KR0135358B1 - Cosmetic composition comprising spherical liquid drop - Google Patents
Cosmetic composition comprising spherical liquid dropInfo
- Publication number
- KR0135358B1 KR0135358B1 KR1019940029893A KR19940029893A KR0135358B1 KR 0135358 B1 KR0135358 B1 KR 0135358B1 KR 1019940029893 A KR1019940029893 A KR 1019940029893A KR 19940029893 A KR19940029893 A KR 19940029893A KR 0135358 B1 KR0135358 B1 KR 0135358B1
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- liquid
- cosmetic composition
- solution
- aqueous solution
- spherical
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- Cosmetics (AREA)
Abstract
본 발명은 알코올성 수용액인 제 1액과 이온성 염 수용액인 제 2액을 혼합하고 여기에 비극성 오일로 된 제 3액을 교반하여 첨가하여 제조되는 구상 액적을 함유하는 화장료 조성물에 있어서, 계면활성제를 함유하지 않으면, 상기 제 2액이 수산화알루미늄 젤상 수용액(pH 7~8)을 함유함을 특징으로 하는 구상 액적을 함유하는 화장품 조성물에 대한 것으로, 계면활성제에서 야기되는 피부 자극을 경감시킬 수 있으며, 구상 액적의 안정도가 매우 뛰어날 뿐 아니라 우수한 사용감을 제공한다.The present invention relates to a cosmetic composition containing a spherical droplet prepared by mixing a first liquid which is an alcoholic aqueous solution and a second liquid which is an ionic salt aqueous solution, and stirring and adding a third liquid of a nonpolar oil thereto. If not contained, the second liquid is a cosmetic composition containing a spherical droplet, characterized in that it contains an aqueous solution of aluminum hydroxide gel phase (pH 7 ~ 8), can reduce the skin irritation caused by the surfactant, The stability of the spherical droplets is not only excellent but also provides an excellent feeling.
Description
본 발명은 구상 액적을 함유하는 화장료 조성물에 대한 것이며, 보다 상세하게 수산화알루미늄의 젤상 수용액(pH 7~8)을 제 2액에 함유함을 특징으로 하는 화장료 조성물에 대한 것이다.The present invention relates to a cosmetic composition containing spherical droplets, and more particularly to a cosmetic composition comprising a gel aqueous solution of aluminum hydroxide (pH 7-8) in a second liquid.
기존의 화장료 중 오일 제품은 넓은 부위를 쉽게 도포할 수 있으며 땀이나 물에 잘 씻겨지지 않는 장점이 있는 반면, 오일의 끈적거림이나 번들거림과 같은 사용감의 단점이 있다. 유화 제품은 상기와 같은 오일 제품의 사용감을 개선시키기 위한 것으로, 계면활성제(유화제)를 상당량 첨가하여 안정성 유화제품으로 만들어 왔으나 계면활성제로 인한 피부자극이 문제가 되어 왔다. 따라서, 오일 제품이 갖는 나쁜 사용감을 개선시키는 동시에, 계면활성제에 의한 피부 자극이 없는 화장료 조성물을 제공하기 위한 연구가 거듭되어 왔으며, 그 결과, 유기 계면활성제를 사용하지 않고, 적절한 분체를 사용하여 오일을 알코올 수용액에 분산시킴으로써, 오일이 알코올 수용액 상에 구상으로 존재하게 되는, 구상 액적을 함유하는 화장료 조성물이 개발되게 되었다.Oil products of the existing cosmetics can be easily applied to a large area and has the advantage of not being washed well with sweat or water, while there is a disadvantage of feeling, such as oily sticky or greasy. Emulsified products are intended to improve the usability of such oil products, and have been added to surfactants (emulsifiers) in significant amounts to make stable emulsion products, but skin irritation due to surfactants has been a problem. Therefore, studies have been repeatedly made to improve the bad feeling of oil products and to provide cosmetic compositions without skin irritation by surfactants. As a result, oils can be prepared using appropriate powders without using organic surfactants. By dispersing it in an aqueous alcohol solution, a cosmetic composition containing spherical droplets in which oil is spherically present on an aqueous alcohol solution has been developed.
구상액적을 함유하는 화장료 조성물에 대한 선행 기술로는 여러가지 첨가제를 함유하는 알코올성 수용액(제 1액)과 물(정제수)에 소량의 칼슘클로라이드(CaCl2)를 비롯한 이온성염을 완전히 녹인 용액(제 2액)을 혼합하여 균일한 상태로 교반한 다음 불용성인 유동파라핀, 실리콘유, 스쿠알란등의 비극성 오일에 마그네슘, 산화물로 구성된 미세한 분말(5~30㎛)인 탈크(Talc), 카오린(Kaolin), 마이카(Mica)등을 적량균일하게 분산시킨 용액(제 3액)을 만들어 제 1액과 제 2액의 혼합액에 제 3액을 첨가하면서 교반하여 만드는 방법이 있는데, 이렇게 하여 만들어진 용액은 정치하면 구상액적의 내상과 이를 둘러싼 외상으로 나누어지게 된다. 그러나, 탈크(Talc), 카오린(Kaolin), 마이카(Mica) 등을 사용할 경우 구상액적의 안정도가 좋지않아 액적이 깨어져서 1개월 정도 정치할 경우 분말상의 침전물이 가라앉는 현상이 발생한다. 또한, 사용시 사용감이 다소 거친 문제점이 있었다.Prior arts for cosmetic compositions containing spherical droplets include a solution in which an ionic salt, including a small amount of calcium chloride (CaCl 2 ), is completely dissolved in an alcoholic aqueous solution (first liquid) containing various additives and water (purified water) (second Liquid) and stirred in a uniform state, and then fine powders (5-30 μm) made of magnesium and oxide to non-polar oils such as insoluble liquid paraffin, silicone oil and squalane, and talc, kaolin, There is a method of making a solution (third liquid) in which the mica and the like are uniformly dispersed and adding the third liquid to the mixed solution of the first liquid and the second liquid, and stirring the solution. It is divided into the inner wound of the droplet and the surrounding trauma. However, when Talc, Kaolin, Mica, etc. are used, spherical droplets are not stable and the powdery precipitates sink when left standing for about one month. In addition, there was a problem that is somewhat rough when using.
본 발명자들은 상기한 바와 같은 종래기술의 문제점을 해결하기 위하여 광범위하고도 철저하게 연구하여 오던 중, 알루미늄 산화물 분말을 pH 7~8인 수산화알루미늄 젤상 수용액 형태로 만들어 제 2액에 첨가하면, 구상액적의 균일성과 안정도가 매우 우수하여 침전물이 생기지 않을 뿐 아니라, 외관상으로 진주(pearl)같은 느낌을 주어 제품으로서의 세련미를 더해 줄 수 있고 또한 사용상으로도 우수한 보습력과 매끄러운 사용감을 주게 됨을 발견하고 본 발명을 완성하게 되었다.The present inventors have been extensively and thoroughly researched to solve the problems of the prior art as described above, when the aluminum oxide powder is added to the second liquid in the form of an aqueous solution of an aluminum hydroxide gel phase of pH 7-8, spherical solution The uniformity and stability of the enemy is very good, so that no precipitate is formed, and the appearance of pearls gives the appearance of a refined product, and also provides excellent moisturizing power and smooth feeling in use. It was completed.
즉, 본 발명의 목적은 구상 액적의 안정도가 우수하며 보다 우수한 사용감을 줄 수 있는 구상 액적을 함유하는 화장료 조성물을 제공하는 것이다.That is, it is an object of the present invention to provide a cosmetic composition containing spherical droplets that are excellent in stability of spherical droplets and which can give a better feeling of use.
본 발명의 또다른 목적은 알코올성 수용액인 제 1액과 이온성염 수용액인 제 2액을 혼합하고 여기에 비극성 오일로 된 제 3 액을 교반하여 첨가하여 제조되는 구상액적을 함유하는 화장료 조성물에 있어서, 상기 제 2액은 수산화알루미늄 젤상 수용액을 함유함을 특징으로 하는 구상 액적을 함유하는 화장료 조성물을 제공하는 것이다.Still another object of the present invention is to provide a cosmetic composition containing a spherical droplet prepared by mixing a first liquid, which is an alcoholic aqueous solution, and a second liquid, which is an ionic salt aqueous solution, followed by stirring and adding a third liquid of nonpolar oil. The second liquid is to provide a cosmetic composition containing a spherical droplet, characterized in that it contains an aqueous solution of aluminum hydroxide gel phase.
이하, 본 발명을 보다 상세히 설명한다.Hereinafter, the present invention will be described in more detail.
본 발명에 의한 구상 액적을 함유한 화장료 조성물은 계면활성제와 마그네슘 산화물 분말을 사용하지 않으며, 알루미늄 산화물 분말을 pH 7~8인 수산화 알루미늄 젤상 수용액으로 만들어 이온성염 수용액인 제 2액에 첨가한다. 본 발명에 의한 구상 액적을 함유하는 화장료 조성물이 갖는 제 2액은 염화칼슘, 염화나트륨, 염화알루미늄, 염화마그네슘과 같은 1~3가지의 이온성염의 수용액이다. 또한, 제 3액으로 사용되는 오일로는 유동파라핀, 실리콘유, 초산토코페롤 또는 식물성유를 예시할 수 있다.The cosmetic composition containing the spherical droplet according to the present invention does not use a surfactant and magnesium oxide powder, and makes the aluminum oxide powder into an aqueous aluminum hydroxide gel solution having a pH of 7 to 8 and adds it to the second liquid which is an ionic salt aqueous solution. The 2nd liquid which the cosmetic composition containing the spherical droplet which concerns on this invention has is an aqueous solution of 1-3 ionic salts, such as calcium chloride, sodium chloride, aluminum chloride, and magnesium chloride. In addition, the oil used as the third liquid may include liquid paraffin, silicone oil, tocopherol acetate or vegetable oil.
본 발명에 의한 구상 액적을 함유하는 화장료 조성물은 기존의 화장품류와는 달리 계면활성제를 사용하지 않았기 때문에 계면활성제로 인한 알레르기성 피부자극을 경감시킬 수 있고, 일반적인 화장료의 단순한 액상과는 달리 외관상으로도 독특한 모양과 빛의 산란을 통해 투명한 보석과 같이 보이게 하는 효과를 얻을 수 있었다.The cosmetic composition containing the spherical droplets according to the present invention can reduce allergic skin irritation due to the surfactant because it does not use a surfactant unlike conventional cosmetics, and in appearance unlike a simple liquid of a general cosmetic Also, the unique shape and scattering of light gave the effect of making it look like a transparent gem.
즉, 본 발명을 요약하면, 본 발명은 알코올성 수용액인 제 1액과 이온성염 수용액인 제 2액을 혼합하고 여기에 비극성 오일로 된 제 3액을 교반하여 첨가하여 제조되는 구상 액적을 함유하는 화장료 조성물에 있어서, 계면활성제를 함유하지 않으며, 상기 제 2액이 수산화 알루미늄 젤상 수용액(pH 7~8)을 함유함을 특징으로 하는 구상액적을 함유하는 화장료 조성물에 대한 것으로, 다음과 같은 효과를 가진다.That is, to summarize the present invention, the present invention is a cosmetic composition containing spherical droplets prepared by mixing the first liquid of the aqueous alcoholic solution and the second liquid of the ionic salt aqueous solution and stirring and adding the third liquid of non-polar oil to it. The composition is a cosmetic composition containing spherical droplets, wherein the composition contains no surfactant and the second liquid contains an aqueous solution of aluminum hydroxide gel phase (pH 7-8), and has the following effects: .
첫째, 계면활성제에서 야기되는 알레르기성 피부자극을 경감시킬 수 있다.First, allergic skin irritation caused by surfactants can be alleviated.
둘째, 구상 액적의 안정도가 매우 우수하므로 저부향으로도 향력을 증가시켜 향의 지속성을 높일 수 있어 오랫동안 향을 즐길 수 있다.Second, because the stability of the spherical droplets is very excellent, it is possible to enjoy the fragrance for a long time by increasing the fragrance even in the low side to increase the persistence of the fragrance.
셋째, 일반적인 화장류의 단순한 액상과는 달리 외관상으로도 독특한 모양과 빛의 산란을 통해 반짝이는 효과를 얻을 수 있으며 펄(pearl)을 적당히 사용할 경우는 제품의 고급성을 더욱 높일 수 있다.Third, unlike the simple liquid phase of general cosmetics, the appearance of the unique shape and light scattering effect can be obtained through the appearance of the pearl (pearl) when properly used can further enhance the luxury of the product.
넷째, 보습력이 있는 오일을 적당량 사용함으로써 배스(bath)제품의 효과와 방향효과를 가진 샤워코롱제품의 효과를 동시에 가질 수 있다.Fourth, by using an appropriate amount of the moisturizing oil can have the effect of the bath product (bath) and the shower cologne product having an aroma effect at the same time.
이하, 실시예 및 실험예를 통해 본 발명을 보다 상세히 설명하지만 실시예 들이 본 발명을 한정하는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to Examples and Experimental Examples, but the Examples are not intended to limit the present invention.
실시예 1 : 오데코롱의 제조Example 1 Preparation of Ode Cologne
향료 5.0 중량부에 에탄올 40.0중량부를 혼합하여 제 1액으로 하고, 물(정제수) 5.0중량부에 칼슘클로라이드 1.0중량부, pH 7~8인 수산화 알루미늄 젤용액 적당량을 완전히 녹인 용액을 제 2액으로 하여 제 1액과 제 2액을 잘 혼합하여 교반한 용액에 유동파라핀 40.0중량부를 서서히 첨가하면서 혼합 교반하였다.40.0 parts by weight of ethanol was mixed with 5.0 parts by weight of fragrance to make a first solution, and 1.0 part by weight of calcium chloride and an appropriate amount of an aluminum hydroxide gel solution having a pH of 7 to 8 were added to 5.0 parts by weight of water (purified water) as a second solution. The mixture was stirred well while slowly mixing 40.0 parts by weight of the liquid paraffin to the stirred solution of the first liquid and the second liquid.
실시예 2 : 샤워코롱의 제조Example 2 Preparation of Shower Cologne
향료 2.5중량부를 에탄올 60.0중량부에 혼합하여 제 1액으로 하고, 물(정제수)4.0중량부에 칼슘클로라이드 1.0중량부, pH 7~8인 수산화알루미늄 젤용액 적당량을 완전히 녹인 용액을 제 2액으로 하여 제 1액과 제 2액을 잘 혼합하여 교반한 용액에 유동파라핀 25.5중량부를 서서히 첨가하면서 혼합 교반하였다.2.5 parts by weight of fragrance was mixed with 60.0 parts by weight of ethanol to make the first solution, and 1.0 parts by weight of calcium chloride and an appropriate amount of an aluminum hydroxide gel solution having a pH of 7 to 8 were added to 4.0 parts by weight of water (purified water) as a second solution. The mixture was stirred well while slowly mixing 25.5 parts by weight of liquid paraffin to the stirred solution of the first liquid and the second liquid.
실시예 3 : 오일 엣센스의 제조Example 3 Preparation of Oil Essence
향료 0.1 중량부에 에탄올 10.0중량부 및 기타 첨가제를 혼합하여 제 1액으로 하고, 물(정제수) 1.0중랴부에 칼슘클로라이드 1.0중량부, pH 7~8인 수산화 알루미늄 젤용액 적당량을 완전히 녹인 용액을 제 2액으로 하여 제 1액과 제 2액을 잘 혼합하여 교반한 용액에 유동파라핀 78.5중량부를 서서히 첨가하면서 혼합 교반하였다.10.0 parts by weight of ethanol and 10.0 parts by weight of ethanol and other additives were mixed to make the first solution. 1.0 part by weight of calcium chloride and a solution of an appropriate amount of aluminum hydroxide gel solution having a pH of 7 to 8 were completely dissolved in 1.0 concentration of water (purified water). The mixture was stirred while slowly adding 78.5 parts by weight of the liquid paraffin to the stirred solution of the first liquid and the second liquid as the second liquid.
실시예 4 : 썬오일의 제조Example 4 Preparation of Sun Oil
향료 0.1중량부를 에탄올 8.0중량부, 자외선 차단제 및 기타 첨가제를 혼합하여 제 1액으로 하고, 물(정제수) 0.5중량부에 칼슘클로라이드 1.0중량부, pH 7~8인 수산화알루미늄 젤용액 적당량을 완전히 녹인 용액을 제 2액으로 하여 제 1액과 제 2액을 잘 혼합하여 교반한 용액에 유동파라핀 85.5중량부를 서서히 혼합 교반하였다.0.1 parts by weight of ethanol, 8.0 parts by weight of ethanol, sunscreen and other additives were mixed to make the first solution, and 0.5 parts by weight of water (purified water) 1.0 parts by weight of calcium chloride and an appropriate amount of an aluminum hydroxide gel solution having a pH of 7 to 8 were completely dissolved. 85.5 parts by weight of the liquid paraffin was slowly mixed and stirred in the solution, which was mixed with the first liquid and the second liquid with the solution as the second liquid.
실시예 5 : 헤어리퀴드의 제조Example 5 Preparation of Hair Liquid
향료 0.5중량부를 에탄올 60.0중량부, 피피지-20메칠글루코스메텔 2.0중량부아비에틸알코올 0.5중량부를 혼합하여 제 1액으로 하고, 물(정제수)20.0중량부에 칼슘클로라이드 1.0중량부, pH 7~8인 수산화알루미늄 젤용액 적당량을 완전히 녹인 용액을 제 2액으로 하여 제 1액과 제 2액을 잘 혼합하여 교반한 용액에 유동파라핀 15.9중량부를 서서히 첨가하면서 혼합 교반하였다.0.5 parts by weight of ethanol, 60.0 parts by weight of ethanol, sebum-20 methyl glucose methyl, 2.0 parts by weight of aviethyl alcohol, 0.5 parts by weight of the first solution was mixed, 20.0 parts by weight of water (purified water) 1.0 parts by weight of calcium chloride, pH 7 ~ A solution in which an appropriate amount of an aluminum hydroxide gel solution of 8 was completely dissolved was used as a second solution, and the mixture was stirred while slowly adding 15.9 parts by weight of liquid paraffin to the stirred solution.
실험예 1 : 구상액적의 안정도 비교Experimental Example 1 Comparison of Stability of Spherical Drops
종래의 구상액적 함유 조성물과 실시예 1~5에 의해 제조된 본 발명에 의한 구상 액적 함유 화장료 조성물을 장기간 방치한 후, 액적이 깨어져 분말상의 침전물이 발생하는지의 여부를 관찰하였다. 그 결과는 아래의 표와 같다.After leaving the spherical droplet-containing composition and the spherical droplet-containing cosmetic composition according to the present invention prepared in Examples 1 to 5 for a long time, it was observed whether the droplets were broken and powdery precipitates were generated. The results are shown in the table below.
[표 1]TABLE 1
상기 표의 결과에서 알 수 있는 바와 같이, 본 발명에 의한 구상 액적 함유 조성물은 기존의 구상 액적 함유 화장료 조성물에 비해 구상 액적의 안정도가 매우 우수하여 장기간 보관하여도 액적의 깨짐이 거의 관찰되지 않았다.As can be seen from the results of the above table, the spherical droplet-containing composition according to the present invention has excellent stability of spherical droplets compared to the conventional spherical droplet-containing cosmetic composition, so that the cracking of the droplets was hardly observed even after long-term storage.
실험예 2 : 사용감 비교 실험Experimental Example 2 Feeling Comparison Experiment
종래의 구상액적 함유 화장료 조성물과 실시예 1~5에 의해 제조된 본 발명에 의한 구상 액적 함유 화장료 조성물의 사용감을 비교하였다. 사용감은 100명의 시험 대상에게 제품을 사용하게 한 후, 피부자극, 향의 지속성 및 보습력의 항목에 대해 가장 좋은(많은)경우를 5로 하고 가장 나쁜(적은)경우를 0으로 하여 점수를 주게 하여 그 평균값으로 측정하였다. 그 결과는 아래의 표와 같다.The feeling of use of the conventional spherical droplet containing cosmetic composition and the spherical droplet containing cosmetic composition by this invention manufactured by Examples 1-5 was compared. The feeling of use is to have 100 test subjects use the product, and then the best (many) cases and 5 for the worst (less) cases are scored for the items of skin irritation, persistence and moisturizing power. It measured by the average value. The results are shown in the table below.
[표 2]TABLE 2
상기 표의 결과에서 알 수 있는 바와 같이, 본 발명에 의한 구상액적 함유 화장료 조성물은 피부에 대한 자극이 거의 없으며, 매우 우수한 사용감을 제공함을 알 수 있었다.As can be seen from the results of the table, it was found that the spherical droplet-containing cosmetic composition according to the present invention has little irritation to the skin and provides a very good feeling of use.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019940029893A KR0135358B1 (en) | 1994-11-15 | 1994-11-15 | Cosmetic composition comprising spherical liquid drop |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019940029893A KR0135358B1 (en) | 1994-11-15 | 1994-11-15 | Cosmetic composition comprising spherical liquid drop |
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| Publication Number | Publication Date |
|---|---|
| KR960016868A KR960016868A (en) | 1996-06-17 |
| KR0135358B1 true KR0135358B1 (en) | 1998-04-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019940029893A KR0135358B1 (en) | 1994-11-15 | 1994-11-15 | Cosmetic composition comprising spherical liquid drop |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20230100656A (en) | 2021-12-28 | 2023-07-05 | (주)바이오제닉스 | Oil drop cosmetic composition having superior stability and preparation method thereof |
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1994
- 1994-11-15 KR KR1019940029893A patent/KR0135358B1/en not_active IP Right Cessation
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20230100656A (en) | 2021-12-28 | 2023-07-05 | (주)바이오제닉스 | Oil drop cosmetic composition having superior stability and preparation method thereof |
| KR20230100674A (en) | 2021-12-28 | 2023-07-05 | (주)바이오제닉스 | Cosmetic composition comprising oil capsule beads having superior stability and a preparation method thereof |
| KR20230100655A (en) | 2021-12-28 | 2023-07-05 | (주)바이오제닉스 | Tinted cosmetic composition comprising a pigment and preparation method thereof |
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| Publication number | Publication date |
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| KR960016868A (en) | 1996-06-17 |
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