JPS633778A - Production of persimmon juice - Google Patents

Production of persimmon juice

Info

Publication number
JPS633778A
JPS633778A JP61146724A JP14672486A JPS633778A JP S633778 A JPS633778 A JP S633778A JP 61146724 A JP61146724 A JP 61146724A JP 14672486 A JP14672486 A JP 14672486A JP S633778 A JPS633778 A JP S633778A
Authority
JP
Japan
Prior art keywords
juice
persimmon
acid
persimmons
persimmon juice
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP61146724A
Other languages
Japanese (ja)
Inventor
Yoshinori Kubo
久保 与▲祇▼則
Takashi Matsuura
隆 松浦
Saburo Niimoto
新本 三郎
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EHIME PREF GOV SEIKA NOGYO KYODO KUMIAI RENGOKAI
Original Assignee
EHIME PREF GOV SEIKA NOGYO KYODO KUMIAI RENGOKAI
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EHIME PREF GOV SEIKA NOGYO KYODO KUMIAI RENGOKAI filed Critical EHIME PREF GOV SEIKA NOGYO KYODO KUMIAI RENGOKAI
Priority to JP61146724A priority Critical patent/JPS633778A/en
Publication of JPS633778A publication Critical patent/JPS633778A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE:To produce clear persimmon juice without forming secondary precipitates, by adding an acid to pressed or strained persimmon juice, enzymically treating and, filtering the treated juice, the heat-treating the filtered juice. CONSTITUTION:Astringent persimmons subjected to astringency removing treatment, sweet persimmons or ripe persimmons are pressed or strained to give persimmon juice and 0.3-0.5% acid, e.g. citric acid, is added to adjust the pH to <=4. 0.02-0.05% enzyme, e.g. soluble pectinase, is then added to the resultant persimmon juice and viscosity of the juice is reduced by keeping at about 40 deg.C for 3-5hr. The resultant juice is further filtered through a diatomaceous earth or ultrafiltered to remove contaminating substances. The filtered juice is then heat-treated at 75-85 deg.C for 10-30sec.

Description

【発明の詳細な説明】 〔発明の背景〕 技術分野 本発明は、柿果?tの製造法に関し、より詳しくは柿の
清澄果汁の製造における二沈殿物の発生を防止した改良
製造法に関する。
[Detailed Description of the Invention] [Background of the Invention] Technical Field The present invention relates to persimmon fruit? More specifically, the present invention relates to an improved production method that prevents the occurrence of two precipitates in the production of clear persimmon juice.

先行技術 本発明は、従来あまり一般的でなかった柿を原料とする
果汁を高品質で提供しようとづるちのであって、この柿
果汁は果汁飲料のみならず神酒、柿酢なとの1II11
副1)各種調味料等の製造にも利用できるものである。
PRIOR ART The present invention is an attempt to provide high quality fruit juice made from persimmons, which have not been commonly used in the past.
Sub-1) It can also be used for manufacturing various seasonings, etc.

柿果汁の製造は、−般に次の工程で行なわれる。The production of persimmon juice is generally carried out in the following steps.

即ら、渋柿を炭酸ガス法、湯抜き法、アルコール法など
により脱渋処理した脱渋果実あるいは月柿、あるいは熟
柿を原料として用い、これを圧搾搾汁機により柿の粗汁
を得るか、あるいはチョッパーパルパー、フイニツシp
−1遠心搾M[により央ごしして柿のピユーレ−を得る
That is, using astringent persimmons that have been treated to remove astringency using a carbon dioxide method, a hot water extraction method, an alcohol method, etc., a moon persimmon, or a ripe persimmon as a raw material, obtain crude persimmon juice using a squeezer, or Or Chopper Pulper, Finitsushi p
-1 Centrifugal squeezing M to obtain persimmon puree.

次に、この粗汁もしくはピユーレ−にベクf−ン分解酵
素を添加したのち、40℃前後で3時間程度加温保持し
て粘度を下げ、これを硅凍上か過機あるいは限外濾過膜
装置によるン濾過によって混濁物質を除去して清澄果汁
を得る。
Next, after adding Vecton-degrading enzyme to this crude juice or puree, it is heated and held at around 40°C for about 3 hours to lower the viscosity, and then filtered using a silica filter or an ultrafiltration membrane device. The turbid substances are removed by filtration to obtain clear juice.

しかしながら、上記の様な工程で得られた柿の清澄果汁
は、製造後1〜2日のうちに沈殿物が発生して製品の品
質を低下さけてしまうことがあった。この沈殿物は、い
わゆる二次沈殿と呼ばれているものであり、綿状ないし
モグナ状で黄褐色を呈するものであるが、暗褐色透明の
上澄部にきわめて浮遊しやすい為に製品の外観を低ドさ
せでしまうのである。
However, in the clarified persimmon juice obtained by the above-described process, a precipitate may be generated within 1 to 2 days after production, resulting in a decrease in the quality of the product. This precipitate is what is called a secondary precipitate, and is flocculent or mogna-like and yellowish brown in color, but it easily floats in the dark brown transparent supernatant, which affects the appearance of the product. This results in a lower level of energy.

よって、飲料業界においてこの二次沈殿の発生を防止す
ることは、品質管理の点において、さらに美観という点
においても大きな課題となっている。
Therefore, preventing the occurrence of secondary precipitation in the beverage industry has become a major issue in terms of quality control and aesthetics.

なお、この二次沈殿による問題は沈殿物を除去づること
によって解決されるが、その為にはさらに再濾過工程お
よび再殺菌密封という工程を設ける必要があった。
Incidentally, the problem caused by this secondary precipitation can be solved by removing the precipitate, but to do so, it is necessary to further provide a re-filtration step and a re-sterilization and sealing step.

〔発明の概要〕[Summary of the invention]

要  旨 本発明者らは、柿果実を圧搾して得た果汁を加熱すると
黄褐色の沈殿物を生じる現象、および柿果汁の殺菌保存
性を向上させる為にpHを下げると沈殿物が発生する現
象を観察し、これらを組み合わゼる事によって、二次沈
殿を防止する事ができる事を見出して本発明を為すに至
った。
Abstract: The present inventors have discovered that when the juice obtained by pressing persimmon fruits is heated, a yellow-brown precipitate is produced, and that the precipitate is produced when the pH is lowered to improve the sterilization preservation of persimmon juice. By observing these phenomena and combining them, the inventors discovered that secondary precipitation can be prevented, leading to the present invention.

即ち、本発明による柿果汁の製造法は、柿果実を搾汁あ
るいは裏ごし処理し、酵素処理したのちろ過して柿果汁
を製造する方法において、ン濾過の前に酸を添加し、そ
の後に熱処理を行って二次沈殿を防止すること、を特徴
とするものである。
That is, the method for producing persimmon juice according to the present invention is a method for producing persimmon juice by squeezing or straining persimmon fruit, treating it with an enzyme, and then filtering it, in which acid is added before filtration, and then heat treatment is performed. This method is characterized by preventing secondary precipitation.

〔発明の詳細な説明〕[Detailed description of the invention]

柿果実 原料である柿は、渋味の有無によって渋柿と甘柿とに大
別することができる。脱渋法とし゛(は炭酸ガス法、瀉
抜き法、アルコール法などがある。
Persimmons, which are a persimmon fruit raw material, can be broadly classified into astringent persimmons and sweet persimmons depending on the presence or absence of astringent taste. Methods for removing astringency include the carbon dioxide method, the purification method, and the alcohol method.

本発明では脱渋していない果実も用いることしできるが
、−膜内に食品としては渋いものは好ましくないので、
原料としては甘柿や脱渋処理した渋柿あるいは熟柿を用
いることが普通である。また脱渋は、目的に反しない限
りいずれの方法も採用することができる。
In the present invention, fruits that have not been removed from astringency can also be used;
As raw materials, it is common to use sweet persimmons, astringent persimmons that have been treated to remove astringency, or ripe persimmons. Further, any method can be used for removing astringency as long as it does not contradict the purpose.

酸 前述の様に本発明は、酵素処理の前あるいは後において
酸を添加してpHを下げ、こののち加熱処理して凝集沈
殿物を発生さけた後、を濾過することによって構成され
る。
Acid As mentioned above, the present invention is constructed by adding an acid to lower the pH before or after the enzyme treatment, followed by heat treatment to avoid the generation of agglomerated precipitates, and then filtration.

本発明で用いることができる酸としては、有機酸、例え
ばリンゴ酸、酒石酸、シュウ酸、コハク酸、クエン酸な
どのジカルボンMを、トリカルボン酸など、また無曙酸
、例えば塩酸、燐酸、炭酸などを挙げることができるが
、特に果実に含まれている酸、たとえばクエン酸、リン
ゴ酸などが好ましい。
Acids that can be used in the present invention include organic acids, such as dicarboxylic acids such as malic acid, tartaric acid, oxalic acid, succinic acid, and citric acid, tricarboxylic acids, and anhydrous acids, such as hydrochloric acid, phosphoric acid, and carbonic acid. Among them, acids contained in fruits, such as citric acid and malic acid, are particularly preferred.

酸の添加は、殺菌保存性を向上さゼる意味からも果汁の
DHが4以下となる様に添加することが好ましい。−般
に搾汁した柿果汁のpHは6前後であるので、酸の添加
量はクエン酸、リンゴ酸等では0.3〜0.5%程度と
なるが、柿の種類、成熟度、その他の条件によっで搾汁
果汁のpHは変動しがちであるので、添加量は上記した
範囲に限定されるものではない。
It is preferable to add acid so that the DH of the fruit juice is 4 or less in order to improve sterilization and storage stability. - Since the pH of squeezed persimmon juice is generally around 6, the amount of acid added is about 0.3 to 0.5% for citric acid, malic acid, etc. However, depending on the type of persimmon, maturity level, etc. Since the pH of the squeezed fruit juice tends to vary depending on the conditions, the amount added is not limited to the above range.

また、酸の添加工程は、酵素処理において使用されるペ
クチン分解酵素の至適pHに応じて決定される。即ち、
最適なpHが4乃至4よりも低い酵素、例えばペクチナ
ーゼでは、酵素処理の前に添加することが好ましく、ま
た最適なOHが4よりも高い酵素、例えばペクチンエス
テラーゼでは、酵素処理の後に添加することもできる。
Further, the acid addition step is determined depending on the optimum pH of the pectinolytic enzyme used in the enzyme treatment. That is,
For enzymes with an optimum pH of 4 to less than 4, such as pectinase, it is preferable to add the enzyme before the enzyme treatment, and for enzymes with an optimum OH higher than 4, such as pectin esterase, to add it after the enzyme treatment. You can also do it.

しかし、酵素処理工程中における微生物による果汁の変
質の危険を避けるという点からは、酸はh9索処理を行
う前に添加しておくことが好ましい。
However, from the viewpoint of avoiding the risk of deterioration of the fruit juice due to microorganisms during the enzyme treatment step, it is preferable to add the acid before performing the H9 cord treatment.

加熱処理 加熱処理は、酸添加による析出物を凝集させ、またベク
ヂン分M l素の活性を失なわける為に行う。加熱が不
十分であると二次沈殿の発生を十分防止する事ができず
、また過度の加熱は果汁のイ5味を劣化させ、色調の褐
色化を招くため好ましくない。従って、加熱温度として
は75〜85℃が好ましく、また加熱時間としては30
〜10秒が好ましい。なお加熱温度が低ければ長い加熱
時間が必要とされ、また加熱温度が高ければ短い加熱時
間で十分である事は言うよ′r−らない。
Heat Treatment The heat treatment is carried out in order to coagulate the precipitates caused by the addition of the acid and to eliminate the activity of the Bekudin component M1. Insufficient heating will not sufficiently prevent the occurrence of secondary precipitation, while excessive heating will deteriorate the taste of the fruit juice and cause the color to turn brown, which is undesirable. Therefore, the heating temperature is preferably 75 to 85°C, and the heating time is 30°C.
~10 seconds is preferred. It goes without saying that if the heating temperature is low, a long heating time is required, and if the heating temperature is high, a short heating time is sufficient.

酵素処理 搾汁した柿果?Iにはペクチンが存在し、強い保護コロ
イド作用を有し、混入した果実の組織の微細片を含有し
て安定な混濁を保っている。よって、透明な柿果汁を得
るにG、L清澄化の為の処理が必要とされており、その
主なものとしてはペクチン分解酵素を用いたーものがあ
る。そして通常その処理は、ペクチン分解酵素を0.0
2〜0.05%の濃度で添加し、40℃前後で3〜5時
間保持する事によって行われている。
Enzyme treated persimmon juice? Pectin is present in I, which has a strong protective colloid effect, and contains fine pieces of contaminated fruit tissue to maintain stable turbidity. Therefore, in order to obtain transparent persimmon juice, a treatment for G and L clarification is required, and the main treatment involves the use of pectin-degrading enzymes. The process usually involves using pectinolytic enzymes at 0.0
This is done by adding at a concentration of 2 to 0.05% and holding it at around 40°C for 3 to 5 hours.

また、単一の酵素の使用だけでは処理が十分でない場合
には複数のペクチン分wI酔累の併用が有効な事、また
セルラーゼ、アミラーゼ、プロテアーゼ、タンニン、ゼ
ラチン等を添加する事によって清澄化が促進される事が
見出されている。よって、本発明で酵素処理とは、単一
のペクチン分解酵素を用いた場合のみならず、複数の′
P!!l索をat用した場合および上記の様な添加物を
用いた場合をも含めて色°うものとする。
In addition, if the treatment is not sufficient with the use of a single enzyme, it is effective to use a combination of multiple pectin components, and clarifying can be achieved by adding cellulases, amylases, proteases, tannins, gelatin, etc. It has been found that it is promoted. Therefore, in the present invention, enzymatic treatment refers not only to the use of a single pectin-degrading enzyme, but also to the use of multiple pectinolytic enzymes.
P! ! This also applies to cases where AT is used as a lubricant and cases where additives such as those mentioned above are used.

〔実施例〕〔Example〕

渋柿(愛宕)100?lをポリエチレン類の袋に入れ、
35%エタノール11を噴霧したのち、40±3℃にて
3日間保存して脱渋した。これを沸騰水中で10分間温
煮して果実を軟化したのち、圧搾搾汁して粗果汁61幻
を得た。次いでクエン酸0.2に9を添加してl) H
4とし、これを40℃に加温して可溶性ペクチナーゼ(
タナベ)を0.02%加え4時間保存してN素処理を行
った。これを80℃ 30秒にて加熱処理し、凝集物の
発生を確認して冷却ののち、ラジオライトを使用して硅
藻土か過を行って、清澄果汁57に3を得た。
Astringent persimmon (Atago) 100? Put l into a polyethylene bag,
After spraying 35% ethanol 11, it was stored at 40±3°C for 3 days to remove astringency. The fruit was boiled in boiling water for 10 minutes to soften the fruit, and then the fruit was squeezed to obtain crude fruit juice 61. Then add 9 to 0.2 of citric acid to make l) H
4 and heated to 40°C to extract soluble pectinase (
Tanabe) was added at 0.02% and stored for 4 hours to perform N treatment. This was heat-treated at 80° C. for 30 seconds, and after cooling after confirming the generation of aggregates, it was filtered through diatomaceous earth using Radiolite to obtain clarified fruit juice 57 to 3.

本製品は、屈折度16” BX、pH4、酸度0.35
%で60日間室温で保管後ら沈殿物の発生は全く見られ
ず、また透明度も良好であった。
This product has a refractive index of 16” BX, pH 4, and acidity 0.35.
%, no precipitation was observed after storage at room temperature for 60 days, and the transparency was also good.

効  果 本発明の様に酵素処理の前あるいは後に酸添加および熱
処理を行うことにより、製造直後から保存流通の段階に
おいて沈殿物の発生がないため、品質が一定で外観も良
好な柿の清澄果汁を得ることができる。
Effect: By performing acid addition and heat treatment before or after enzyme treatment as in the present invention, no precipitate is generated immediately after production and during storage and distribution, resulting in clear persimmon juice with constant quality and good appearance. can be obtained.

従って、飲料業界における柿果汁の二次沈殿防止という
課題を解決することができた。また、このことによって
、従来法における二次沈殿の再ン濾過除去および再殺菌
密封という工程を不要とし、工業的生産性の向上に寄与
するところが大きい。
Therefore, the problem of preventing secondary precipitation of persimmon juice in the beverage industry could be solved. Furthermore, this eliminates the need for the steps of re-filtration and re-sterilization sealing of the secondary precipitate in the conventional method, which greatly contributes to improving industrial productivity.

また、製品の品質が一定した美しい透明性を保持した柿
果汁を提供したため、各種の果実飲料ならびに神酒、柿
酢などの醸造品にも柿果汁の新たな用途を開き、社会的
、経済的にも貢献するところ大なるものがある。
In addition, because we have provided persimmon juice with consistent product quality and beautiful transparency, we have opened up new uses for persimmon juice in various fruit drinks and brewed products such as sacred sake and persimmon vinegar, contributing to social and economic benefits. There is also a great contribution to make.

Claims (1)

【特許請求の範囲】 1、柿果実を搾汁あるいは裏ごし処理し、酵素処理した
のちろ過して柿果汁を製造する方法において、ろ過の前
に酸を添加し、その後に熱処理を行つて二次沈殿を防止
することを特徴とする、柿果汁の製造法。 2、酸の添加を酵素処理の前に行うことを特徴とする、
特許請求の範囲第1項に記載の方法。
[Scope of Claims] 1. A method for producing persimmon juice by squeezing or straining persimmon fruit, treating it with enzymes, and then filtering it, in which an acid is added before filtration, and then heat treatment is performed to produce secondary juice. A method for producing persimmon juice, which is characterized by preventing precipitation. 2. Characterized by adding acid before enzyme treatment,
A method according to claim 1.
JP61146724A 1986-06-23 1986-06-23 Production of persimmon juice Pending JPS633778A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP61146724A JPS633778A (en) 1986-06-23 1986-06-23 Production of persimmon juice

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP61146724A JPS633778A (en) 1986-06-23 1986-06-23 Production of persimmon juice

Publications (1)

Publication Number Publication Date
JPS633778A true JPS633778A (en) 1988-01-08

Family

ID=15414128

Family Applications (1)

Application Number Title Priority Date Filing Date
JP61146724A Pending JPS633778A (en) 1986-06-23 1986-06-23 Production of persimmon juice

Country Status (1)

Country Link
JP (1) JPS633778A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010025936A (en) * 1999-09-01 2001-04-06 왕정환 The Method of making water sweet persimnon and sweet persimmon pure.
JP2008194021A (en) * 2007-02-10 2008-08-28 Fancl Corp Soluble calcium component derived from plant, and method for producing the same
US20100240600A1 (en) * 2007-06-12 2010-09-23 Hiroshima University Anti-Norovirus Agent and Composition Containing the Same
WO2012131129A1 (en) * 2011-03-25 2012-10-04 Consejo Superior De Investigaciones Científicas (Csic) Persimmon-derived food products and production method thereof
KR102091841B1 (en) * 2019-10-11 2020-03-20 주식회사 대신물산 Sweet persimmon juice and preparation method thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010025936A (en) * 1999-09-01 2001-04-06 왕정환 The Method of making water sweet persimnon and sweet persimmon pure.
JP2008194021A (en) * 2007-02-10 2008-08-28 Fancl Corp Soluble calcium component derived from plant, and method for producing the same
US20100240600A1 (en) * 2007-06-12 2010-09-23 Hiroshima University Anti-Norovirus Agent and Composition Containing the Same
US8431168B2 (en) * 2007-06-12 2013-04-30 Hiroshima University Anti-norovirus agent and composition containing the same
US8790718B2 (en) 2007-06-12 2014-07-29 Hiroshima University Method of disinfection or infection control against norovirus
WO2012131129A1 (en) * 2011-03-25 2012-10-04 Consejo Superior De Investigaciones Científicas (Csic) Persimmon-derived food products and production method thereof
ES2389067A1 (en) * 2011-03-25 2012-10-23 Consejo Superior De Investigaciones Científicas (Csic) Persimmon-derived food products and production method thereof
KR102091841B1 (en) * 2019-10-11 2020-03-20 주식회사 대신물산 Sweet persimmon juice and preparation method thereof

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