JPS6470450A - Novel nitrogen-containing perfluorocarboxylic fluoride and its preparation - Google Patents
Novel nitrogen-containing perfluorocarboxylic fluoride and its preparationInfo
- Publication number
- JPS6470450A JPS6470450A JP62227468A JP22746887A JPS6470450A JP S6470450 A JPS6470450 A JP S6470450A JP 62227468 A JP62227468 A JP 62227468A JP 22746887 A JP22746887 A JP 22746887A JP S6470450 A JPS6470450 A JP S6470450A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- fluoride
- preparation
- bind
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Hydrogenated Pyridines (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Pyrrole Compounds (AREA)
Abstract
NEW MATERIAL:A compound of formula I (R1, R2 are 1-5C perfluoroalkyl, or they bind to each other directly or through O or N atoms to form a N- containing 5-7-membered ring). EXAMPLE:Perfluoro[3-(N,N-dimethylamino)-n-butyryl fluoride]. USE:A synthetic intermediate of fluorine-compound products such as surface active agents, agrochemicals, or medicines or monomers for fluorine-containing polymers. PREPARATION:A reactive derivative such as an acid halide of 3-dialkylamino-n- butyric acid of formula II (R1', R2' are 1-5C alkyl, they may bind to each other directly or through O or N atom an N-containing heterocycle) is electrolyzed in liquid hydrogen fluoride to give the compound of formula I. In the reaction, the concentration of the compound of formula II is usually 1-80wt.% and the current density is usually 0.01-10A/dm<2>.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62227468A JPS6470450A (en) | 1987-09-10 | 1987-09-10 | Novel nitrogen-containing perfluorocarboxylic fluoride and its preparation |
US07/242,308 US4985556A (en) | 1987-09-10 | 1988-09-09 | Perfluoro(dialkylaminopropene) derivatives |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62227468A JPS6470450A (en) | 1987-09-10 | 1987-09-10 | Novel nitrogen-containing perfluorocarboxylic fluoride and its preparation |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6470450A true JPS6470450A (en) | 1989-03-15 |
JPH0251896B2 JPH0251896B2 (en) | 1990-11-08 |
Family
ID=16861350
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP62227468A Granted JPS6470450A (en) | 1987-09-10 | 1987-09-10 | Novel nitrogen-containing perfluorocarboxylic fluoride and its preparation |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6470450A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5188747A (en) * | 1990-09-04 | 1993-02-23 | Matsushita Electric Industrial Co., Ltd. | Fluorine-containing lubricant compounds |
US5266724A (en) * | 1990-09-04 | 1993-11-30 | Matsushita Electric Industrial Co., Ltd. | Fluorine-containing compounds |
JP2002145846A (en) * | 2000-11-09 | 2002-05-22 | Mitsui Chemicals Inc | Method for manufacturing amino acid fluoride derivative |
JP2020522481A (en) * | 2017-06-09 | 2020-07-30 | アルケマ フランス | High-purity 1,1,1,2,3,3-hexafluoropropane, its production method and its use |
-
1987
- 1987-09-10 JP JP62227468A patent/JPS6470450A/en active Granted
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5188747A (en) * | 1990-09-04 | 1993-02-23 | Matsushita Electric Industrial Co., Ltd. | Fluorine-containing lubricant compounds |
US5266724A (en) * | 1990-09-04 | 1993-11-30 | Matsushita Electric Industrial Co., Ltd. | Fluorine-containing compounds |
JP2002145846A (en) * | 2000-11-09 | 2002-05-22 | Mitsui Chemicals Inc | Method for manufacturing amino acid fluoride derivative |
JP2020522481A (en) * | 2017-06-09 | 2020-07-30 | アルケマ フランス | High-purity 1,1,1,2,3,3-hexafluoropropane, its production method and its use |
US11661387B2 (en) | 2017-06-09 | 2023-05-30 | Arkema France | High-purity 1,1,1,2,3,3-hexafluoropropane, method for producing same and use thereof |
Also Published As
Publication number | Publication date |
---|---|
JPH0251896B2 (en) | 1990-11-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EXPY | Cancellation because of completion of term |