of crushing to a minimum particle size by boiling in water; Extracting the liquid extract by introducing the pulverized material into the first pressurizing pump and pressurizing it; Filtering the extract through a first filter made of 80 mesh; Removing the natural dye by introducing an extract filtered through the fine particles into a reaction tank by adsorption of activated carbon; Putting the material that has passed through the reaction tank into a second pressurizing pump and performing secondary pressurization; Putting the material that has passed through the pressure pump into a second filter made of 120 mesh and performing secondary filtration; Subjecting the second filtered material to a third filter having a thickness of 1 μm and performing third filtering; It is characterized by consisting of a process of mixing and stirring the obtained transparent plant extract and the chemical pigment to each mixing tank.
본 발명을 적용하면, 다양한 식물잎에 포함되는 천연염료를 제거하고, 그 약리작용을 행하는 기능성물질은 제거하지 않은 상태에서, 해당 추출액에 화학염료를 혼합함으로써 해당 식물잎의 고유 색상이 아닌 다양한 색상처리를 행할 수 있게 되고, 그 약리기능을 그대로 보존할 수 있게 한 염료제조방법을 제공하게 되는 효과가 있다.Applying the present invention, by removing the natural dyes contained in the various plant leaves, and without removing the functional material that performs the pharmacological action, by mixing the chemical dyes in the extract, various colors other than the intrinsic color of the plant leaves It is effective to provide a dye production method which enables the treatment to be carried out, and the pharmacological function thereof can be preserved as it is.
Description
본 발명은 식물잎을 이용한 섬유 염료 제조장치 및 그 방법에 관한 것으로, 보다 상세하게 식물의 고유 약리기능을 유지하면서, 그 염색 색상을 자유롭게 선택할 수 있도록 식물잎의 액기스에서 투명 추출액을 취출하고, 다양한 염료를 배합하여 소망하는 색상으로 직물을 염색할 수 있게 한 식물잎을 이용한 섬유 염료 제조장치 및 그 방법에 관한 것이다.The present invention relates to a fiber dye manufacturing apparatus using the plant leaves and a method thereof, and more particularly, while maintaining the inherent pharmacological function of the plant, and extracting the transparent extract from the extract of the plant leaves to freely select the dyeing color, The present invention relates to a fiber dye manufacturing apparatus using plant leaves and a method for dyeing fabrics in a desired color by blending dyes.
주지된 바와 같이, 염색방법에는 화학염색법과 천연염료로 염색하는 천연염색방법이 있다. 현재까지 의류에 사용되는 일반적인 염색방법 중 화학염료를 사용한 화학염색법으로 이는 색상이 선명하게 나타난다는 장점이 있으나, 염색후에 생성되는 폐수로 인하여 심각한 수질오염을 야기한다는 문제점이 있다. As is well known, the dyeing method includes a chemical dyeing method and a natural dyeing method of dyeing with natural dyes. Chemical dyeing method using a chemical dye of the general dyeing method used in clothing until now has the advantage that the color appears clearly, but there is a problem that causes serious water pollution due to the waste water generated after dyeing.
이와 같은 문제를 해결하기 위해서 염색후 생성되는 폐수를 정화하기 위한 여러가지 노력이 있었으나 이를 근본적으로 해결하지는 못하고 있다. In order to solve this problem, various efforts have been made to purify the wastewater generated after dyeing, but this has not been fundamentally solved.
이에, 폐수를 방출하지 않아서 화학염색법을 대처할 수 있는 천연염색방법에 관심이 증대되고 이에 대해서 연구가 진행된 결과, 천연염색방법은 폐수를 방출하지 않아 환경 친화적이라는 점이외에 사용되는 염재자체가 천연의 재료이므로 피부에 문제를 일으키지 않으며, 사용되는 염재에 따라 원적외선을 방사하거나 소취, 방취의 기능을 갖을 뿐 아니라 그 색도도 자연스럽고 아름답다는 것이 알려지게 되면서 천연염색방법으로 염색된 의류에 대해서 소비자들의 수요가 증대되고 있으며 이에 천연염색방법으로 의류를 제작하는 업체가 증가하고 있는 상황이다. Therefore, interest in natural dyeing methods that can cope with the chemical dyeing method by not releasing wastewater has increased, and as a result of research, the natural dyeing method is environmentally friendly because it does not discharge wastewater. Therefore, it does not cause skin problems, and it is known that not only does it emit far infrared rays, deodorant and deodorant, but also its color is natural and beautiful according to the dyeing materials used. There is a growing number of companies that manufacture clothing by the natural dyeing method.
그러나, 이와 같은 천연염색방법은 주로 식물 등에서 추출한 염료를 이용하여 염색을 행하게 되는 데, 이러한 천연염색방법은 식물의 고유색 때문에 우아한 색상을 연출하기도 하지만, 반면에 식물의 고유색 때문에 그 색이 한정될 수 밖에 없다는 문제가 있었다. However, such a natural dyeing method is mainly to dye using a dye extracted from plants, such natural dyeing method may produce an elegant color due to the intrinsic color of the plant, while the color may be limited due to the intrinsic color of the plant There was only a problem.
즉, 예컨대 쑥같은 식물의 잎을 이용한 염색시 그 쑥이 갖는 효능을 가지면서 쑥색상외의 다른 색상으로 직물을 염색할 수 없다는 한계가 있었다. That is, for example, when the dye using the leaves of the plant, such as mugwort had the effect that the mugwort had a limit that can not dye the fabric in a color other than mugwort color.
본 발명은 상기한 종래 기술의 사정을 감안하여 이루어진 것으로, 식물의 고유 약리기능을 유지하면서, 그 염색 색상을 자유롭게 선택할 수 있도록 식물잎의 액기스에서 투명 추출액을 취출하고, 다양한 염료를 배합하여 소망하는 색상으로 직물을 염색할 수 있게 한 식물잎을 이용한 섬유 염료 제조장치 및 그 방법을 제공함에 그 목적이 있다.The present invention has been made in view of the above-described state of the art, and while maintaining the inherent pharmacological function of the plant, the transparent extract is extracted from the extract of the plant leaves so that the dyeing color can be freely selected, and various dyes are combined and desired. It is an object of the present invention to provide an apparatus and a method for producing a fiber dye using plant leaves that can dye a fabric in color.
상기한 목적을 달성하기 위해, 본 발명의 바람직한 실시예에 따르면 식물의 잎 등을 펌프에 인입시켜 가압함으로써 그 잎 등으로부터 미립자의 추출액을 추출하기 위한 제 1, 2 가압펌프와; 상기 가압펌프로부터 추출된 미립자액을 여과시키기 위한 제 1, 2, 3 여과기와; 제 1 여과기를 통과한 추출액으로부터 천연염료를 제거시키기 위해 내부에 활성탄층이 구성된 반응탱크와; 상기 반응탱크에서 천연염료가 제거된 추출액을 기타 화학염료와 혼합하여 교반시키기 위한 혼합 탱크로 구성되어 식물잎으로부터 투명 기능성 추출액을 추출하고, 소망하는 안료를 첨가함으로써 고유 약리기능은 유지하면서 다양한 색상의 염료를 제조하는 것을 특징으로 하는 식물잎을 이용한 섬유 염료 제조장치가 제공된다.In order to achieve the above object, according to a preferred embodiment of the present invention, the first and second pressure pumps for extracting the extract of the fine particles from the leaves and the like by pressing the leaves and the like of the plant into the pump; First, second and third filters for filtering the particulate liquid extracted from the pressure pump; A reaction tank having an activated carbon layer therein for removing natural dyes from the extract liquid passing through the first filter; The reaction tank consists of a mixing tank for mixing and stirring the natural dye-free extracts with other chemical dyes to extract the transparent functional extract from the plant leaves, and by adding the desired pigment, while maintaining the inherent pharmacological function of various colors There is provided a fiber dye production apparatus using plant leaves, characterized in that to produce a dye.
바람직하게, 상기 제 1, 2, 3 여과기는 각각 80메쉬, 120 메쉬, 1 ㎛로 이루어진 것을 특징으로 하는 식물잎을 이용한 섬유 염료 제조장치가 제공된다.Preferably, the first, second, third filter is provided with a fiber dye production apparatus using a plant leaf, characterized in that consisting of 80 mesh, 120 mesh, 1 ㎛ each.
바람직하게, 상기 반응탱크는 내측벽에 온도센서가 구성되고, 그 온도센서의 후면에 히터선이 장입된 것을 특징으로 하는 식물잎을 이용한 섬유 염료 제조장치가 제공된다.Preferably, the reaction tank is provided with a fiber dye production apparatus using a plant leaf, characterized in that the temperature sensor is configured on the inner wall, the heater wire is inserted into the rear of the temperature sensor.
바람직하게, 상기 반응탱크의 내부온도는 상시 50℃∼95℃를 유지하도로 하는 것을 특징으로 하는 식물잎을 이용한 섬유 염료 제조장치가 제공된다.Preferably, the internal temperature of the reaction tank is provided with a fiber dye production apparatus using a plant leaf, characterized in that to maintain a constant 50 ℃ to 95 ℃.
바람직하게, 상기 반응탱크 내부에 안착된 활성탄은 전체 반응탱크 면적의 3.3%를 점유하도록 구성된 것을 특징으로 하는 식물잎을 이용한 섬유 염료 제조장치가 제공된다.Preferably, there is provided an apparatus for producing fiber dye using plant leaves, wherein the activated carbon seated inside the reaction tank is configured to occupy 3.3% of the total reaction tank area.
한편, 본 발명은 채취한 식물의 잎을 깨끗하게 세정하고, 물에 데쳐서 최소 입도로 분쇄하는 과정과; 분쇄물질을 제 1 가압펌프에 인입시키고 가압하여 액상의 추출액을 추출하는 과정과; 추출액을 80 mesh로 이루어진 제 1 여과기를 통과시켜 여과하는 과정과; 미립자로 여과된 추출액을 반응탱크에 인입시켜 활성탄의 흡착작용에 의해 천연염료를 제거하는 과정과; 반응탱크를 통과한 물질을 제 2 가압펌프에 투입하여 2차 가압하는 과정과; 상기 가압펌프를 통과한 물질을 120 mesh로 이루어진 제 2 여과기에 투입하여 2차 여과하는 과정과; 2차 여과된 물질을 1㎛의 제 3 여과기에 투입하여 3차 여과하는 과정과; 얻어진 투명 식물 추출액과 화학안료를 혼합 탱크에 각각 투입하여 혼합 교반시키는 과정으로 이루어진 것을 특징으로 하는 식물잎을 이용한 섬유 염료 제조방법이 제공된다. On the other hand, the present invention cleans the leaves of the collected plant, and the process of crushing to a minimum particle size by boiling in water; Extracting the liquid extract by introducing the pulverized material into the first pressurizing pump and pressurizing it; Filtering the extract through a first filter made of 80 mesh; Removing the natural dye by introducing an extract filtered through the fine particles into a reaction tank by adsorption of activated carbon; Putting the material that has passed through the reaction tank into a second pressurizing pump and performing secondary pressurization; Putting the material that has passed through the pressure pump into a second filter made of 120 mesh and performing secondary filtration; Subjecting the second filtered material to a third filter having a thickness of 1 μm and performing third filtering; Provided are a method for producing a fiber dye using plant leaves, comprising the steps of mixing and stirring the obtained transparent plant extracts and chemical pigments into a mixing tank, respectively.
이하, 본 발명에 대해 도면을 참조하여 상세하게 설명한다.EMBODIMENT OF THE INVENTION Hereinafter, this invention is demonstrated in detail with reference to drawings.
도 1은 본 발명의 일실시예에 따른 식물잎을 이용한 섬유 염료 제조장치의 개략적인 구성을 나타내는 블록구성도이다.1 is a block diagram showing a schematic configuration of a fiber dye production apparatus using a plant leaf according to an embodiment of the present invention.
이를 참조하면, 본 발명의 일실시예에 따른 식물잎을 이용한 섬유 염료 제조장치(100)는 식물의 잎 등을 펌프에 인입시켜 가압함으로써 그 잎 등으로부터 미립자의 추출액을 추출하기 위한 복수개의 가압펌프(10, 40)와; 상기 가압펌프(10)로부터 추출된 미립자액을 여과시키기 위한 3개의 여과기(20, 50, 60)와; 제 1 여과기(30)를 통과한 추출액으로부터 천연염료를 제거시키기 위해 내부에 활성탄층이 구성된 반응탱크(30)와; 반응탱크(30)에서 천연염료가 제거된 추출액을 기타 화학염료와 혼합하여 교반시키기 위한 혼합 탱크(70)로 구성되어져 있다.Referring to this, the fiber dye manufacturing apparatus 100 using a plant leaf according to an embodiment of the present invention is a plurality of pressurized pump for extracting the extract of the fine particles from the leaf, such as by pressing the leaf of the plant into the pump (10, 40); Three filters (20, 50, 60) for filtering the particulate liquid extracted from the pressure pump (10); A reaction tank 30 having an activated carbon layer therein for removing natural dyes from the extract liquid having passed through the first filter 30; The reaction tank 30 is composed of a mixing tank 70 for mixing and stirring the extract from which the natural dye is removed.
이때, 상기 가압펌프(10, 40)는 복수개로 구성되어 상기 반응탱크(30)의 전단과 후단에 각각 구성되어져 있으며, 제 1 여과기(20)는 80 mesh로, 제 2, 3 여과기(50, 60)는 제 2 가압펌프(40)의 후단에 각각 구성되며 120 mesh와, 1㎛로 각각 구성된다.At this time, the pressure pump (10, 40) is composed of a plurality of the front and rear ends of the reaction tank 30, respectively, the first filter 20 is 80 mesh, the second, third filter (50, 60 is respectively configured at the rear end of the second pressure pump 40 and 120 mesh and 1 μm, respectively.
또한, 상기 반응탱크(30)는 그 내부 바닥면에 활성탄층(32)이 구성되어져 있는 바, 활성탄(도시 생략)이 그 활성탄층(32)에 안착되어져 있으며, 활성탄은 graphite 구조의 미세 결정이 불규칙하게 분산하는 부분과 메칠렌 고리 부분이 공존한다. 또, 내부세공 구조가 발달해서 3,000㎡/g 에 달하는 뚜렷하게 커다란 비표면적을 갖는다.In addition, the reaction tank 30 has an activated carbon layer 32 formed on its inner bottom surface, and activated carbon (not shown) is deposited on the activated carbon layer 32, and the activated carbon has fine crystals of graphite structure. An irregularly dispersed portion and a methylene ring portion coexist. In addition, the internal pore structure is developed to have a distinctly large specific surface area of 3,000 m 2 / g.
활성탄은 장시간에 걸쳐 유체상에 고체 표면이 접촉하고 있으면 유체상의 특정성분은 고체 표면에 모이고 유체상 내부의 농도와 고체표면의 농도가 다른 상태가 된다. 이 현상이 흡착(Adsorption)이며, 이때 유체상 중의 농도와 고체 표면 농도의 관계는 양상(兩相)의 화학 포텐셜이 알맞으면 평형을 이루고 흡착 평형관계(Adsorption Equilibrium Relation)라 불리우는 관계가 성립한다.When activated carbon is in contact with a solid surface in a fluid phase for a long time, certain components of the fluid phase are collected on the solid surface and the concentration of the inside of the fluid phase is different from that of the solid surface. This phenomenon is Adsorption, where the relationship between the concentration in the fluid phase and the solid surface concentration is balanced if the chemical potential of the phase is appropriate and a relationship called Adsorption Equilibrium Relation is established.
또한, 이러한 관계는 온도에 많은 영향을 받게 된다. 활성탄에서의 흡착은 다음과 같은 원리에 의해서 이루어진다. 활성탄 입자는 흡착을 지배하는 마이크로(Micro)세공(2nm이하)과 마이크로 입자의 간극으로 된 매크로(Macro)세공(수 ㎛)의 2원적인 구조를 갖고 있다. 입상 활성탄의 지름은 수 mm이고 이 입자 내부의 흡착점에 입자 외부로부터 흡착질 분자가 확산되어 도달해 가기 때문에 여러 가지 경로를 거쳐 흡착이 이루어진다. 매크로 세공 내부를 채우고 있는 유체 가운데로 확산에 의해 이동되고, 마이크로 세공 내를 확산해서 흡착되는 직렬형 확산이 그중 하나이다. 또 하나의 확산 형태는 흡착제 내부의 표면 위를 흡착상태의 분자가 인접하는 흡착점으로 이동하는 표면확산(Surface Diffusion)이다.In addition, this relationship is much influenced by temperature. Adsorption on activated carbon is carried out by the following principle. Activated carbon particles have a dual structure of micropores (2 nm or less) that dominate the adsorption and macropores (several micrometers) formed as a gap between the microparticles. The diameter of the granular activated carbon is several mm, and since the adsorbate molecules diffuse and reach the adsorption point inside the particles, adsorption is carried out through various paths. One of them is a series diffusion which is moved by diffusion into the fluid filling the macropores and diffuses and adsorbs within the micropores. Another type of diffusion is Surface Diffusion, in which the molecules in the adsorbed state move to the adjacent adsorption point on the surface inside the adsorbent.
상기한 활성탄층(32)은 온도와 밀접한 관계를 가지므로 본 발명에서는 상기 반응탱크(30)의 내부가 일정 온도 예컨대, 50℃∼95℃를 유지할 수 있도록 내측벽에 온도센서(34)가 부착되어져 있으며 그 측벽에 히터선(36)이 장입되어져 있다.Since the activated carbon layer 32 has a close relationship with temperature, in the present invention, the temperature sensor 34 is attached to the inner wall so that the inside of the reaction tank 30 can maintain a constant temperature, for example, 50 ° C to 95 ° C. The heater wire 36 is inserted in the side wall.
따라서, 온도센서(34)로부터 검출된 온도가 기설정 온도범위인 50℃∼95℃보다 낮은 온도이거나 높은 온도일 경우 설정온도 50℃∼95℃를 상시 유지할 수 있도록 상기 히터선(36)을 구동시키도록 한다. 활성탄은 전체 반응탱크(30)의 3.3% 중량이 되도록 한다.Therefore, when the temperature detected from the temperature sensor 34 is lower or higher than the preset temperature range of 50 ° C to 95 ° C, the heater wire 36 is driven so as to maintain the set temperature of 50 ° C to 95 ° C at all times. Let's do it. Activated carbon is 3.3% by weight of the total reaction tank (30).
도 2는 본 발명의 일실시예에 따른 식물잎을 이용한 섬유 염료 제조장치를 통해 복합 염료를 제조하는 공정을 도시한 공정도이다.Figure 2 is a process diagram showing a process for producing a composite dye through a fiber dye manufacturing apparatus using a plant leaf according to an embodiment of the present invention.
먼저, 채취한 식물의 잎을 깨끗하게 세정하고, 물에 데쳐서 입도 500㎛이하, 바람직하게는 최소 입도로 분쇄하여 본 발명의 일실시예에 따른 식물잎을 이용한 섬유 염료 제조장치(100)의 제 1 가압펌프(10)에 인입시키고 가압하여 액상의 추출액을 추출한다. 이때, 식물의 잎은 쑥, 미나리, 아카시아, 은행 등 인체에 생화학적으로 유익한 식물의 잎을 일컫는다.First, the leaves of the collected plant is cleaned and washed with water, the particle size of 500㎛ or less, preferably pulverized to a minimum particle size of the first fiber dye production apparatus 100 using a plant leaf according to an embodiment of the present invention Into the pressurized pump 10 and pressurized to extract the liquid extract. At this time, the leaves of the plant refers to the leaves of plants that are biochemically beneficial to the human body, such as wormwood, buttercup, acacia, ginkgo.
추출액을 80 mesh로 이루어진 제 1 여과기(20)를 통과시켜 여과하고, 미립자로 여과된 추출액을 상기 반응탱크(30)에 인입시킨다. 반응탱크(30)내의 온도는 상시 50℃∼95℃가 유지되도록 하며, 추출액은 반응탱크(30)내에 안착된 활성탄에 의해 그 천연염료분이 흡착되게 된다. 따라서, 상기 반응탱크(30)를 통과한 추출액은 천연염료가 제거된 식물잎의 투명한 기능성 물질만이 존재하게 된다.The extract is filtered by passing through a first filter (20) made of 80 mesh, the extract filtered by the fine particles is introduced into the reaction tank (30). The temperature in the reaction tank 30 is always maintained at 50 ℃ to 95 ℃, the extract is the natural dye is adsorbed by the activated carbon seated in the reaction tank (30). Therefore, the extract passed through the reaction tank 30 is only a transparent functional material of the plant leaves from which the natural dye is removed.
반응탱크(30)를 통과한 물질은 제 2 가압펌프(40)를 통해 2차 가압되고, 120 mesh로 이루어진 제 2 여과기(50)를 통과하고, 1㎛의 제 3 여과기(60)를 통과하면서 미립자의 투명 식물 추출액이 얻어지게 된다.The material passing through the reaction tank 30 is secondarily pressurized through the second pressure pump 40, passes through the second filter 50 made of 120 mesh, and passes through the third filter 60 having a thickness of 1 μm. A transparent plant extract of fine particles is obtained.
이때, 얻어진 투명 식물 추출액에는 식물잎 자체의 약리 기능물질만이 존재하고, 천연염료가 제거된 상태이므로 희망하는 색상의 화학염료와 혼합하는 혼합 탱크(70)에 각각 인입시키고 혼합 교반한다. 그러면, 천연/화학 혼합 염료가 제조되게 된다. 즉, 색상은 해당 식물잎의 색상과 무관하게 희망하는 색상으로 제조할 수 있으며, 그 기능은 해당 식물잎의 약리기능을 모두 포함할 수 있는 염료액을 제조할 수 있게 되는 것이다.In this case, only the pharmacologically functional substance of the plant leaf itself exists in the obtained transparent plant extract, and since the natural dye is removed, it is introduced into the mixing tank 70 mixing with the chemical dye of the desired color and mixed and stirred. This results in a natural / chemical mixed dye. In other words, the color can be produced in the desired color irrespective of the color of the plant leaf, the function is to be able to produce a dye solution that can include all of the pharmacological function of the plant leaf.
한편, 본 발명의 실시예에 따른 식물잎을 이용한 섬유 염료 제조장치 및 그 방법은 단지 상기한 실시예에 한정되는 것이 아니라 그 기술적 요지를 이탈하지 않는 범위내에서 다양한 변경이 가능하다. On the other hand, the fiber dye production apparatus and method using a plant leaf according to an embodiment of the present invention is not limited to the above embodiment, but various modifications can be made within the scope without departing from the technical gist.
상기한 바와 같이, 본 발명에 따른 식물잎을 이용한 섬유 염료 제조장치 및 그 방법은 다양한 식물잎에 포함되는 천연염료를 제거하고, 그 약리작용을 행하는 기능성물질은 제거하지 않은 상태에서, 해당 추출액에 화학염료를 혼합함으로써 해당 식물잎의 고유 색상이 아닌 다양한 색상처리를 행할 수 있게 되고, 그 약리기능을 그대로 보존할 수 있게 한 염료제조방법을 제공하게 되는 효과가 있다.As described above, the fiber dye production apparatus and method using the plant leaves according to the present invention is to remove the natural dyes contained in the various plant leaves, and the functional material that performs the pharmacological action, in the state without removing the By mixing the chemical dyes it is possible to perform a variety of color processing, not the intrinsic color of the plant leaves, it is effective to provide a dye production method that can preserve the pharmacological function as it is.
도 1은 본 발명의 일실시예에 따른 식물잎을 이용한 섬유 염료 제조장치의 개략적인 구성을 나타내는 블록구성도,1 is a block diagram showing a schematic configuration of a fiber dye production apparatus using a plant leaf according to an embodiment of the present invention,
도 2는 본 발명의 일실시예에 따른 식물잎을 이용한 섬유 염료 제조장치를 통해 복합 염료를 제조하는 공정을 도시한 공정도이다.Figure 2 is a process diagram showing a process for producing a composite dye through a fiber dye manufacturing apparatus using a plant leaf according to an embodiment of the present invention.
*도면의 주요부분에 대한 부호의 설명** Description of the symbols for the main parts of the drawings *
10:제1가압펌프, 20:제1여과기,10: first pressure pump, 20: first filter,
30:반응탱크, 32;활성탄층,30: reaction tank, 32; activated carbon layer,
34:온도센서, 36;히터선,34: temperature sensor, 36; heater wire,
40:제2가압펌프, 50:제2여과기,40: second pressure pump, 50: second filter,
60:제3여과기, 70:혼합탱크.60: 3rd filter, 70: mixing tank.
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