JPS6438A - Method for recovering resorcin - Google Patents

Method for recovering resorcin

Info

Publication number
JPS6438A
JPS6438A JP19135887A JP19135887A JPS6438A JP S6438 A JPS6438 A JP S6438A JP 19135887 A JP19135887 A JP 19135887A JP 19135887 A JP19135887 A JP 19135887A JP S6438 A JPS6438 A JP S6438A
Authority
JP
Japan
Prior art keywords
water
acetone
oil
diisopropylbenzene
resorcin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP19135887A
Other languages
Japanese (ja)
Other versions
JPH0138A (en
Inventor
Takao Ogino
Masayuki Takeda
Masanori Yamamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Petrochemical Industries Ltd
Original Assignee
Mitsui Petrochemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Petrochemical Industries Ltd filed Critical Mitsui Petrochemical Industries Ltd
Priority to JP62-191358A priority Critical patent/JPH0138A/en
Priority claimed from JP62-191358A external-priority patent/JPH0138A/en
Publication of JPS6438A publication Critical patent/JPS6438A/en
Publication of JPH0138A publication Critical patent/JPH0138A/en
Pending legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To obtain high-purity resorcin from an aqueous phase at a high recovery ratio, by decomposing an oxidation product of m-diisopropylbenzene with molecular oxygen with an acid, distilling away acetone, adding a specific compound to the obtained residue and separating an oil from water in the presence of a specific amount of water.
CONSTITUTION: m-Diisopropylbenzene is oxidized with molecular oxygen to provide an oxidation product containing m-diisopropylbenzene dihydroperoxide, which is then decomposed in the presence of an aromatic hydrocarbon solvent (preferably toluene) to distil away acetone. At least one of monohydric phenols, nitriles, cyclic ether compound and water-insoluble dialkyl ketone in an amount so as to provide ≥5pts.wt. based on 100pts.wt. above-mentioned solvent contained in the still residue after removing the acetone is added to separate an oil from water in the presence of water (5W80wt.%, especially 15W60wt.% water concentration) in an amount sufficient to form two liquid phases to recover resorcin from the obtained aqueous phase. In separating the oil from the water, acetone concentration is preferably ≤10wt.%.
COPYRIGHT: (C)1989,JPO&Japio
JP62-191358A 1987-02-17 1987-07-29 How to recover resorcinol Pending JPH0138A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP62-191358A JPH0138A (en) 1987-02-17 1987-07-29 How to recover resorcinol

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP62-32324 1987-02-17
JP3232487 1987-02-17
JP62-191358A JPH0138A (en) 1987-02-17 1987-07-29 How to recover resorcinol

Publications (2)

Publication Number Publication Date
JPS6438A true JPS6438A (en) 1989-01-05
JPH0138A JPH0138A (en) 1989-01-05

Family

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010110482A1 (en) 2009-03-25 2010-09-30 住友化学株式会社 Method of purifying dihydroxybenzene

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010110482A1 (en) 2009-03-25 2010-09-30 住友化学株式会社 Method of purifying dihydroxybenzene
JP2010248180A (en) * 2009-03-25 2010-11-04 Sumitomo Chemical Co Ltd Process for purification of dihydroxybenzene
US8530705B2 (en) 2009-03-25 2013-09-10 Sumitomo Chemical Company, Limited Purification method of dihydroxybenzene

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