JPS63302285A - Drier for powder - Google Patents
Drier for powderInfo
- Publication number
- JPS63302285A JPS63302285A JP13684587A JP13684587A JPS63302285A JP S63302285 A JPS63302285 A JP S63302285A JP 13684587 A JP13684587 A JP 13684587A JP 13684587 A JP13684587 A JP 13684587A JP S63302285 A JPS63302285 A JP S63302285A
- Authority
- JP
- Japan
- Prior art keywords
- powder
- gas
- vertical container
- closed vertical
- heating source
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000843 powder Substances 0.000 title claims description 47
- 239000006185 dispersion Substances 0.000 claims description 22
- 238000001035 drying Methods 0.000 claims description 22
- 239000000463 material Substances 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 10
- 239000000428 dust Substances 0.000 claims description 7
- 238000007664 blowing Methods 0.000 claims description 4
- 230000003213 activating effect Effects 0.000 claims description 2
- 239000007789 gas Substances 0.000 description 35
- 239000002184 metal Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 3
- 230000005587 bubbling Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000009491 slugging Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000013019 agitation Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
Landscapes
- Drying Of Solid Materials (AREA)
Abstract
(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.
Description
【発明の詳細な説明】 〈産業上の利用分野〉 本発明は粉体の乾燥装置に関する。[Detailed description of the invention] <Industrial application field> The present invention relates to a powder drying device.
粉体を取扱う食品、医薬品、樹脂、更には新素材等の業
界では、該粉体を乾燥することが日常的に行なわれるが
、いうまでもなく、該乾燥によって所期の通りの均質な
製品の得られることが要請される。特に近年の多様化し
た高技術製品時代では、乾燥を行なうそれぞれの具体的
場面において、かかる要請が一層強い。In the food, pharmaceutical, resin, and new materials industries that handle powder, it is common practice to dry the powder. It is requested that the following be obtained. Particularly in the recent era of diversified high-tech products, such demands are becoming stronger in each specific drying situation.
本発明は上記のような要請に応える粉体の乾燥装置に関
するものである。The present invention relates to a powder drying apparatus that meets the above requirements.
〈従来の技術、その問題点〉
従来、粉体の乾燥装置として、静置式、回転式、気流式
、4IJl拌式、噴霧式、流動層式等、種々の形式の装
置が、粉体の性状や乾燥目的等との関係で、適宜に選択
使用されている。これらの従来装置はそれぞれに相応の
利点を有するが、その反面で、静置式の従来装置には乾
燥に要する時間が長いという問題点があり、また回転式
、気流式、攪拌式の各従来装置には微粉の発塵が多く、
場合によっては粉体の破壊や切断を引き起こすという問
題点があり、更に噴霧式の従来装置にはその付帯設備も
含めて装置規模が大き過ぎるという問題点があり、そし
て流動層式の従来装置には、とりわけ粉体が30周履程
度以下の微粉である場合に、該粉体を安定して流動化す
ること自体が困難で、したがって実用に供し難いという
問題点がある。<Prior art and its problems> Conventionally, various types of drying equipment for powder, such as a static type, a rotating type, an air flow type, a 4IJl stirring type, a spray type, and a fluidized bed type, have been used to dry powder. It is used selectively depending on the drying purpose, etc. Each of these conventional devices has its own merits, but on the other hand, the stationary type conventional devices have the problem of long drying times, and the rotary, air flow, and agitation types conventional devices There is a lot of fine dust,
In some cases, the powder may be broken or cut.Furthermore, conventional spray-type equipment has the problem of being too large, including its ancillary equipment, and conventional fluidized-bed equipment has the problem of being too large. However, especially when the powder is a fine powder of about 30 cycles or less, it is difficult to stably fluidize the powder, and therefore it is difficult to put it into practical use.
〈発明が解決しようとする問題点、その解決手段〉
本発明は叙上の如き従来の問題点を解決する新たな乾燥
装置を提供するものである。<Problems to be Solved by the Invention and Means for Solving the Problems> The present invention provides a new drying device that solves the conventional problems as described above.
しかして本発明は、
振動発生源及び主加熱源を装備する密閉系竪型容器があ
る種の自由運動を与えられるようにスプリングの如き弾
性体で支持されており、該密閉系竪型容器には原料供給
口及び形成される粉体の流動層高よりも上方に気体排出
口並びに該流動層高内に製品排出口が開設され、また該
製品排出口の下方に気体分散材が装着されていて、更に
該気体分散材の下方には副加熱源を装備する気体送入路
が配管されており、振動発生源及び主加熱源を機f@さ
せて密閉系竪型容器を振動及び加熱させるその一方で副
加熱源を機能させて気体送入路から気体分散材を介し密
閉系竪型容器内へ加熱気体を吹き込むことにより、原料
供給口から供給した粉体を流動化させつつ加熱雰囲気下
で乾燥するように構成してなる粉体の乾燥装置に係る。Therefore, the present invention provides a system in which a closed vertical container equipped with a vibration generation source and a main heating source is supported by an elastic body such as a spring so as to give a certain kind of free movement to the closed vertical container. A gas discharge port is provided above the raw material supply port and the height of the fluidized bed for the powder to be formed, and a product discharge port is provided within the fluidized bed height, and a gas dispersion material is installed below the product discharge port. Furthermore, a gas inlet passage equipped with a sub-heating source is piped below the gas dispersion material, and the vibration generation source and the main heating source are activated to vibrate and heat the closed vertical container. On the other hand, by activating the auxiliary heating source and blowing heated gas into the closed vertical container from the gas supply path through the gas dispersion material, the powder supplied from the raw material supply port is fluidized and kept in a heated atmosphere. The present invention relates to a powder drying device configured to dry powder.
本発明において肝要な点は、粉体が従来の流動層装置で
はその流動化が不可能といわれる数ILm〜数十終腸の
微粉であっても、該粉体にある種の自由運動を与える振
動を加え、併せて該粉体に分散気体を下方から吹き込む
と、該粉体は、バブリングやスラッギングの少ない、あ
たかも液体の如き安定した流動層を形成するという特有
の現象を活用し、かかる現象下、該流動層高内において
加熱雰囲気下に粉体の均質な乾燥を具現させる処にある
。The important point in the present invention is that even if the powder is a fine powder with a size of several ILm to several tens of ILm, which is said to be impossible to fluidize with a conventional fluidized bed device, a certain kind of free movement is imparted to the powder. By applying vibration and at the same time blowing a dispersion gas into the powder from below, the powder forms a stable fluidized bed, almost like a liquid, with little bubbling or slugging. The second step is to achieve homogeneous drying of the powder in a heated atmosphere within the fluidized bed.
以下、図面に基いて本発明の構成を更に詳細に説明する
。Hereinafter, the configuration of the present invention will be explained in more detail based on the drawings.
〈実施例〉
第1図は本発明の一実施例を一部断面状態でjlす全体
図である0円筒状の密閉系竪型容器11が取付枠12に
立設されており、振動モータ13を装備する該取付枠1
2はスプリング14a、14bで基台15に支持されて
いる。密閉系竪型容器11には、その上方から下方へ順
に、気体排出口21、原料供給口22a、22b、及び
製品排出口23が開設され、その側周面に主加熱源とし
て加熱用熱媒体の流通可能なジャケット31が装備され
ており、製品排出口23の下方に気体分散材41が装着
されていて、気体分散材41の更に下方に副加熱源とし
てヒータ51を装備する気体送入路61が配管されてい
る。この場合、気体分散。<Embodiment> FIG. 1 is an overall view, partially in section, of an embodiment of the present invention. A cylindrical closed vertical container 11 is erected on a mounting frame 12, and a vibration motor 13 The mounting frame 1 equipped with
2 is supported by a base 15 with springs 14a and 14b. The closed vertical container 11 is provided with a gas outlet 21, raw material supply ports 22a, 22b, and a product outlet 23 in this order from the top to the bottom, and a heating medium is provided as a main heating source on the side circumferential surface thereof. A gas dispersion material 41 is installed below the product discharge port 23, and a heater 51 is provided as an auxiliary heat source further below the gas dispersion material 41. 61 is piped. In this case, gas dispersion.
材41は中央部の気体分散材41aとその周部の気体分
散材41bとに2分割されており、それぞれの気体分散
材41a、41bを介し密閉系竪型容器11内へ吹き込
まれる気体の温度及び量がヒータ51および付帯のコン
プレッサ71並びにバルブ81a、81b、81cによ
ってル制御され得るようになっている。そして、いずれ
も後述する粉体Aの流動層高との関係で、気体排出口2
1は該流動層高よりも上方に、また製品排出[]23は
該流動層高内に、それぞれ配置されている。The material 41 is divided into two parts, a gas dispersion material 41a at the center and a gas dispersion material 41b at the periphery. and the amount can be controlled by the heater 51 and the associated compressor 71 and valves 81a, 81b, 81c. In both cases, due to the height of the fluidized bed of powder A, which will be described later,
1 is located above the fluidized bed height, and the product discharge [ ] 23 is located within the fluidized bed height.
振動モータ13を稼動させて密閉系竪型容器11を振動
させ、したがって気体分散材41も振動させて、更に気
体送入路61から気体分散材41を介し密閉系竪型容器
11内へ気体を吹き込むと、密閉系竪型容器11内の粉
体Aはあたかも液体の如き安定した流動層を形成するの
で、かかる流動層高内においてジャケット31及びヒー
タ51による加熱雰囲気下に粉体Aを充分均質に乾燥す
る構成である。The vibration motor 13 is operated to vibrate the closed vertical container 11, and therefore the gas dispersion material 41 is also vibrated, and gas is further introduced into the closed vertical container 11 from the gas supply path 61 via the gas dispersion material 41. When the powder A is blown into the closed vertical container 11, it forms a stable fluidized bed as if it were a liquid. It is configured to dry quickly.
第2図は、本発明の他の一実施例を一部断面状態で示す
全体図である。下部が逆円錐状に絞り込まれた円筒状の
密閉系竪型容器16の下・端に振動モータ18が装備さ
れ、該密閉系竪型容器16は取付枠17に立設されてい
て、取付枠17はスプリング19a、19bで基台20
に支持されている。密閉系竪型容器16には、その上方
から下方へ順に、気体排出口24、微粉返送口25、原
料供給口26、及び製品排出口27が開設され、その側
周面に主加熱源として加熱用熱媒体の流通可能なジャケ
ット32が装備されていて、製品排出口27の下方に気
体分散材42が装着されており、気体分散材42の更に
下方にブロア72及びバルブ82aを付帯して副加熱源
としてのヒータ52を装備する気体送入路62が配管さ
れている。FIG. 2 is an overall view, partially in section, of another embodiment of the present invention. A vibration motor 18 is installed at the bottom and end of a cylindrical closed vertical container 16 whose lower part is narrowed into an inverted conical shape, and the closed vertical container 16 is erected on a mounting frame 17. 17 is a base 20 with springs 19a and 19b.
is supported by The closed vertical container 16 has a gas discharge port 24, a fine powder return port 25, a raw material supply port 26, and a product discharge port 27 opened in this order from the top to the bottom, and the side circumferential surface of the container 16 is heated as a main heating source. A gas dispersion material 42 is installed below the product discharge port 27, and a blower 72 and a valve 82a are attached below the gas dispersion material 42 to provide a sub-assembly. A gas inlet passage 62 equipped with a heater 52 as a heat source is provided.
そして、第1図の場合と同様、加熱雰囲気下に流動化す
る粉体Bの流動層高よりも上方に開設された気体排出口
24は集塵器91へと連結され、気体排出口24から気
体に同伴して飛散する微粉を集塵器91で回収した後、
該微粉をバルブ82bを介して微粉返送口25へと返送
し、また原料供給口26はスクリューフィーダ92aを
介して原料貯蔵容器92へと連結され、原料貯蔵容器9
2内の粉体Bをスクリューフィーダ92aで原料供給口
26へと連続的に定量供給し、更に製品排出口27は密
閉系竪型容器16の外部から粉体Bの流動層高内へと挿
入されたパイプの先端に開設され、該流動層高内におい
て均質に乾燥された製品を集塵器93及びバルブ82c
を介して回収するようになっている。As in the case of FIG. 1, the gas outlet 24 opened above the height of the fluidized bed of the powder B fluidized in the heated atmosphere is connected to the dust collector 91, and the gas outlet 24 is connected to the dust collector 91. After collecting the fine particles scattered along with the gas in the dust collector 91,
The fine powder is returned to the fine powder return port 25 via the valve 82b, and the raw material supply port 26 is connected to the raw material storage container 92 via the screw feeder 92a.
Powder B in 2 is continuously fed in a fixed amount to the raw material supply port 26 by the screw feeder 92a, and the product discharge port 27 is inserted into the fluidized bed height of the powder B from the outside of the closed vertical container 16. A dust collector 93 and a valve 82c are installed at the tip of the pipe to collect the product homogeneously dried in the fluidized bed height.
It is designed to be collected through.
いうまでもないが、図示した実施例は本発明の好適例で
あり、本発明が該実施例に限定されるというものではな
い。図示を省略するが、振動モータで代表される振動発
生源やスプリングで代表される弾性体の個数、ジャケッ
トやコイル更にはヒータで代表される加熱手段等は、例
えば粉体の性状、密閉系竪型容器の形状や大きさ、乾燥
目的等との関係で適宜に選択され、必要に応じて適宜に
併用され得る。また気体分散材は、それぞれの1−1的
に応じた開「1径を有するパンチングメタル、焼結金属
、素焼、濾布等が適宜に使用され得る。そして、粉体の
性状や乾燥目的との関係で、密閉系竪型容器内へ吹き込
む気体を不活性ガスにしたり、或は該密閉系竪型容器内
を加圧下又は減圧下に操作することもできる。Needless to say, the illustrated embodiment is a preferred example of the present invention, and the present invention is not limited to this embodiment. Although not shown in the drawings, the vibration generation source represented by a vibration motor, the number of elastic bodies represented by springs, the heating means represented by jackets and coils, and heaters, etc. They are appropriately selected depending on the shape and size of the mold container, the purpose of drying, etc., and can be used in combination as appropriate. Further, as the gas dispersion material, punching metal, sintered metal, unglazed metal, filter cloth, etc. having an open diameter of 1-1 mm can be used as appropriate depending on the properties of the powder and the purpose of drying. For this reason, the gas blown into the closed vertical container can be an inert gas, or the inside of the closed vertical container can be operated under pressurized or reduced pressure.
く作用〉
次に、本発明の作用をf51図に示した実施例の具体的
使用状態で説IJTする。直径300 +wmX高さ6
00mmの密閉系竪型容器11内へ、平均粒径1OJL
a+、真比改0.8g/mJl 嵩比屯0.2g/■文
、湿分lO%の合成樹脂粉体を、原料供給口22a、2
2bから高さ200■■まで供給した、気体分散材41
a、41bはともに平均開口径5ル諺の多孔質金属板で
ある。振動モータ13を稼動させて、密閉系竪型容器1
1に全振幅1.5smX振動数100H2で斜め上方の
振動を加え、併せてジャケラ)31に80℃のスチーム
を流通させ、またヒータ51で80℃に加熱した除湿空
気を気体分散材41aを介し12見/分、気体分散材4
1bを介し81/分の割合で吹き込んだ、乾燥当初、粉
体は表面が平面状に盛り上がり、バブリングやスラッギ
ングの少ない流動層を形成し、該流動層内には明らかな
攪拌乃至旋回運動が認められ、盛り上がった粉体の表面
からは無数の小気泡が発生していた。かかる流動層の形
成は乾燥が進むに伴なってより安定化し、乾燥の最終段
階では該流動層があたかも液体の如き様相を呈し、その
層高は運転開始前に比べて約1.5倍にまで盛り上がっ
ていた。30分間運転した後、製品排出口23から回収
した製品は、湿分0.01%以下であり、その性状は極
めて良好であった。Functions> Next, the functions of the present invention will be explained with reference to a specific usage state of the embodiment shown in Fig. f51. Diameter 300 +wm x height 6
00mm sealed vertical container 11, average particle size 1OJL
Synthetic resin powder with a+, Shinhi Kai 0.8g/mJl, Kahitun 0.2g/■bun, and moisture content 1O% is fed to the raw material supply ports 22a, 2
Gas dispersion material 41 supplied from 2b to height 200■■
Both a and 41b are porous metal plates with an average opening diameter of 5 mm. By operating the vibration motor 13, the closed vertical container 1
1 is subjected to diagonal upward vibration with a total amplitude of 1.5 sm and a frequency of 100 H2, and at the same time, steam at 80°C is passed through the jacket 31, and dehumidified air heated to 80°C by the heater 51 is passed through the gas dispersion material 41a. 12 views/min, gas dispersion material 4
1b at a rate of 81/min. At the beginning of drying, the powder surface swelled into a planar shape, forming a fluidized bed with little bubbling or slugging, and clear stirring or swirling movement was observed within the fluidized bed. Countless small bubbles were generated from the surface of the powder. The formation of such a fluidized bed becomes more stable as the drying progresses, and at the final stage of drying, the fluidized bed appears as if it were a liquid, and the height of the bed is approximately 1.5 times higher than before the start of operation. It was so exciting. After running for 30 minutes, the product recovered from the product outlet 23 had a moisture content of 0.01% or less, and its properties were extremely good.
〈発明の効果〉
以上説明した通りであるから、本発明には、機械的振動
と気体の吹き込みとの相乗作用で粉体を流動化させるこ
とにより、該粉体が数十fiLm〜数ド■以下の微粉で
あっても、比較的少量の吹き込み気体で短時間に均質な
乾燥品を得ることができ、しかも乾燥に際して粉体の破
壊や切断を引き起こすこともないという優れた効果があ
る。<Effects of the Invention> As explained above, the present invention has the following advantages: By fluidizing the powder by the synergistic effect of mechanical vibration and gas blowing, the powder can be reduced to several tens of fiLm to several dots. Even with the following fine powders, a homogeneous dried product can be obtained in a short time with a relatively small amount of blown gas, and there is an excellent effect that the powder does not break or break during drying.
第1図と第2図は未発IIの各別の一実施例を一部断面
状態で示す全体図である。
11.16・・密閉系竪型容器
12.17・・取付枠、13.18・・振動モータ14
a、i4b、19a、19b・−スプリング15.20
−・基台、21.24・・気体排出口22a、22b、
26・・原ネ4供給口23.27・・製品排出[]
31.32・・ジャケット
41a、41b、42−気体分散材
51.52・・ヒータ、61.62・・気体送入路81
a〜81C982a〜82C・・バルブ91.93・・
集塵器、A、B・・粉体特許出願人 中央化工機株式会
社
代理人 弁理士 入 山 宏 正
第1図
履(3)面9しFIG. 1 and FIG. 2 are overall views, partially in cross section, of different embodiments of the unreleased II. 11.16... Closed vertical container 12.17... Mounting frame, 13.18... Vibration motor 14
a, i4b, 19a, 19b・-Spring 15.20
-・Base, 21.24・・Gas outlet 22a, 22b,
26...Raw energy 4 supply port 23.27...Product discharge [] 31.32...Jacket 41a, 41b, 42-gas dispersion material 51.52...Heater, 61.62...Gas feed path 81
a~81C982a~82C...Valve 91.93...
Dust collector, A, B... Powder patent applicant Chuo Kakoki Co., Ltd. Agent Patent attorney Hiroshi Iriyama Figure 1, page 3, page 9
Claims (1)
がある種の自由運動を与えられるようにスプリングの如
き弾性体で支持されており、該密閉系竪型容器には原料
供給口及び形成される粉体の流動層高よりも上方に気体
排出口並びに該流動層高内に製品排出口が開設され、ま
た該製品排出口の下方に気体分散材が装着されていて、
更に該気体分散材の下方には副加熱源を装備する気体送
入路が配管されており、振動発生源及び主加熱源を機能
させて密閉系竪型容器を振動及び加熱させるその一方で
副加熱源を機能させて気体送入路から気体分散材を介し
密閉系竪型容器内へ加熱気体を吹き込むことにより、原
料供給口から供給した粉体を流動化させつつ加熱雰囲気
下で乾燥するように構成してなる粉体の乾燥装置。 2、主加熱源が密閉系竪型容器に周設されたジャケット
又はヒータである特許請求の範囲第1項記載の粉体の乾
燥装置。 3、主加熱源が密閉系竪型容器に内装されたコイル又は
ヒータである特許請求の範囲第1項記載の粉体の乾燥装
置。 4、密閉系竪型容器がその上部よりも下部が絞り込まれ
たものである特許請求の範囲第1項〜第3項のいずれか
一つの項記載の粉体の乾燥装置。 5、気体排出口に集塵器が連結された特許請求の範囲第
1項〜第4項のいずれか一つの項記載の粉体の乾燥装置
。 6、気体分散材が2分割されたものである特許請求の範
囲第1項〜第5項のいずれか一つの項記載の粉体の乾燥
装置。 7、密閉系竪型容器が減圧下又加圧下で操作されるもの
である特許請求の範囲第1項〜第6項のいずれか一つの
項記載の粉体の乾燥装置。[Claims] 1. A closed vertical container equipped with a vibration generation source and a main heating source is supported by an elastic body such as a spring so as to give a certain kind of free movement, and the closed vertical container is equipped with a vibration generating source and a main heating source. The container has a raw material supply port, a gas discharge port above the height of the fluidized bed of powder to be formed, and a product discharge port within the fluidized bed height, and a gas dispersion material is installed below the product discharge port. has been,
Furthermore, a gas supply path equipped with a sub-heating source is installed below the gas dispersion material, and the vibration generating source and the main heating source function to vibrate and heat the closed vertical container. By activating the heating source and blowing heated gas into the closed vertical container from the gas supply path through the gas dispersion material, the powder supplied from the raw material supply port is fluidized and dried in a heated atmosphere. A powder drying device consisting of: 2. The powder drying apparatus according to claim 1, wherein the main heating source is a jacket or a heater provided around a closed vertical container. 3. The powder drying apparatus according to claim 1, wherein the main heating source is a coil or heater housed in a closed vertical container. 4. The powder drying apparatus according to any one of claims 1 to 3, wherein the closed vertical container is narrower at the bottom than at the top. 5. The powder drying apparatus according to any one of claims 1 to 4, wherein a dust collector is connected to the gas outlet. 6. The powder drying apparatus according to any one of claims 1 to 5, wherein the gas dispersion material is divided into two parts. 7. The powder drying apparatus according to any one of claims 1 to 6, wherein the closed vertical container is operated under reduced pressure or increased pressure.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13684587A JPS63302285A (en) | 1987-05-29 | 1987-05-29 | Drier for powder |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13684587A JPS63302285A (en) | 1987-05-29 | 1987-05-29 | Drier for powder |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS63302285A true JPS63302285A (en) | 1988-12-09 |
Family
ID=15184848
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP13684587A Pending JPS63302285A (en) | 1987-05-29 | 1987-05-29 | Drier for powder |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS63302285A (en) |
-
1987
- 1987-05-29 JP JP13684587A patent/JPS63302285A/en active Pending
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