JPS6248525B2 - - Google Patents

Info

Publication number
JPS6248525B2
JPS6248525B2 JP59085658A JP8565884A JPS6248525B2 JP S6248525 B2 JPS6248525 B2 JP S6248525B2 JP 59085658 A JP59085658 A JP 59085658A JP 8565884 A JP8565884 A JP 8565884A JP S6248525 B2 JPS6248525 B2 JP S6248525B2
Authority
JP
Japan
Prior art keywords
gas
liquid
conical tube
pipe
throat
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP59085658A
Other languages
Japanese (ja)
Other versions
JPS60227814A (en
Inventor
Sadaka Sonobe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to JP59085658A priority Critical patent/JPS60227814A/en
Publication of JPS60227814A publication Critical patent/JPS60227814A/en
Publication of JPS6248525B2 publication Critical patent/JPS6248525B2/ja
Granted legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明は環境衛生及び公害防止機器に応用で
き、気体中の有害成分を除去する気液接触装置に
関するものである。 (従来技術) 従来一般に気体中の有害成分を液体を使用して
除去する装置は種の形式のものが提案されている
が、原理的には如何にして気液接触を有効に行な
うかということであり、気液接触の形式により
種々に分類される。 これらは液体を微細な液滴となし、気体と接触
させる形式のジエツトスクラツバー、スプレー
塔、気体を気泡として液体中を通過させる形式と
しての泡鏡式多孔板式等の棚段塔と、液体のエネ
ルギーを利用して気体を分断乃至気液混相を形成
させる気体巻き込み方式と、散気管等を使用する
気泡発生器を設けた気泡塔、充填物の濡れ表面と
気体とを接触させる形式の充填塔などである。 以上のように大別される形式のものが広く一般
的に使用されており、その改良として液滴の微細
化の研究、接触時間を長くする研究、発生気泡の
微細化、気泡発生の簡素化、充填物の形状の研究
等、省エネルギー、効率の向上等に向けて開発が
行なわれ、多くの発明がなされている。 しかしながら根本的には、以上の各種装置には
気体供給用の機器、液体供給用機器を必要とし、
当然ながら各々駆動用エネルギーも必要であつ
た。また装置の形式によつては過大なエネルギー
を必要とするものもあつた。更に液体供給用機器
には配管、バルブ、計装等付帯設備を必要とし、
設備費としては単に供給用機器に止まらなかつ
た。また前記棚段塔、気体巻き込み方式、気泡塔
等には、気体を自給式にしたものも実用化されて
いるが、装置は単一機能的で効率を向上させるた
め、気液を混合する部分に種々な機構を施し、複
雑化していた。 (発明が解決しようとする問題点) 本発明者は多年にわたり各形式の気液接触装置
を製作し、販売して来た経験より、単一機能の装
置ではあきたらず、省エネルギー、コンパクトで
安価な、高能率の気液接触装置を目指して鋭意研
究を進めた結果、本発明に到達したものである。 (問題点を解決するための手段) このため本発明は、管断面に対して切線方向
に、気体を供給する気体供給管を装着し、下部に
液吸込み口を設けた吸液兼気液混合管、その上方
に同心に連設され、上端径が縮小した円錐管、該
円錐管の上端径と同径で該円錐管上に連結された
スロート、該スロート上に連設され上端が拡張し
た倒立円錐管、該倒立円錐管を覆うように配設さ
れた有蓋円筒、該円筒と倒立円錐管との間に介設
された充填層、前記各部材を内包し下部に液溜を
形成したハウジングとよりなる構成としたもので
ある。 (作用) さて以上の構成により、吸液兼気液混合管内
で、液吸込み口より吸込まれた液体と気体との気
液混相の旋回流を形成し、1段階としての気液接
触が行なわれ、また断面積の小さいスロートを通
過する過程において、旋回流は軸方向流れに転換
すると共に、流速の増大により、円心部分の気体
も吸込まれて安全な気液混相状態となり、2段階
としての気液接触部分を形成し、また倒立円錐管
を通過する過程において流速が逐次減少するた
め、気液混相流体は微細液滴と気体とに分離し、
液滴は気体中に分散懸垂状態となつて、気体と共
に倒立円錐管より排出されると共に、流れ方向が
上向きより下向きとなり、充填物表面を均一に濡
らし、充填物表面と気体との接触により、効率の
よい気液接触が行なわれる。 (実施例) 以下本発明の実施例を図面について説明する
と、第1図及び第2図は本発明の実施例を示し、
1は吸液兼気液混合管で、該混合管1の管断面に
対して切線方向に気体を供給する気体供給管2が
連結されている。吸液兼気液混合管1の上端には
円錐管3が連設されており、該円錐管3の上端径
は縮小され、この縮小径と同径のスロート4が該
円錐管3上に連結されている。またスロート4上
には上端が拡張された倒立円錐管5が連結されて
おり、この円錐管5を覆うように有蓋円筒6が設
けられ、該円筒6と倒立円錐管5間には繊維材等
よりなる充填層7が介設されている。そしてこれ
らの各部材は、液溜8とその上に連設された蓋板
を有する外筒9に内包されている。また図中10
は充填材、11は気体送入管、12は気体出口、
13は液入口ノズル、14はドレンノズル、15
は液吸込み口、Aは液体である。 次に以上の如く構成された実施例について作用
を説明すると、気体送入管11より気体供給管2
を経て供給された供給気体の圧力により、吸液兼
気液混合管1内で、液吸込み口15より吸込まれ
た液体と気体との気液混相の旋回流を形成し、1
段階目の気液接触が行なわれる。しかし気体と液
体は比重差が大きいため、旋回によつて生じる遠
心力により、気体は中心部分に集まり易いが、吸
液兼気液混合管1に比べて断面積の小さいスロー
ト4を通過する過程において、旋回流は軸方向流
れに転換すると共に、流速の増大により中心部分
の気体も吸込まれて完全な気液混相状態となる。
この部分で2段階目の気液接触部分を形成する。 次いでスロート4を通過した気液混相流体は、
倒立円錐管5を通過する過程において流速が逐次
減少するため、気液混相流体は微細液滴と気体と
に分離し、液滴は気体中に分散懸垂状態となつ
て、気体と共に倒立円錐管5外に排出される。こ
の倒立円錐管5の部分が液滴と気体との3段階目
の気液接触部分を形成する。 また倒立円錐管5より排出された気体と液滴
は、有蓋円筒6の蓋部に当つて流れ方向が上向き
より下向きとなる。この流れ方向が下向きに変換
した液滴は充填物7の表面を均一に濡らし、充填
物7の表面と気体との接触により4段階目の気液
接触が行なわれる。なお、気体中に蒸発する水分
の補給の目的で、有蓋円筒6及び充填材10の上
部に、洗浄用の供給水の圧力によるスプレー装置
を設けることもできる。また性能、効率に影響す
る気液比は、供給気体の供給圧力を調節すること
により調節することができる。 (発明の効果) 以上詳細に説明した如く本発明は、1段階目よ
り4段階目に及び種々の形式の気液接触が行なわ
れ、しかも各接触形式の特徴を1個の装置内で適
用することにより、総合的に高効率の気液接触が
行なわれ、気体中の有害成分を除去することがで
きる。また気体供給管下端よりスロート上端迄
は、気液混相流体の連続層を形成すると共に、気
液混相の見掛け比重と液体との比重差によつて生
ずる圧力差により、吸液兼気液混合管の液吸込み
口より自動的に吸液されるため、吸液兼気液混合
管への液供給のための機器は不要となる。 従つて供給気体の圧力は、吸液兼気液混合管内
において旋回流を生成するに必要な圧力と、装置
内での圧力損失を補う圧力の和であつて、他装置
の如く気体供給のためのエネルギーは必要でな
く、総合的には省エネルギーを達成できる。また
構造も簡単で安価であり、しかも高効率で、殆ど
補修費を必要としない等の効果を奏するものであ
る。 次に第1図の装置において下記具体例寸法で試
験した結果を第1表に示す。 吸液兼気液混合管1:ID100mmφ 気体供給管2:ID100mmφ スロート4:ID40mmφ 倒立円錐管5:450mmH 有蓋円筒6:300mmφ×600mmH 外筒9:500mmφ×650mmH 液溜8:900mmφ×500mmH 充填層7:ビニロツク、高さ400mm 以上の寸法の装置において、供給気体量2m3
min、供給気体圧力325mm〜335mm(水柱)で試験
した。なお、第1表における出口濃度は光明理化
学社製ガス検知管、入口濃度の※印はガス検知
管、他はボンベ中のガス減量と風量より計算した
値である。第1表よりみて、本発明装置が優秀な
性能を有することが分る。 【表】
DETAILED DESCRIPTION OF THE INVENTION (Field of Industrial Application) The present invention relates to a gas-liquid contact device that can be applied to environmental sanitation and pollution prevention equipment and removes harmful components from gas. (Prior Art) Conventionally, various types of devices have been proposed for removing harmful components from gases using liquids, but in principle, the problem is how to effectively make gas-liquid contact. It is classified into various types depending on the type of gas-liquid contact. These include jet scrubbers and spray towers that form liquid into fine droplets and bring them into contact with gas, and plate towers such as bubble mirror and perforated plate types that allow gas to pass through the liquid as bubbles. The gas entrainment method utilizes the energy of the liquid to split the gas or form a gas-liquid mixed phase, the bubble column is equipped with a bubble generator using a diffuser, and the wet surface of the packed material comes into contact with the gas. Such as packed towers. The above-mentioned types are widely and commonly used, and their improvements include research on making droplets smaller, research on increasing contact time, making bubbles smaller, and simplifying bubble generation. Many inventions have been made through research into the shape of fillers and other developments aimed at saving energy and improving efficiency. Fundamentally, however, the various devices mentioned above require gas supply equipment and liquid supply equipment.
Naturally, each required energy for driving. Additionally, some types of equipment required excessive energy. Furthermore, liquid supply equipment requires ancillary equipment such as piping, valves, and instrumentation.
Equipment costs were not limited to just supply equipment. In addition, among the plate towers, gas entrainment systems, bubble towers, etc., those that are self-contained with gas have been put into practical use, but in order to improve efficiency with a single function, the equipment has a part that mixes gas and liquid. Various mechanisms were applied to it, making it complicated. (Problems to be solved by the invention) Based on the experience of manufacturing and selling various types of gas-liquid contact devices over many years, the present inventor has realized that it is not enough to create a single-function device, and that it is energy-saving, compact, and inexpensive. The present invention was achieved as a result of intensive research aimed at creating a highly efficient gas-liquid contact device. (Means for Solving the Problems) Therefore, the present invention provides a liquid suction and gas-liquid mixing system in which a gas supply pipe for supplying gas is installed in the tangential direction with respect to the cross section of the pipe, and a liquid suction port is provided at the bottom. A conical tube connected concentrically above the conical tube and having a reduced upper end diameter, a throat connected to the conical tube with the same diameter as the upper end diameter of the conical tube, and a conical tube connected above the throat and having an expanded upper end. An inverted conical tube, a covered cylinder arranged to cover the inverted conical tube, a filling layer interposed between the cylinder and the inverted conical tube, and a housing containing each of the above-mentioned members and forming a liquid reservoir in the lower part. The structure consists of the following. (Function) With the above configuration, a gas-liquid mixed-phase swirling flow of the liquid and gas sucked from the liquid suction port is formed in the liquid suction and gas-liquid mixing tube, and gas-liquid contact is performed as one stage. In addition, in the process of passing through the throat with a small cross-sectional area, the swirling flow is converted to an axial flow, and due to the increase in flow velocity, the gas at the center of the circle is also sucked in, creating a safe gas-liquid mixed phase state. As the gas-liquid contact area is formed and the flow rate decreases sequentially during the process of passing through the inverted conical tube, the gas-liquid multiphase fluid separates into fine droplets and gas.
The droplets are dispersed in the gas and suspended, and are discharged from the inverted conical tube together with the gas, and the flow direction changes from upward to downward, uniformly wetting the surface of the packing, and due to contact between the surface of the packing and the gas, Efficient gas-liquid contact is performed. (Example) Examples of the present invention will be described below with reference to the drawings. FIGS. 1 and 2 show examples of the present invention,
Reference numeral 1 denotes a liquid suction and gas-liquid mixing tube, and a gas supply tube 2 is connected to the mixing tube 1 for supplying gas in a tangential direction to the cross section of the tube. A conical tube 3 is connected to the upper end of the liquid suction and gas-liquid mixing tube 1, and the diameter of the upper end of the conical tube 3 is reduced, and a throat 4 having the same diameter as this reduced diameter is connected to the conical tube 3. has been done. Further, an inverted conical tube 5 whose upper end is expanded is connected to the throat 4, and a covered cylinder 6 is provided to cover the conical tube 5, and between the cylinder 6 and the inverted conical tube 5 there is a fiber material etc. A filling layer 7 consisting of the following is interposed. Each of these members is housed in an outer cylinder 9 having a liquid reservoir 8 and a lid plate connected thereto. Also, 10 in the figure
is a filling material, 11 is a gas inlet pipe, 12 is a gas outlet,
13 is a liquid inlet nozzle, 14 is a drain nozzle, 15
is a liquid suction port, and A is a liquid. Next, the operation of the embodiment configured as above will be explained.
Due to the pressure of the supply gas supplied through the liquid suction and gas-liquid mixing pipe 1, a gas-liquid mixed phase swirling flow of the liquid and gas sucked from the liquid suction port 15 is formed.
The first stage of gas-liquid contact is carried out. However, since there is a large difference in specific gravity between gas and liquid, the gas tends to gather in the center due to the centrifugal force generated by swirling. At this time, the swirling flow is converted to an axial flow, and the gas in the center is also sucked in due to the increase in flow velocity, resulting in a complete gas-liquid mixed phase state.
This part forms the second stage gas-liquid contact part. Next, the gas-liquid multiphase fluid that passed through the throat 4 is
As the flow rate decreases sequentially during the process of passing through the inverted conical tube 5, the gas-liquid multiphase fluid is separated into fine droplets and gas, and the droplets are dispersed and suspended in the gas, and pass through the inverted conical tube 5 together with the gas. is discharged outside. This portion of the inverted conical tube 5 forms the third stage gas-liquid contact portion between the droplet and the gas. Further, the gas and liquid droplets discharged from the inverted conical tube 5 hit the lid portion of the covered cylinder 6, and the flow direction becomes downward rather than upward. The droplets whose flow direction has changed downward uniformly wet the surface of the packing 7, and the fourth stage of gas-liquid contact is performed by contacting the surface of the packing 7 with the gas. In addition, for the purpose of replenishing moisture that evaporates into the gas, a spray device using the pressure of supply water for cleaning may be provided above the covered cylinder 6 and the filling material 10. Further, the gas-liquid ratio, which affects performance and efficiency, can be adjusted by adjusting the supply pressure of the supply gas. (Effects of the Invention) As explained in detail above, the present invention allows various types of gas-liquid contact to be performed from the first stage to the fourth stage, and moreover, applies the characteristics of each contact type within one device. As a result, highly efficient gas-liquid contact is performed in total, and harmful components in the gas can be removed. In addition, from the lower end of the gas supply pipe to the upper end of the throat, a continuous layer of gas-liquid multiphase fluid is formed, and due to the pressure difference caused by the difference in the apparent specific gravity of the gas-liquid multiphase and the specific gravity of the liquid, the liquid suction and gas-liquid mixing pipe Since the liquid is automatically sucked from the liquid suction port, there is no need for equipment to supply liquid to the liquid suction and gas-liquid mixing tube. Therefore, the pressure of the supplied gas is the sum of the pressure necessary to generate a swirling flow in the liquid suction/gas-liquid mixing pipe and the pressure to compensate for the pressure loss within the device, and is the sum of the pressure necessary to generate a swirling flow in the liquid suction and gas-liquid mixing pipe, and the pressure to compensate for pressure loss within the device. energy is not required, and overall energy savings can be achieved. In addition, the structure is simple and inexpensive, and it is highly efficient, requiring almost no repair costs. Next, Table 1 shows the results of tests conducted using the apparatus shown in FIG. 1 with the following specific dimensions. Liquid suction and gas-liquid mixing pipe 1: ID100mmφ Gas supply pipe 2: ID100mmφ Throat 4: ID40mmφ Inverted conical tube 5: 450mmH Covered cylinder 6: 300mmφ×600mmH Outer cylinder 9: 500mmφ×650mmH Liquid reservoir 8: 900mmφ×500mmH Filled layer 7 : For vinyl locks, equipment with a height of 400 mm or more, the supply gas amount is 2 m 3 /
min, feed gas pressure between 325 mm and 335 mm (water column). Note that the outlet concentration in Table 1 is a gas detection tube made by Komei Rikagaku Co., Ltd., the inlet concentration marked with * is a gas detection tube, and the other values are calculated from the gas loss in the cylinder and the air volume. From Table 1, it can be seen that the device of the present invention has excellent performance. 【table】

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本発明の実施例を示す気液接触装置の
正面断面図、第2図は第1図のX〜X断面図であ
る。 図の主要部分の説明、1……吸液兼気液混合
管、2……気体供給管、3……円錐管、4……ス
ロート、5……倒立円錐管、6……有蓋円筒、7
……充填層、8……液溜、9……外筒(ハウジン
グ)、A……液体。
FIG. 1 is a front cross-sectional view of a gas-liquid contact device showing an embodiment of the present invention, and FIG. 2 is a cross-sectional view taken along the line X to X in FIG. Explanation of the main parts of the diagram, 1...liquid suction and gas-liquid mixing tube, 2...gas supply pipe, 3...conical tube, 4...throat, 5...inverted conical tube, 6...covered cylinder, 7
...Filled layer, 8...Liquid reservoir, 9...Outer cylinder (housing), A...Liquid.

Claims (1)

【特許請求の範囲】[Claims] 1 管断面に対して切線方向に、気体を供給する
気体供給管を装着し、下部に液吸込み口を設けた
吸液兼気液混合管、その上端に同心に連設され、
上端径が縮小した円錐管、該円錐管の上端径と同
径で該円錐管上に連結されたスロート、該スロー
ト上に連設され上端が拡張した倒立円錐管、該倒
立円錐管を覆うように配設された有蓋円筒、該円
筒と倒立円錐管との間に介設された充填層、前記
各部材を内包し下部に液溜を形成したハウジング
とよりなることを特徴とする気液接触装置。
1 A gas supply pipe for supplying gas is installed in the tangential direction with respect to the cross section of the pipe, and a liquid suction and gas-liquid mixing pipe is provided with a liquid suction port at the bottom, and the pipe is connected concentrically to the upper end thereof,
A conical tube with a reduced upper end diameter, a throat having the same diameter as the upper end diameter of the conical tube and connected to the conical tube, an inverted conical tube connected to the throat and having an enlarged upper end, and a conical tube that covers the inverted conical tube. A gas-liquid contact characterized by comprising a covered cylinder disposed in the cylinder, a packed layer interposed between the cylinder and the inverted conical tube, and a housing enclosing each of the above-mentioned members and forming a liquid reservoir in the lower part. Device.
JP59085658A 1984-04-27 1984-04-27 Gas-liquid contacting device Granted JPS60227814A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP59085658A JPS60227814A (en) 1984-04-27 1984-04-27 Gas-liquid contacting device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP59085658A JPS60227814A (en) 1984-04-27 1984-04-27 Gas-liquid contacting device

Publications (2)

Publication Number Publication Date
JPS60227814A JPS60227814A (en) 1985-11-13
JPS6248525B2 true JPS6248525B2 (en) 1987-10-14

Family

ID=13864921

Family Applications (1)

Application Number Title Priority Date Filing Date
JP59085658A Granted JPS60227814A (en) 1984-04-27 1984-04-27 Gas-liquid contacting device

Country Status (1)

Country Link
JP (1) JPS60227814A (en)

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US20110217218A1 (en) * 2010-03-02 2011-09-08 Exxonmobil Research And Engineering Company Systems and Methods for Acid Gas Removal

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106237824A (en) * 2016-08-23 2016-12-21 陈淼 A kind of minimum discharge desulfurization and dedusting eddy flow pallet spray tower
CN106237824B (en) * 2016-08-23 2019-02-19 陈淼 A kind of desulfurization and dust-removal method using minimum discharge desulfurization and dedusting eddy flow pallet spray tower

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