JPS649984A - Production of tetraglycidylamino compound - Google Patents
Production of tetraglycidylamino compoundInfo
- Publication number
- JPS649984A JPS649984A JP16539487A JP16539487A JPS649984A JP S649984 A JPS649984 A JP S649984A JP 16539487 A JP16539487 A JP 16539487A JP 16539487 A JP16539487 A JP 16539487A JP S649984 A JPS649984 A JP S649984A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- dehydrohalogenation
- mmhg
- subjecting
- subjected
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000001875 compounds Chemical class 0.000 title abstract 4
- 238000006704 dehydrohalogenation reaction Methods 0.000 abstract 2
- 150000004985 diamines Chemical class 0.000 abstract 2
- 238000000199 molecular distillation Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract 1
- FDLQZKYLHJJBHD-UHFFFAOYSA-N [3-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=CC(CN)=C1 FDLQZKYLHJJBHD-UHFFFAOYSA-N 0.000 abstract 1
- ISKQADXMHQSTHK-UHFFFAOYSA-N [4-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=C(CN)C=C1 ISKQADXMHQSTHK-UHFFFAOYSA-N 0.000 abstract 1
- 125000004956 cyclohexylene group Chemical group 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 abstract 1
Landscapes
- Epoxy Compounds (AREA)
Abstract
PURPOSE:To obtain the titled compound having high quality and low viscosity as well as reduced residual halogen amount, by reacting a specific diamine with an excess epihalohydrin in the presence of water and subjecting the product to dehydrohalogenation and then subjecting the product to molecular distillation. CONSTITUTION:A diamine (e.g. m- or p-xylylenediamine) expressed by the formula (A is phenylene or cyclohexylene) is reacted with a stoichiometrically excess epihalohydrin (e.g. epichlorohydrin) in the presence of water to afford a polyhalohydrin compound, which is subjected to dehydrohalogenation and the resultant tetraglycidylamino compound is subjected to e.g. molecular distillation in high vacuum area of >=10<-3>mmHg or middle vacuum area of 10<-3>mmHg.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16539487A JPS649984A (en) | 1987-07-03 | 1987-07-03 | Production of tetraglycidylamino compound |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16539487A JPS649984A (en) | 1987-07-03 | 1987-07-03 | Production of tetraglycidylamino compound |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS649984A true JPS649984A (en) | 1989-01-13 |
Family
ID=15811567
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP16539487A Pending JPS649984A (en) | 1987-07-03 | 1987-07-03 | Production of tetraglycidylamino compound |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS649984A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007223912A (en) * | 2006-02-21 | 2007-09-06 | Mitsubishi Gas Chem Co Inc | Method for producing tetraglycidylamino compound |
| EP2143718A4 (en) * | 2007-05-08 | 2011-10-12 | Mitsubishi Gas Chemical Co | PROCESS FOR PRODUCING TETRAGLYCIDYLAMINO COMPOUND |
-
1987
- 1987-07-03 JP JP16539487A patent/JPS649984A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007223912A (en) * | 2006-02-21 | 2007-09-06 | Mitsubishi Gas Chem Co Inc | Method for producing tetraglycidylamino compound |
| EP2143718A4 (en) * | 2007-05-08 | 2011-10-12 | Mitsubishi Gas Chemical Co | PROCESS FOR PRODUCING TETRAGLYCIDYLAMINO COMPOUND |
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