JPS63239136A - Production of inorganic fiber - Google Patents

Production of inorganic fiber

Info

Publication number
JPS63239136A
JPS63239136A JP7564987A JP7564987A JPS63239136A JP S63239136 A JPS63239136 A JP S63239136A JP 7564987 A JP7564987 A JP 7564987A JP 7564987 A JP7564987 A JP 7564987A JP S63239136 A JPS63239136 A JP S63239136A
Authority
JP
Japan
Prior art keywords
centrifugal acceleration
content
fiber
particles
average
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP7564987A
Other languages
Japanese (ja)
Inventor
Ryoji Takagi
良二 高木
Seiichi Myojin
明神 清一
Toru Kurita
亨 栗田
Hidetoki Noguchi
野口 秀時
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Chemical and Materials Co Ltd
Original Assignee
Nippon Steel Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Chemical Co Ltd filed Critical Nippon Steel Chemical Co Ltd
Priority to JP7564987A priority Critical patent/JPS63239136A/en
Publication of JPS63239136A publication Critical patent/JPS63239136A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/04Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor
    • C03B37/05Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor by projecting molten glass on a rotating body having no radial orifices
    • C03B37/055Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor by projecting molten glass on a rotating body having no radial orifices by projecting onto and spinning off the outer surface of the rotating body

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Glass Compositions (AREA)

Abstract

PURPOSE:To reduce the content of particles in the formed fiber and to improve the quality of the fiber by increasing the centrifugal acceleration or peripheral velocity of the rotary drum of a multistage rotary drum type centrifugal fiberizing device in the production of inorg. fiber by the device. CONSTITUTION:The melt as the material for producing the inorg. fiber such as rock wool and glass wool is supplied to the multistage rotary drum type centrifugal fiberizing device, and inorg. fiber is produced. In this case, the centrifugal acceleration or peripheral velocity of the rotary drum is increased to reduce the content of the particles in the inorg. fiber. As a concrete production method, the mean centrifugal acceleration of the rotary drum from the second stage on is increased to >=10X10<3>G, hence the content of the particles having >=88mu diameter in the inorg. fiber can be reduced to <=20%, and the content of the particles having >=177mu diameter in the inorg. fiber can be reduced to <=10% by increasing the acceleration to >=15X10<3>G.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は無機繊維の繊維化方法に関する。[Detailed description of the invention] [Industrial application field] The present invention relates to a method for forming inorganic fibers.

更に詳しくは無Rm帷中に混入する未繊維化粒子を低減
させる!IlN化方法に関する。
More specifically, it reduces unfiberized particles mixed into Rm-free cloth! This invention relates to an IINization method.

〔従来の技術〕[Conventional technology]

ロックウール、グラスウール、スラグウール、ミネラル
ウール等の名称で呼ばれている無RIJ& ’+Lは、
原料の溶融物を種々の形状の回転体に接触させたり、流
下させたりして繊維化している。特に多段回転ドラムの
円周面に流下させて繊維化する装置は一般的に使用され
ている。
Non-RIJ&'+L is called rock wool, glass wool, slag wool, mineral wool, etc.
The molten raw material is made into fibers by bringing it into contact with rotating bodies of various shapes or by flowing it down. In particular, devices are commonly used that produce fibers by flowing them down onto the circumferential surface of a multi-stage rotating drum.

多段回転ドラム型遠心繊維化装置は、回転軸が互いに平
行で、通常水平にぞして各段のドラムを前面より見て千
鳥状に配置した2〜5個の比較的厚さが薄く、内部水冷
された円筒形の回転ドラムを高速で回転させる。
A multi-stage rotating drum type centrifugal fiberizing device consists of two to five relatively thin drums arranged horizontally in a staggered manner, with rotating axes parallel to each other and viewed from the front of each drum. A water-cooled cylindrical rotating drum is rotated at high speed.

一方、キュポラ、電気炉などの原料溶融装置で溶融した
溶融物を第1段の回転ドラムの円周面に供給し、順次下
方の第2段、第3段等の各ドラムの円周面に移して薄く
展延させ、遠心力により各ドラムから繊維を放出させる
On the other hand, the molten material melted by a raw material melting device such as a cupola or electric furnace is supplied to the circumferential surface of the first stage rotating drum, and then sequentially applied to the circumferential surface of each of the lower drums such as the second and third stages. The fibers are transferred and spread thinly, and centrifugal force releases the fibers from each drum.

従来、回転ドラムの平均遠心加速度(rω2、但しrは
ドラム半径、ωは角速度、でありm力の加速度Gの倍数
で表示する)は通常4.5〜7.0X10”Gで運転さ
れている。この時の繊維中に混入する未繊維化粒子(通
常ショットと称し、秤々の大きさによって表示されるが
、代表的に88μ以上のショットの含有率であられす。
Conventionally, the average centrifugal acceleration of the rotating drum (rω2, where r is the drum radius and ω is the angular velocity, expressed as a multiple of the acceleration G of m force) is normally operated at 4.5 to 7.0 x 10"G. At this time, the content of unfiberized particles (usually called shot) mixed into the fibers is indicated by the size of the scale, but typically the shot content is 88μ or more.

)含有率は25〜30%程度である。) The content is about 25 to 30%.

粒子の発生原因としては、微小な粒子は繊維化の際、繊
維を引張る役割をするもので、繊維の尻尾を有し、ta
維形成上ある程度の含有はやむを得ないものもある。し
かし200μ以上の大きい粒子は溶融物が第1回転ドラ
ムに流下する流れの乱れにより発生したり、ドラムとの
衝突により発生したり、ドラム円周部に展延した溶融物
の膜状分裂流が波状に飛散したりするもの、あるいはド
ラム表面に固着した層が剥離じて生成するものからなっ
ている。
The cause of the generation of particles is that minute particles play the role of pulling fibers during fiberization, and they have fiber tails and ta
In some cases, inclusion of a certain amount is unavoidable due to fiber formation. However, large particles of 200μ or more are generated due to turbulence in the flow of the melt flowing down to the first rotating drum, due to collision with the drum, or due to a film-like split flow of the melt spread around the drum circumference. It consists of things that scatter in a wave pattern, or things that are generated when a layer stuck to the drum surface peels off.

これらの発生原因と考えられる現象から考えると、回転
ドラムの径を大きくしたり、ドラムの回転数を増加して
も、それは同時に粒子発生をも増大させることになると
も考えられ、必ずしも粒子含有率を低減できるとは従来
光えられなかった。
Considering the phenomena that are thought to be the cause of these occurrences, it is thought that even if the diameter of the rotating drum is increased or the rotational speed of the drum is increased, it will also increase the generation of particles at the same time, and the particle content will not necessarily increase. Until now, it has not been possible to reduce the

〔発明が解決しようとする問題点〕[Problem that the invention seeks to solve]

前記の如く、従来の多段回転ドラム型遠心繊維化装置で
は繊維中のショットが88μ以上の粒子含有率で表わし
て25〜30%と多いという問題点があった。
As mentioned above, the conventional multistage rotating drum type centrifugal fiber forming apparatus has a problem in that the content of shot in the fibers is as high as 25 to 30%, expressed as a particle content of 88 μm or more.

本発明はこの粒子含有率を20%以下に低減させる事を
目的とする。
The purpose of the present invention is to reduce this particle content to 20% or less.

本発明は特に多段回転ドラム型遠心繊維化装置の運転条
件を調整して粒子含有率を低減させる事を目的とする。
In particular, the present invention aims to reduce the particle content by adjusting the operating conditions of a multi-stage rotating drum type centrifugal fiberizing apparatus.

〔問題点を解決するための手段〕[Means for solving problems]

本発明者等は前記のような問題点を解決するため研究を
行い、粒子の発生原因には前記の如く種々の要因があり
、溶融物の第1ドラムへの降下流の乱れ防止とかドラム
に衝突する際の飛散防止とか、あるいは生成した繊維と
粒子の質量の相異から繊維を前方へ吹きとばすエアプレ
ナムの風速等も重要であるが、これらの他の要因を可能
な限り粒子減少の条件に設定したとして、回転ドラムの
運転条件としては回転ドラムの遠心加速度を増大さゼる
と意外にもショットを大巾に低減できる事を見出し、本
発明を完成した。
The present inventors have conducted research to solve the above-mentioned problems, and found that the causes of particle generation are various factors as mentioned above. Although it is important to prevent scattering during collision, and to blow the fibers forward due to the difference in mass between the generated fibers and particles, such as the wind speed of the air plenum, it is important to consider these other factors as conditions for reducing particles as much as possible. The inventors have discovered that, surprisingly, the number of shots can be significantly reduced by increasing the centrifugal acceleration of the rotating drum under the operating conditions of the rotating drum, and has completed the present invention.

すなわち本発明は多段回転ドラム型遠心繊維化装置によ
る態様繊維のwA造において、回転ドラムの遠心加速度
又は周速度を増大させることにより粒子含有率を低減さ
ぼることを特徴とする無り絨紺の製造方法である。
That is, the present invention relates to the production of plain carpet, which is characterized in that the particle content is reduced by increasing the centrifugal acceleration or circumferential speed of the rotating drum in the process of manufacturing fibers using a multi-stage rotating drum type centrifugal fiber forming apparatus. It's a method.

回転ドラムの遠心加速度の平均値をとると便宜であるが
、′/IJ論各ドラムの遠心加速度の合計値をとっても
同じである。第1段の回転ドラムはディス1〜リビユー
ターの役目をしているので、第1段回転ドラムの遠心加
速度を加えて平均してもよいし、合計値をとってもよい
が、より相関関数を上げるためには第2段以降の回転ド
ラムの遠心加速度の合計値又は平均値を増大させること
が好ましい。回転ドラムの遠心加速度は、ドラムの半径
をr、角速度をωとするとrω2で表わされる値で、各
ドラムの平均値としてはrω2をとる事になる単位はm
/5eC2であるが、通常重力の加速度Gの何倍である
かで表示している。
It is convenient to take the average value of the centrifugal acceleration of the rotating drums, but it is also the same if we take the total value of the centrifugal accelerations of each drum. Since the first stage rotating drum plays the role of disk 1~reviewer, the centrifugal acceleration of the first stage rotating drum may be added and averaged, or the total value may be taken, but in order to further increase the correlation function, In this case, it is preferable to increase the total value or average value of the centrifugal acceleration of the rotating drums in the second and subsequent stages. The centrifugal acceleration of a rotating drum is a value expressed as rω2, where the radius of the drum is r and the angular velocity is ω.The unit for taking rω2 as the average value of each drum is m.
/5eC2, but it is usually expressed in terms of how many times the acceleration G of gravity is.

研究の結果、回転ドラム遠心加速度と粒子含有率との関
係は次式で表わされる。
As a result of research, the relationship between rotating drum centrifugal acceleration and particle content is expressed by the following equation.

297μ以上の粒子含有率(%)をWs−3177μ以
上の粒子含有率(%)をWs−288μ以上の粒子含有
率(%)をWs−1と表示すると W    =5.85−0.281 X10−3r(、,2 W    =18.9−1.02X10−3rω2W 
   =34.0−1.35X10’rω2但し[ω2
は第2段以降の平均遠心加速度である即ち、平均遠心加
速度を増大させると粒子含有率を低減させることができ
る。これを理論的に考察すると次の通りである。繊維の
質”Jiberとショットの質mm5hotを比較する
とmfiber<<” 5hotで、これらの運動エネ
ルギーの差へE=−r ω (m   −m    )
となる。回転ド2      5hot   fibo
rラムの遠心加速度が大きくなる程、これらの運動エネ
ルギーの差は増大し、エアプレナムの高速気流による飛
翔の行程差が大きくなり、エアプレナムの高速気流によ
る分離効率が向上するためである。
If the particle content (%) of 297μ or more is expressed as Ws-31 The particle content (%) of 77μ or more is expressed as Ws-1, the particle content (%) of 288μ or more is expressed as Ws-1. W = 5.85-0.281 X10 -3r(,,2 W =18.9-1.02X10-3rω2W
=34.0-1.35X10'rω2 However, [ω2
is the average centrifugal acceleration after the second stage, that is, increasing the average centrifugal acceleration can reduce the particle content. A theoretical consideration of this is as follows. Comparing the fiber quality "Jiber" and the shot quality mm5hot, mfiber<<"5hot, the difference in kinetic energy between them is E = -r ω (m - m)
becomes. rotation de 2 5hot fibo
This is because as the centrifugal acceleration of the r-ram increases, the difference in kinetic energy increases, the difference in flight distance due to the high-speed airflow of the air plenum increases, and the separation efficiency due to the high-speed airflow of the air plenum improves.

88μ以上の粒子含有率Ws−iを20%以下にするに
はrω を10.4xlO” G以上とすればよい。
In order to make the content Ws-i of particles of 88μ or more 20% or less, rω may be set to 10.4xlO''G or more.

遠心加速度はrω2で表わされるから、遠心加速度を増
大させるには具体的には、回転ドラム径を大きくする事
と回転数を大きくする事になる。
Since the centrifugal acceleration is expressed as rω2, specifically, increasing the centrifugal acceleration involves increasing the diameter of the rotating drum and increasing the rotational speed.

2乗で効いているので、回転数を大きくする事が特に効
果的である。従って遠心加速度を増大させる事は同時に
周速度rωを増大させる事でもある。
Since it is effective as a square, increasing the rotation speed is particularly effective. Therefore, increasing the centrifugal acceleration also increases the peripheral speed rω.

〔実施例〕〔Example〕

4段回転ドラム型遠心繊維化装置を用いて、ドラム径を
夫々360#1111φ、400屑φ、460麿φ、5
4ONRφの場合について、遠心加速度を変化させた。
Using a 4-stage rotating drum type centrifugal fiberizing device, the drum diameters were 360 #1111φ, 400 #1111φ, 400 #1111φ, 460mmφ, and 5 mm.
For the case of 4ONRφ, the centrifugal acceleration was varied.

この場合、原料溶融装置から第1回転ドラムへの溶融物
の流下条件や、エア・ブレナムの風速、風m等地の条件
は同一にして試験した。
In this case, the test was carried out under the same conditions as the flow conditions of the melt from the raw material melting device to the first rotating drum, the wind speed of the Air Blenheim, the wind m, etc.

横軸にNO2以降の回転ドラムの平均遠心加速度(遠心
加速度の合計値と対応)をとり、縦軸に生成繊維中の8
8μ以上の粒子含有率と、177μ以上の粒子含有率を
とった試験結果を第1図に示す。
The horizontal axis shows the average centrifugal acceleration (corresponding to the total centrifugal acceleration) of the rotating drum after NO2, and the vertical axis shows the average centrifugal acceleration of the rotating drum after NO2.
The test results for the particle content of 8μ or more and the particle content of 177μ or more are shown in FIG.

遠心加速度を増大させる事により、粒子含有率を直線的
に低減し得る事が明らかである。
It is clear that by increasing the centrifugal acceleration, the particle content can be reduced linearly.

177μ以上の粒子含有率よりも、88μ以上の粒子含
有率の方がより大巾に低減している。これはより大径の
粒子は溶融物の流下条件等信の要因にもよっているのに
対し、遠心加速度は小径の粒子低減により、効果的であ
る事が明らかである。
The particle content of 88 μm or more is reduced more widely than the particle content of 177 μm or more. It is clear that centrifugal acceleration is more effective in reducing small diameter particles, whereas larger diameter particles depend on factors such as melt flow conditions.

(発明の効果) 多段回転ドラム型遠心m維化装置によるR線繊維の製造
において、原料溶融物の第1回転ドラムへの流下条件や
、エア・ブレナムの風速、風量等信の条件を一定にした
場合に、生成するiIi維中の粒子含有率は、回転ドラ
ムの遠心加速度又は周速度を増大させる事により大巾に
低減させる事ができる。無Rm雑の品質向上に実用的効
果は橿めて大きい。
(Effect of the invention) In the production of R-line fibers using a multi-stage rotating drum type centrifugal fiber forming apparatus, the flow conditions of the raw material melt to the first rotating drum, the air speed, air volume, etc. of the air brenum are kept constant. In this case, the particle content in the generated IIIi fibers can be significantly reduced by increasing the centrifugal acceleration or circumferential speed of the rotating drum. The practical effect on improving the quality of non-RM miscellaneous products is extremely large.

【図面の簡単な説明】[Brief explanation of drawings]

第1図はNo2回転ドラム以時の平均遠心加速度(遠心
加速度の合計値と対応)と粒子含有率との関係を示した
図表である。 出願人代理人  藤  本  博  光*kiJrJR
An令*tllL (X? 0t(NO’) )I騨2 第 l 図
FIG. 1 is a chart showing the relationship between the average centrifugal acceleration (corresponding to the total value of centrifugal acceleration) and particle content after No. 2 rotating drum. Applicant's agent Hiroshi Fujimoto *kiJrJR
An order*tllL (X? 0t(NO') )I key 2 Fig.

Claims (1)

【特許請求の範囲】 1、多段回転ドラム型遠心繊維化装置による無機繊維の
製造において回転ドラムの遠心加速度又は周速度を増大
させることにより粒子含有率を低減させることを特徴と
する無機繊維の製造方法。 2、第2段以降の回転ドラムの平均遠心加速度を@rω
^2@とし、無機繊維中の88μ以上の粒子含有率をW
_s_−_1(%)とした時 W_s_−_1=34.0−1.35×10^−^3@
rω^2@の式により、平均遠心加速度を増大させるこ
とにより粒子含有率を低減させる特許請求の範囲第1項
記載の無機繊維の製造方法。 3、第2段以降の回転ドラムの平均遠心加速度を@rω
^2@とし、無機繊維中の177μ以上の粒子含有率を
W_s_−_2(%)とした時 W_s_−_2=18.9−1.02×10^−^3@
rω^2@の式により、平均遠心加速度を増大させるこ
とにより粒子含有率を低減させる特許請求の範囲第1項
記載の無機繊維の製造方法。 4、第2段以降の回転ドラムの平均遠心加速度を@rω
^2@とし、無機繊維中の297μ以上の粒子含有率を
W_s_−_3(%)とした時 W_s_−_3=5.85−0.281 ×10^−^3@rω^2@ の式により、平均遠心加速度を増大させることにより、
粒子含有率を低減させる特許請求の範囲第1項記載の無
機繊維の製造方法。 5、遠心加速度又は周速度の制御値として、第2段以降
の回転ドラムの遠心加速度の合計値又は周速度の合計値
をそれぞれとる特許請求の範囲第1項記載の無機繊維の
製造方法。 6、遠心加速度又は周速度の制御値として、第2段以降
の回転ドラムの平均遠心加速度又は平均周速度をそれぞ
れとる特許請求の範囲第1項記載の無機繊維の製造方法
。 7、第2段以降の回転ドラムの平均遠心加速度を10×
10^3以上とすることにより、無機繊維中の88μ以
上の粒子含有率を20%以下に低減させる特許請求の範
囲第1項記載の無機繊維の製造方法。 8、第2段以降の回転ドラムの平均遠心加速度を15×
10^3G以上とすることにより、無機繊維中の177
μ以上の粒子含有率を10%以下に低減させる特許請求
の範囲第1項記載の無機繊維の製造方法。
[Claims] 1. Production of inorganic fibers using a multi-stage rotating drum type centrifugal fiber forming apparatus, characterized in that the particle content is reduced by increasing the centrifugal acceleration or circumferential speed of the rotating drum. Method. 2. The average centrifugal acceleration of the rotating drum from the second stage onwards is @rω
^2@, and the content of particles of 88μ or more in the inorganic fiber is W
When _s_-_1 (%) W_s_-_1=34.0-1.35×10^-^3@
The method for producing inorganic fibers according to claim 1, wherein the particle content is reduced by increasing the average centrifugal acceleration according to the formula rω^2@. 3. The average centrifugal acceleration of the rotating drums from the second stage onwards is @rω
@2@, and when the content of particles of 177μ or more in the inorganic fiber is W_s_-_2 (%), W_s_-_2=18.9-1.02×10^-^3@
The method for producing inorganic fibers according to claim 1, wherein the particle content is reduced by increasing the average centrifugal acceleration according to the formula rω^2@. 4. The average centrifugal acceleration of the rotating drum from the second stage onwards is @rω
@2@, and when the content of particles of 297μ or more in the inorganic fiber is W_s_-_3 (%), according to the formula W_s_-_3=5.85-0.281 ×10^-^3@rω^2@ , by increasing the average centrifugal acceleration,
The method for producing an inorganic fiber according to claim 1, which reduces the particle content. 5. The method for producing inorganic fibers according to claim 1, wherein the control value for the centrifugal acceleration or circumferential velocity is the total value of the centrifugal acceleration or the total value of the circumferential velocity of the rotary drums from the second stage onwards, respectively. 6. The method for producing inorganic fibers according to claim 1, wherein the control value for centrifugal acceleration or circumferential velocity is the average centrifugal acceleration or average circumferential velocity of the rotating drums from the second stage onwards, respectively. 7. The average centrifugal acceleration of the rotating drums from the second stage onwards is 10x
10^3 or more, the method for producing inorganic fibers according to claim 1, wherein the content of particles of 88μ or more in the inorganic fibers is reduced to 20% or less. 8. The average centrifugal acceleration of the rotating drums from the second stage onwards is 15x
By setting it to 10^3G or more, 177 in inorganic fibers
The method for producing inorganic fibers according to claim 1, wherein the content of particles larger than μ is reduced to 10% or less.
JP7564987A 1987-03-27 1987-03-27 Production of inorganic fiber Pending JPS63239136A (en)

Priority Applications (1)

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JP7564987A JPS63239136A (en) 1987-03-27 1987-03-27 Production of inorganic fiber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7564987A JPS63239136A (en) 1987-03-27 1987-03-27 Production of inorganic fiber

Publications (1)

Publication Number Publication Date
JPS63239136A true JPS63239136A (en) 1988-10-05

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JP7564987A Pending JPS63239136A (en) 1987-03-27 1987-03-27 Production of inorganic fiber

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2692915A4 (en) * 2011-03-31 2014-08-20 Nichias Corp Method for manufacturing bio-soluble inorganic fiber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2692915A4 (en) * 2011-03-31 2014-08-20 Nichias Corp Method for manufacturing bio-soluble inorganic fiber

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