KR100330192B1 - Composition for Dried Bone Extract Powder and Manufacturing Method Thereof - Google Patents
Composition for Dried Bone Extract Powder and Manufacturing Method Thereof Download PDFInfo
- Publication number
- KR100330192B1 KR100330192B1 KR1020000006274A KR20000006274A KR100330192B1 KR 100330192 B1 KR100330192 B1 KR 100330192B1 KR 1020000006274 A KR1020000006274 A KR 1020000006274A KR 20000006274 A KR20000006274 A KR 20000006274A KR 100330192 B1 KR100330192 B1 KR 100330192B1
- Authority
- KR
- South Korea
- Prior art keywords
- bone
- glucosamine
- weight
- powder
- salt
- Prior art date
Links
- 210000000988 bone and bone Anatomy 0.000 title claims abstract description 65
- 239000000843 powder Substances 0.000 title claims abstract description 43
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
- 239000000203 mixture Substances 0.000 title claims abstract description 11
- MSWZFWKMSRAUBD-UHFFFAOYSA-N beta-D-galactosamine Natural products NC1C(O)OC(CO)C(O)C1O MSWZFWKMSRAUBD-UHFFFAOYSA-N 0.000 claims abstract description 38
- MSWZFWKMSRAUBD-IVMDWMLBSA-N 2-amino-2-deoxy-D-glucopyranose Chemical compound N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O MSWZFWKMSRAUBD-IVMDWMLBSA-N 0.000 claims abstract description 35
- 229960002442 glucosamine Drugs 0.000 claims abstract description 32
- 150000003839 salts Chemical class 0.000 claims abstract description 23
- 229920001353 Dextrin Polymers 0.000 claims abstract description 17
- 239000004375 Dextrin Substances 0.000 claims abstract description 17
- 235000019425 dextrin Nutrition 0.000 claims abstract description 17
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229920002101 Chitin Polymers 0.000 claims abstract description 12
- 239000004576 sand Substances 0.000 claims abstract description 12
- 239000006188 syrup Substances 0.000 claims abstract description 8
- 235000020357 syrup Nutrition 0.000 claims abstract description 8
- 229920002472 Starch Polymers 0.000 claims abstract description 7
- 235000019698 starch Nutrition 0.000 claims abstract description 7
- 239000008107 starch Substances 0.000 claims abstract description 7
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 6
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000011709 vitamin E Substances 0.000 claims abstract description 6
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 6
- 229940046009 vitamin E Drugs 0.000 claims abstract description 6
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 4
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 4
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 235000015278 beef Nutrition 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 9
- 238000001694 spray drying Methods 0.000 claims description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 159000000007 calcium salts Chemical class 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 229930003799 tocopherol Natural products 0.000 claims description 4
- 229960001295 tocopherol Drugs 0.000 claims description 4
- 239000011732 tocopherol Substances 0.000 claims description 4
- 235000010384 tocopherol Nutrition 0.000 claims description 4
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 3
- 239000008213 purified water Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- QCQCHGYLTSGIGX-GHXANHINSA-N 4-[[(3ar,5ar,5br,7ar,9s,11ar,11br,13as)-5a,5b,8,8,11a-pentamethyl-3a-[(5-methylpyridine-3-carbonyl)amino]-2-oxo-1-propan-2-yl-4,5,6,7,7a,9,10,11,11b,12,13,13a-dodecahydro-3h-cyclopenta[a]chrysen-9-yl]oxy]-2,2-dimethyl-4-oxobutanoic acid Chemical compound N([C@@]12CC[C@@]3(C)[C@]4(C)CC[C@H]5C(C)(C)[C@@H](OC(=O)CC(C)(C)C(O)=O)CC[C@]5(C)[C@H]4CC[C@@H]3C1=C(C(C2)=O)C(C)C)C(=O)C1=CN=CC(C)=C1 QCQCHGYLTSGIGX-GHXANHINSA-N 0.000 claims 1
- 210000001185 bone marrow Anatomy 0.000 abstract description 7
- 241000234282 Allium Species 0.000 abstract description 5
- 235000002732 Allium cepa var. cepa Nutrition 0.000 abstract description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 5
- 239000011575 calcium Substances 0.000 abstract description 5
- 229910052791 calcium Inorganic materials 0.000 abstract description 5
- 239000000047 product Substances 0.000 abstract description 5
- 235000002566 Capsicum Nutrition 0.000 abstract description 4
- 239000006002 Pepper Substances 0.000 abstract description 4
- 235000016761 Piper aduncum Nutrition 0.000 abstract description 4
- 235000017804 Piper guineense Nutrition 0.000 abstract description 4
- 235000008184 Piper nigrum Nutrition 0.000 abstract description 4
- 240000002234 Allium sativum Species 0.000 abstract description 3
- FZHXIRIBWMQPQF-UHFFFAOYSA-N Glc-NH2 Natural products O=CC(N)C(O)C(O)C(O)CO FZHXIRIBWMQPQF-UHFFFAOYSA-N 0.000 abstract description 3
- 244000273928 Zingiber officinale Species 0.000 abstract description 3
- 235000006886 Zingiber officinale Nutrition 0.000 abstract description 3
- 150000001413 amino acids Chemical class 0.000 abstract description 3
- 235000004611 garlic Nutrition 0.000 abstract description 3
- 235000008397 ginger Nutrition 0.000 abstract description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 3
- 239000011707 mineral Substances 0.000 abstract description 3
- 239000007921 spray Substances 0.000 abstract description 3
- 235000005254 Allium ampeloprasum Nutrition 0.000 abstract description 2
- 240000006108 Allium ampeloprasum Species 0.000 abstract description 2
- 241001474374 Blennius Species 0.000 abstract description 2
- 241000283690 Bos taurus Species 0.000 abstract description 2
- 239000011785 micronutrient Substances 0.000 abstract description 2
- 235000013369 micronutrients Nutrition 0.000 abstract description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract description 2
- 244000203593 Piper nigrum Species 0.000 abstract 1
- 235000015872 dietary supplement Nutrition 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 235000014347 soups Nutrition 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000004599 antimicrobial Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 241000722363 Piper Species 0.000 description 3
- MSWZFWKMSRAUBD-QZABAPFNSA-N beta-D-glucosamine Chemical compound N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O MSWZFWKMSRAUBD-QZABAPFNSA-N 0.000 description 3
- 239000000546 pharmaceutical excipient Substances 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- CBOJBBMQJBVCMW-BTVCFUMJSA-N (2r,3r,4s,5r)-2-amino-3,4,5,6-tetrahydroxyhexanal;hydrochloride Chemical compound Cl.O=C[C@H](N)[C@@H](O)[C@H](O)[C@H](O)CO CBOJBBMQJBVCMW-BTVCFUMJSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229960001911 glucosamine hydrochloride Drugs 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 235000002639 sodium chloride Nutrition 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 229920001661 Chitosan Polymers 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- 229920002245 Dextrose equivalent Polymers 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 206010003246 arthritis Diseases 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 235000008504 concentrate Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 230000006806 disease prevention Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 210000001031 ethmoid bone Anatomy 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 125000001841 imino group Chemical group [H]N=* 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000014109 instant soup Nutrition 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 235000021404 traditional food Nutrition 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
본 발명은 글루코사민이 함유된 사골 분말 조성물 및 그 제조방법에 관한 것이다. 보다 상세하게는 게껍질에서 키틴을 분해하여 글루코사민을 제조하고, 소뼈에서 열수추출한 사골엑기스를 농축하여 분무건조시 부형제는 점성을 방지하기 위하여 환원당등급(DE: Dextrose Equivalent)이 20이하인 물엿과 산패방지제로 비타민E를 첨가하여 미립형의 사골 분말을 얻는다. 분무건조한 사골 분말 60-70 중량%에 글루코사민 5-10 중량%와 소금 0.8-1.3 중량%, 덱스트린 15-25 중량%를 첨가하여 사골 분말 제품을 얻는다.The present invention relates to a bone bone powder composition containing glucosamine and a method for producing the same. More specifically, glucosamine was prepared by decomposing chitin in crab shells, and the bone marrow extract extracted from bovine bone was concentrated to prevent viscosity when spray-dried. To prevent viscosity, starch syrup having a reducing sugar grade (DE) of 20 or less was used to prevent rancidity. Vitamin E is added to obtain fine bone bone powder. To 60-70% by weight of the spray dried sand bone powder, 5-10% by weight of glucosamine, 0.8-1.3% by weight of salt, and 15-25% by weight of dextrin are added to obtain a bone bone product.
상기의 사골 분말에 말토덱스트린, 마늘, 건파, 양파, 후추, 생강및해조칼슘 등을 혼합하여 즉석용 사골곰탕을 제조할 수 있다.Maltodextrin, garlic, dried leek, onion, pepper, ginger and seaweed calcium may be mixed with the bone bone powder to prepare instant bone bone soup.
본 발명은 사골엑기스에 함유된 풍부한 아미노산과 무기물 및 미량 영양소가 다량 함유되어 있고, 글루코사민에 유리형의 일급 아미노기를 가지는 글루코사민-2-아미노-2-데옥시-디-글루코피라네이스(glucosamine-2-amino-2-deoxy-D-glucopyranase; GlcN)이 함유되어 있는 사골 분말을 휴대하기 간편하게 분말화 시켰으므로 노약자, 환자, 수험생 및 직장인의 피로회복 및 영양보충에 제공할 수 있다.The present invention is a glucosamine-2-amino-2-deoxy-di-glucopyranes (glucosamine-2) containing abundant amino acids, minerals and micronutrients contained in the bone bone extract, and having a free primary amino group in glucosamine. The bone-bone powder containing -amino-2-deoxy-D-glucopyranase (GlcN) is easily powdered and can be used for fatigue recovery and nutritional supplements for the elderly, patients, examinees and office workers.
Description
본 발명은 쇠고기뼈에서 추출한 사골엑기스를 분무건조하여 글루코사민(D-Glucosamine)과 소금을 첨가하여 구성된 사골 분말 조성물 및 그 제조방법에 관한 것이다. 보다 상세하게는 게껍질에서 키틴(Chitin)을 분해하여 글루코사민을 제조하고, 소뼈를 열수추출하여 얻은 사골엑기스를 농축하여 분무건조시 부형제로 물엿과 산패방지제로 비타민E를 첨가하여 분무건조하여 얻어진 미립형의 사골 분말에 글루코사민과 소금을 첨가하여 사골 분말 제품을 얻는다.The present invention relates to a bone bone powder composition and a method for preparing the same, which are formed by spray-drying a bone bone extract extracted from beef bone and adding glucosamine (D-Glucosamine) and salt. More specifically, glucosamine was prepared by decomposing chitin in the crab shell, and concentrated bone marrow extract obtained by hot water extraction of bovine bone was added by spray drying by adding vitamin E as starch syrup and antiseptic agent during spray drying. Glucosamine and salt are added to the ethmoid bone powder to obtain an ethmoid powder product.
전통적으로 사골은 쇠고기뼈에서 우려낸 국물로서 쇠고기, 양파, 소금, 후추등을 넣고 곰탕을 제조하여 밥과 함께 먹는 보양식이다. 쇠고기뼈에는 무기물과 단백질이 주성분으로 이들이 고온에서 분해되어 아미노산, 칼슘, 인 및 미량의 영양소가 생성되므로 노약자나 어린이 뿐만아니라 정상인도 체내에서 흡수가 용이하여 건강식품으로 널리 애용되어 온 전통음식이다.Traditionally, beef bone is a broth made from beef bones, which is made with beef, onions, salt, pepper, etc. Mineral bones and proteins are the main ingredients in beef bones, so they are decomposed at high temperatures to produce amino acids, calcium, phosphorus and trace nutrients. Therefore, it is a traditional food that has been widely used as a health food because it is easily absorbed by the elderly as well as children.
한편 글루코사민은 키틴, 키토산의 구성당으로서 유리의 1급 이미노기를 가지는 글루코사민에는 글루코사민-2-아미노-2-데옥시-디-글루코피라네이스글루코사미네이스(glucosamine-2-amino-2-deoxy-D-glucopyranase; GlcN)가 함유되어 있으며Glucosamine is a constituent of chitin and chitosan, and glucosamine having a free primary imino group includes glucosamine-2-amino-2-deoxy-di-glucopyranisglucosamine (glucosamine-2-amino-2-deoxy-). D-glucopyranase; GlcN)
글루코사민은 체내에서 방사능 배출, 장내 세균의 기질이용성, 변형성 관절염에 대한 유용성 등으로 인하여 환자, 노약자, 운동선수 등에게 의약품이나 식품으로 공급하여 효과를 거두고 있다고 알려져 있다.Glucosamine is known to be effective by supplying medicines or foods to patients, the elderly, athletes, etc. due to radioactivity in the body, substrate availability of intestinal bacteria, and usefulness for deformable arthritis.
본 발명과 관련된 종래기술은 한국특허공고 84-457호 즉석곰탕의 제조방법, 한국특허공고 88-217호 인스탄트용 곰탕원료의 제조방법, 한국특허공개 99-2317호 군 냄새가 제거된 농축사골분말과 그 제조방법 등이 있으나 일반적인 건조 및 가공방법에 관한 것으로 본 발명과는 기술적 구성이 다른 것들이다.The prior art related to the present invention is a method for producing instant instant soup in Korean Patent Publication No. 84-457, a method for preparing Gomtang raw material for instant patent in Korean Patent Publication No. 88-217, and Korean Patent Publication No. 99-2317 for enriched bone powder And the production method and the like, but relates to a general drying and processing method is a technical configuration different from the present invention.
본 발명은 종래에 사골엑기스의 분무건조시 살균 목적으로 소금을 첨가하였으나 조해성으로 인하여 건조물이 분무건조기 내부벽에 침착되는 경우가 많고 작업성을 저해하는 원인이 되어 왔다. 본 발명은 건조조제 겸 부형제로서 사골엑기스의 점성을 방지하기 위하여 물엿과 산패방지제로 비타민E(토코페롤)를 첨가하여 미립형의 사골 분말을 제조하여 게껍질로부터 분리하여 건조한 글루코사민과 덱스트린 및 소금을 혼합하여 인스탄트용 사골 분말제품을 제조하는 것을 목적으로 한다.In the present invention, salt is added for sterilization purposes during spray drying of bone bone extract, but dry matters are often deposited on the inner wall of the spray dryer due to deliquescent property, which has been a cause of impairing workability. The present invention is a dry adjuvant and excipient to add the vitamin E (tocopherol) as starch syrup and antiseptic agent to prevent the viscosity of the bone marrow extract to prepare a fine bone bone powder, separated from crab shells and mixed dry glucosamine, dextrin and salt It is intended to produce a bone bone powder product for instants.
도 1은 본 발명의 사골엑기스 제조공정도이다.1 is a process for producing bone bone extract of the present invention.
도 2는 본 발명의 글루코사민 제조공정도이다.2 is a glucosamine production process of the present invention.
본 발명은 게껍질로부터 키틴을 제조하는 공정, 키틴으로부터 글루코사민을 제조하는 공정, 쇠고기뼈로부터 사골엑기스를 추출하여 분무건조하는 공정과 이들 공정으로부터 제조된 글루코사민과 사골 분말에 소금 및 덱스트린을 혼합하는 공정으로 구성되어 있다. 이한 각 공정에 대한 자세한 설명은 다음과 같다.The present invention provides a process for preparing chitin from crab shell, a process for preparing glucosamine from chitin, a process for extracting sand bone extract from beef bone and spray drying, and a process for mixing salt and dextrin to glucosamine and bone bone powder prepared from these processes. It consists of. Detailed description of each of these processes is as follows.
[제 1공정]: 키틴 제조공정[Step 1]: Chitin Manufacturing Process
정선된 게껍질을 온수로 세척 및 탈수하여 이물질을 제거한 후 탈수하여 5-7% 염산 수용액에 실온에서 3시간 침전시킨 상태에서 서서히 교반하여 칼슘을 용해한다. 용해된 칼슘염에 3-5% NaOH 용액에 80-90℃에서 3시간 교반하여 단백질을 분해시키고, 용해된 칼슘염을 중화시킨 후 물로 세척한다. 원심분리하여 수분을 제거하고 70-80℃에서 열풍건조하여 키틴을 제조한다.Selected crab shells are washed with warm water and dehydrated to remove foreign substances, and then dehydrated and slowly stirred in a solution of 5-7% hydrochloric acid at room temperature for 3 hours to dissolve calcium. The dissolved calcium salt was dissolved in 3-5% NaOH solution at 80-90 ° C. for 3 hours to decompose the protein, neutralize the dissolved calcium salt and wash with water. Water is removed by centrifugation and hot air dried at 70-80 ° C. to prepare chitin.
[제 2공정]: 글루코사민 제조공정[Step 2]: Glucosamine Production Process
상기에서 제조된 키틴에 35% 농염산을 첨가하여 70-80℃에서 5-8시간 가수분해한 후, 활성탄으로 탈색 및 여과 한다. 이 여액을 진공감압 상태에서 농축하고 5℃로 냉각하여 결정화시키고 물을 첨가하여 pH를 4-6으로 조정한 후 결정체를 침전시키고 탈수하여 100% 에탄올로 정제한다. 결정체를 여과 및 건조하여 글루코사민염산염(D-GlucosamineㆍHCl)을 제조한다.After adding 35% concentrated hydrochloric acid to the chitin prepared above, hydrolysis at 70-80 ° C. for 5-8 hours, decolorization and filtration with activated carbon. The filtrate is concentrated under vacuum, cooled to 5 ° C. to crystallize, the pH is adjusted to 4-6 by the addition of water, the precipitate is precipitated, dehydrated and purified by 100% ethanol. Crystals were filtered and dried to prepare glucosamine hydrochloride (D-Glucosamine.HCl).
[제 3공정]: 사골엑기스 분말 제조공정[3rd process]: Sand bone extract powder manufacturing process
일정한 크기로 절단한 쇠고기뼈를 물로 수세하여 사골에 정제수를 혼합한 후, 110-115℃에서 1-2시간 동안 가열하면서 3∼4kg/cm2로 압력을 유지하여 추출한 후, 사골엑기스 상부에 떠오르는 기름기와 부유물을 분리한 후 농축 및 여과하고 9 5-105℃에서 20-40분간 살균한 후, 냉각하여 지방을 제거한 농축액을 여과하여 얻은 사골엑기스에 건조조제 겸 부형제로서 사골엑기스의 점성을 방지하기 위하여 환원당등급(DE: Dextrose Equivalent) 20이하인 물엿 5-30 중량%와 산패방지제로 비타민E(토코페롤)를 0.01-1%를 첨가하여 120℃로 30분간 분무건조한 후 포장하여 인스턴트용 사골 분말제품을 제조한다.Wash the beef bone cut to a certain size with water and mix the purified water to the bone bone, and then extracted by maintaining the pressure at 3 ~ 4kg / cm 2 while heating at 110-115 ℃ for 1-2 hours, then floated on the top of the bone bone extract After separating oil and suspended solids, concentrated and filtered, sterilized at 9 5-105 ℃ for 20-40 minutes, and cooling the concentrated solution from which fat was removed to prevent the viscosity of the bone marrow extract as a drying aid and excipient. 5-30% by weight of starch syrup with a reducing sugar grade (DE: Dextrose Equivalent) of 20 or less and 0.01-1% of vitamin E (tocopherol) as an antiseptic agent are spray-dried at 120 ° C. for 30 minutes, and then packaged to make instant bone powder products. Manufacture.
＜실시예 1＞<Example 1>
잘게 분쇄한 게껍질 1kg의 이물질을 제거한 후 6%-HCl 수용액 2리터를 가하여 실온에서 3시간 용해한 칼슘염에 4%-NaOH 용액 2리터를 넣고 85℃에서 3시간 교반하여 칼슘염을 중화시켜 물로 세척하고, 슬러리는 원심분리한 후 80℃에서 열풍건조하여 키틴 150g을 제조하였다.After removing 1kg of finely crushed crab shell, add 2 liters of 6% -HCl aqueous solution, add 2 liters of 4% -NaOH solution to calcium salt dissolved at room temperature for 3 hours, and stir at 85 ℃ for 3 hours to neutralize calcium salt with water. After washing, the slurry was centrifuged and hot-air dried at 80 ° C. to prepare 150 g of chitin.
상기와 같이 제조한 키틴 150 g에 35%-HCl 20 리터(ℓ)를 첨가하여 75에서 6시간 가수분해하여 활성탄으로 탈색한 여액을 진공감압으로 농축하고 5℃에서 결정화시켜 pH를 4-6으로 조정한 후 100% 에탄올 20 리터로 정제한다. 결정체를 여과 및 건조하여 글루코사민염산염(D-GlucosamineㆍHCl) 90 g을 제조하였다.20 liter (ℓ) of 35% -HCl was added to 150 g of the chitin prepared as described above, and the filtrate, which was decolorized with activated charcoal by hydrolysis at 75 for 6 hours, was concentrated under vacuum and crystallized at 5 ° C. to pH 4-6. After adjustment is purified with 20 liters of 100% ethanol. The crystals were filtered and dried to prepare 90 g of glucosamine hydrochloride (D-Glucosamine.HCl).
＜실시예 2＞<Example 2>
2-3cm 크기로 절단한 쇠고기뼈 5kg을 물로 수세하여 정제수 10리터에 넣고 110℃에서 2시간 동안 가열하면서 3kg/cm2로 압력으로 사골을 추출한 후 상온으로 냉각하여 사골엑기스 상부에 떠오르는 기름기와 부유물을 제거하였다. 사골엑기스를 감압농축 및 여과하고 95℃에서 30분간 살균한 후, 상온으로 냉각하여 재차 지방을 제거하여 사골엑기스 농축액 2리터를 얻고 120℃에서 30분간 분무건조한 후 포장하여 인스턴트용 사골 분말제품을 제조한다5kg of beef bone cut into 2-3cm size was washed with water, put into 10 liters of purified water, heated at 110 ℃ for 2 hours, extracted from the bone bone with pressure at 3kg / cm 2 , cooled to room temperature and cooled to room temperature. Was removed. The bone marrow extract was concentrated under reduced pressure and filtered, sterilized at 95 ° C. for 30 minutes, cooled to room temperature to remove fat again to obtain 2 liters of bone marrow extract concentrate, spray dried at 120 ° C. for 30 minutes, and then packaged to prepare instant bone powder products. do
＜실시예 3＞<Example 3>
실시예 1의 글루코사민 10중량%, 실시예 2의 사골 분말 69중량%와 덱스트린 20중량% 및 소금 1.0중량%를 혼합하여 사골 분말을 제조하였다.Bone powder was prepared by mixing 10% by weight of glucosamine of Example 1, 69% by weight of bone bone powder of Example 2, 20% by weight of dextrin and 1.0% by weight of salt.
＜시험예＞: 관능검사<Test example>: Sensory test
본 발명의 사골 분말을 조성비에 따라 더운물에 풀었을 때 분산정도 와 맛, 색도 등을 시험하기 위하여 잘 훈련된 25세에서 30세의 남녀 10명을 대상으로 관능검사를 실시하여 표 1에 나타냈다.When the bone bone powder of the present invention was dissolved in hot water according to the composition ratio, a sensory test was conducted on 10 men and women 25 to 30 years of age who are well trained to test the degree of dispersion, taste, color, and the like.
표 1. 조성비별 관능검사 결과Table 1. Sensory test results by composition ratio
(대단히 양호: ◎, 양호: ○, 보통: △, 불량: ×)(Very good: ◎, Good: ○, Normal: △, Poor: ×)
A: 사골 분말 75, 글루코사민 5, 덱스트린 19, 소금 1 중량%A: sand bone powder 75, glucosamine 5, dextrin 19, salt 1% by weight
B: 사골 분말 75, 글루코사민 9, 덱스트린 15, 소금 1 중량%B: sand bone powder 75, glucosamine 9, dextrin 15, salt 1% by weight
C: 사골 분말 70, 글루코사민 10, 덱스트린 19, 소금 1 중량%C: sand bone powder 70, glucosamine 10, dextrin 19, salt 1% by weight
D: 사골 분말 70, 글루코사민 9, 덱스트린 20, 소금 1 중량%D: Sand bone powder 70, Glucosamine 9, Dextrin 20, Salt 1% by weight
E: 사골 분말 65, 글루코사민 15, 덱스트린 19, 소금 1 중량%E: sand bone powder 65, glucosamine 15, dextrin 19, salt 1% by weight
F: 사골 분말 65, 글루코사민 10, 덱스트린 24, 소금 1 중량%F: Sand bone powder 65, Glucosamine 10, Dextrin 24, Salt 1% by weight
G: 사골 분말 60, 글루코사민 19, 덱스트린 20, 소금 1 중량%G: sand bone powder 60, glucosamine 19, dextrin 20, salt 1% by weight
H: 사골 분말 60, 글루코사민 15, 덱스트린 24, 소금 1 중량%H: sand bone powder 60, glucosamine 15, dextrin 24, salt 1% by weight
상기의 결과로부터 조성 C(사골 분말 70, 글루코사민 10, 덱스트린 19, 소금 1 중량%), 조성 D(사골 분말 70, 글루코사민 9, 덱스트린 20, 소금 1 중량%) 및 조성 E(사골 분말 65, 글루코사민 15, 덱스트린 19, 소금 1 중량%)의 배합비가 분산성, 맛, 색도가 우수한 것으로 나타났다.From the results above, composition C (bone bone powder 70, glucosamine 10, dextrin 19, salt 1% by weight), composition D (bone bone powder 70, glucosamine 9, dextrin 20, salt 1% by weight) and composition E (bone bone powder 65, glucosamine 15, dextrin 19, salt (1% by weight) was found to be excellent in dispersibility, taste, and color.
＜적용예＞: 사골 분말곰탕의 제조<Application Example>: Production of Beef Bone Powder Gomtang
말토덱스트린에 마늘, 양파, 건파, 후추, 소금, 생강 및 해조칼슘을 혼합하여 수분함량을 1% 이하로 건조하여 글루코사민과 사골엑기스를 혼합하여 사골 분말곰탕을 제조한다. 이들의 배합비는 글루코사민 5중량%, 사골 분말 66중량%, 말토덱스트린 16.1중량%, 마늘 0.6중량%, 건파 0.5%, 양파 1.0중량%, 후추 0.2중량%, 생강0.1중량%, 해조칼슘 10.5%를 혼합하여 곰탕용 사골 분말을 제조한다. 곰탕용 사골 분말에 더운물을 붓고 쌀밥과 함께 시식하면 맛있는 곰탕을 즐길 수가 있다.Garlic, onion, dried leek, pepper, salt, ginger and algae calcium are mixed with maltodextrin to dry the water content to 1% or less to prepare glucosamine and bone bone extract to prepare a bone bone powder gourmet. Their blending ratio is 5% by weight of glucosamine, 66% by weight of bone powder, 16.1% by weight maltodextrin, 0.6% by weight garlic, 0.5% dry onion, 1.0% by weight onion, 0.2% by weight pepper, 0.1% by weight ginger and 10.5% seaweed calcium. Mixing to prepare a bone bone powder for Gomtang. You can enjoy delicious Gomtang by pouring hot water into the bone bone powder for Gomtang and tasting it with rice.
본 발명의 사골엑기스는 분무건조시 부형제로 물엿과 산패방지제로 토코페롤을 첨가하여 양호한 형태의 사골 분말을 얻을 수 있다. 또한 풍부한 아미노산과 무기물 및 미량 영양소가 다량 함유되어 있는 사골 분말과, 유리의 일급 아미노기를 가지는 글루코사민-2-아미노-2-데옥시-디-글루코피라네이스(GlcN)의 구조로되어 있는 글루코사민과, 소금 및 덱스트린을 혼합한 인스탄트용 사골 분말은 영양분과 질병예방에 유용한 성분들이 다량 함유되어 있다.The bone marrow extract of the present invention can be obtained by adding tocopherol as starch syrup and antiseptic agent as an excipient during spray drying to obtain a fine bone bone powder. Also, a bone bone powder containing abundant amino acids, a large amount of minerals and micronutrients, glucosamine having a structure of glucosamine-2-amino-2-deoxy-di-glucopyranease (GlcN) having a free primary amino group, The bone bone powder for instant blended with salt and dextrin is rich in nutrients and ingredients useful for disease prevention.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020000006274A KR100330192B1 (en) | 2000-02-10 | 2000-02-10 | Composition for Dried Bone Extract Powder and Manufacturing Method Thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020000006274A KR100330192B1 (en) | 2000-02-10 | 2000-02-10 | Composition for Dried Bone Extract Powder and Manufacturing Method Thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20010083341A KR20010083341A (en) | 2001-09-01 |
| KR100330192B1 true KR100330192B1 (en) | 2002-04-03 |
Family
ID=19645380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020000006274A KR100330192B1 (en) | 2000-02-10 | 2000-02-10 | Composition for Dried Bone Extract Powder and Manufacturing Method Thereof |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR100330192B1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101401176B1 (en) | 2013-01-18 | 2014-06-17 | 충북대학교 산학협력단 | Method for manufacturing deep soup made of cattle bone |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20240085725A (en) * | 2022-12-08 | 2024-06-17 | 씨제이제일제당 (주) | Method for preparing a meat broth composition for retort food with enhanced fragrance and flavor |
-
2000
- 2000-02-10 KR KR1020000006274A patent/KR100330192B1/en not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101401176B1 (en) | 2013-01-18 | 2014-06-17 | 충북대학교 산학협력단 | Method for manufacturing deep soup made of cattle bone |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20010083341A (en) | 2001-09-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP4738856B2 (en) | Method for producing N-acetylglucosamine-containing composition | |
| JP5390085B2 (en) | Method for enriching glucoraphanin in radish seed preparations | |
| CN103416801A (en) | Pitaya functional drink | |
| JP2005524406A (en) | Low isoflavone high saponin soy protein product and method for producing the same | |
| TWI227661B (en) | Water-soluble bean-based extracts | |
| CN1530376A (en) | Extraction of eight products, such as pectine, naringin, etc. | |
| CN102138686A (en) | Preparation method of concentrated juice of yacon adopting bio-enzyme technology | |
| CN102919890B (en) | Composite, preparation method thereof and food comprising composite | |
| WO2010044255A1 (en) | Process for producing phosphorylated water-soluble polysaccharide | |
| WO2017057187A1 (en) | Gardenia pigment preparation | |
| KR100330192B1 (en) | Composition for Dried Bone Extract Powder and Manufacturing Method Thereof | |
| KR940001543B1 (en) | Process for making natural seasonigs from sea-tangle | |
| US6228993B1 (en) | Soy isoflavone concentrate process and product | |
| CN110810619A (en) | Extraction process for extracting selenoprotein from soybeans | |
| KR20140072595A (en) | A natural seasoning containing an extract of ramie leaves and the preparation method thereof | |
| KR20170089545A (en) | Manufacturing method of leek extract and manufacturing method of seasoning material comprising leek extract | |
| JP2005289850A (en) | Production method of material containing high concentration of quercetin | |
| KR100369619B1 (en) | Manufacturing method of fruit jam using tangle extract liquid | |
| KR102602832B1 (en) | Method of manufacture of surfactant using soyasaponin in sprout peanut extract | |
| JP2006333818A (en) | Method for producing composition highly containing gamma-aminobutyric acid | |
| CA2530804A1 (en) | Process for the production of lupin extracts | |
| EP0271964B1 (en) | Method for preparing protein hydrolysates soluble in an acid environment, and the hydrolysates obtained | |
| KR19980071300A (en) | Method for preparing zinc-containing minerals in plant embryos | |
| CN111374295A (en) | Preparation method and application of high-quality food-grade plant-derived compound amino acid | |
| JPH0356424A (en) | Potassium supplementary agent, production thereof and food, drink and medicine containing the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| E701 | Decision to grant or registration of patent right | ||
| GRNT | Written decision to grant | ||
| FPAY | Annual fee payment |
Payment date: 20080313 Year of fee payment: 7 |
|
| LAPS | Lapse due to unpaid annual fee |