JPS62218472A - Antifreeze for flash quick freezing - Google Patents
Antifreeze for flash quick freezingInfo
- Publication number
- JPS62218472A JPS62218472A JP61060428A JP6042886A JPS62218472A JP S62218472 A JPS62218472 A JP S62218472A JP 61060428 A JP61060428 A JP 61060428A JP 6042886 A JP6042886 A JP 6042886A JP S62218472 A JPS62218472 A JP S62218472A
- Authority
- JP
- Japan
- Prior art keywords
- antifreeze
- ethyl alcohol
- acid ester
- weight
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 230000002528 anti-freeze Effects 0.000 title claims abstract description 22
- 238000007710 freezing Methods 0.000 title claims abstract description 15
- 230000008014 freezing Effects 0.000 title claims description 14
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 16
- -1 glycerol fatty acid ester Chemical class 0.000 claims abstract description 15
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 11
- 235000019441 ethanol Nutrition 0.000 claims abstract description 11
- 229930195729 fatty acid Natural products 0.000 claims abstract description 11
- 239000000194 fatty acid Substances 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229920002050 silicone resin Polymers 0.000 claims abstract description 7
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 12
- 235000011187 glycerol Nutrition 0.000 claims description 8
- 239000004471 Glycine Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 description 13
- 239000000203 mixture Substances 0.000 description 10
- 235000013305 food Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 229960002449 glycine Drugs 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000003507 refrigerant Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 235000021067 refined food Nutrition 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000012267 brine Substances 0.000 description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 description 2
- WPUMTJGUQUYPIV-JIZZDEOASA-L disodium (S)-malate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](O)CC([O-])=O WPUMTJGUQUYPIV-JIZZDEOASA-L 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
- 235000003599 food sweetener Nutrition 0.000 description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 235000019265 sodium DL-malate Nutrition 0.000 description 2
- 239000001394 sodium malate Substances 0.000 description 2
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 239000003765 sweetening agent Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 239000005635 Caprylic acid (CAS 124-07-2) Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 235000013611 frozen food Nutrition 0.000 description 1
- 235000013905 glycine and its sodium salt Nutrition 0.000 description 1
- YEAZPMHWNDZTLC-UHFFFAOYSA-N hexanoic acid;propane-1,2,3-triol Chemical compound OCC(O)CO.CCCCCC(O)=O YEAZPMHWNDZTLC-UHFFFAOYSA-N 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229940049920 malate Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
Description
【発明の詳細な説明】
（産業上の利用分野）
本発明は瞬間急速冷凍用不凍液に関し、特に農水産物や
加工食品類の瞬間急速冷凍用の冷媒に通した不凍液に関
する。DETAILED DESCRIPTION OF THE INVENTION (Industrial Application Field) The present invention relates to an antifreeze solution for flash-quick freezing, and particularly to an antifreeze solution passed through a refrigerant for flash-quick freezing agricultural and marine products and processed foods.
（従来の技術）
近年、農水産物や加工食品類を冷凍品として処理し、流
通販売する場合が多（なってきている。(Prior Art) In recent years, agricultural and marine products and processed foods are often processed into frozen products and distributed and sold.
このような冷凍食品は、該当食品等を適当に前処理した
後、食品の品質を損わないように急速冷凍したもので、
一般には冷凍室内で一１８℃以下の温度で保持され、利
用されている。従来のこの種の急速冷凍法としては、被
冷凍物を適当な冷媒中に浸漬したり、冷媒を吹きつけた
りして冷凍する方法が知られている。このような冷媒（
本願では不凍液と称する）としては、従来から液体窒素
、ブライン、糖液、エチルアルコール−食塩水−プロピ
レングリコール混合液等が知られている。These frozen foods are made by appropriately pre-treating the food, etc., and then quickly freezing it to avoid damaging the quality of the food.
Generally, it is kept and used at a temperature of -18°C or lower in a freezing room. As a conventional quick freezing method of this type, methods are known in which the object to be frozen is immersed in a suitable refrigerant or the object is blown with the refrigerant. Refrigerants like this (
Liquid nitrogen, brine, sugar solution, ethyl alcohol-salt water-propylene glycol mixture, and the like are conventionally known as antifreeze solutions (referred to as antifreeze solutions in this application).
しかしながら、上記従来の不凍液のうち、液体窒素は高
価で、凍結のための設備が大掛りとなり、経費も高くつ
くという欠点があり、またブライン、糖液は食品に浸透
するので、使用範囲が限定され、またエチルアルコール
−食塩水−プロピレングリコール混合液は不安定で沈澱
を生じ易く、到達最低温度も一３０℃と高く、瞬間急速
冷凍液としては充分満足のいくものではなかった。また
従来の不凍液は冷凍時間が長くかかり、また冷凍品の品
質を損なうという欠点がある。However, among the conventional antifreeze solutions mentioned above, liquid nitrogen is expensive, requires large-scale freezing equipment, and costs are high.Also, brine and sugar solution permeate into foods, so their range of use is limited. Furthermore, the ethyl alcohol-saline-propylene glycol mixture was unstable and prone to precipitation, and the lowest temperature it reached was as high as -30°C, making it unsatisfactory as a flash freezing liquid. Conventional antifreeze solutions also have the drawback of requiring a long freezing time and impairing the quality of frozen products.
（発明が解決しようとする問題点）
本発明の目的は、瞬間急速冷凍に適する−６０℃以下の
到達最低温度を有し、かつ被冷凍物の種類によらず、適
用範囲が広く、かつ冷凍物の品質を損なわない不凍液を
提供することにある。(Problems to be Solved by the Invention) It is an object of the present invention to have a minimum temperature of -60°C or less suitable for flash quick freezing, and to have a wide range of application regardless of the type of frozen object. Our goal is to provide antifreeze that does not impair product quality.
（問題点を解決するための手段）
本発明は、エチルアルコール３０〜６０重量部、純水３
０〜５０重量部、シリコン樹脂０．１〜５重量部、プロ
ピレングリコール０．５〜１０重！）！、グリセリン脂
肪酸エステル０．１〜５重量部、およびグリシン０．１
〜５重量部を含有することを特徴とする。(Means for solving the problem) The present invention consists of 30 to 60 parts by weight of ethyl alcohol, 3 parts by weight of pure water,
0 to 50 parts by weight, silicone resin 0.1 to 5 parts by weight, propylene glycol 0.5 to 10 parts by weight! )! , 0.1 to 5 parts by weight of glycerin fatty acid ester, and 0.1 part of glycine
~5 parts by weight.
本発明の不凍液の主成分は、エチルアルコールと純水（
典型的には蒸溜水）であり、これらの含有量が上記範囲
外では、例えば水の含有量が多くなりすぎると到達最低
温度が高くなり、またエチルアルコールの量が多すぎる
と不凍液のロスが多くなり、コスト高となる。The main components of the antifreeze of the present invention are ethyl alcohol and pure water (
If the content is outside the above range, for example, if the content of water is too high, the minimum temperature reached will be high, and if the amount of ethyl alcohol is too large, loss of antifreeze will occur. This increases the cost.
本発明に用いるシリコン樹脂は、シロキサン結合を有す
る高分子化合物で、液中に均一に分散または溶解し得る
ものであればよく、ポリアルキルシロキサン（Ｃ＝１〜
２０）、例えばポリジメチルシロキサン（いわゆるシリ
コンオイル）をいう。The silicone resin used in the present invention may be a polymeric compound having a siloxane bond, as long as it can be uniformly dispersed or dissolved in a liquid, and polyalkylsiloxane (C=1 to
20), for example, polydimethylsiloxane (so-called silicone oil).
これらのシリコン樹脂は、必要に応じてソルビタン脂肪
酸エステル、グリセリン脂肪酸エステル、蔗糖脂肪酸エ
ステル等の界面活性剤とともに水中に分散させて用いら
れる。These silicone resins are used by being dispersed in water together with a surfactant such as a sorbitan fatty acid ester, a glycerin fatty acid ester, or a sucrose fatty acid ester, if necessary.
グリセリン脂肪酸エステルとしては、グリセリンとカプ
リル酸、カプロン酸、オレイン酸などの飽和または不飽
和脂肪酸とのエステル、例えばグリセリンモノカプリル
酸エステル、グリセリンモノカプロン酸エステル、ポリ
グリセリンモノオレイン酸エステル等が用いられる。As the glycerin fatty acid ester, esters of glycerin and saturated or unsaturated fatty acids such as caprylic acid, caproic acid, and oleic acid are used, such as glycerin monocaprylic acid ester, glycerin monocaproic acid ester, polyglycerin monooleic acid ester, etc. .
本発明に用いるプロピレングリコールは保存剤、グリセ
リン脂肪酸エステルは界面活性剤、グリシン（またはア
ミノ酢酸）は変色防止剤として添加される。いずれの添
加剤も上記範囲外の含量ではその効果が低下するか、ま
たは添加量が不必要に多くなる。なお、本発明の不凍液
には、上記必須成分以外に例えばアルコールの臭気を柔
げるための甘味料としてｄ、Ｊ−リンゴ酸ナトリウム等
を添加することができる。Propylene glycol used in the present invention is added as a preservative, glycerin fatty acid ester is added as a surfactant, and glycine (or aminoacetic acid) is added as a discoloration preventive agent. If the content of any of the additives is outside the above range, the effect will be reduced or the amount added will be unnecessarily large. In addition to the above-mentioned essential components, the antifreeze solution of the present invention may contain, for example, sodium d,J-malate as a sweetener to soften the odor of alcohol.
上記構成成分はいずれも国内の食品衛生法で許可された
もので、人体に悪影響を及ぼすものではない。All of the above components are permitted under Japan's Food Sanitation Law and do not have any adverse effects on the human body.
本発明の不凍液の製造方法は、上記各成分が均一に混合
され、安定な溶液を形成すれば如何なる方法でもよいが
、
（１）常温または加温下に蒸溜水とグリセリン脂肪酸エ
ステルを急速に攪拌混合する、
（２）常温または加温下にグリシン、プロピレングリコ
ールおよび甘味料を混合し、次いでこれにエチルアルコ
ールを添加して急速に攪拌混合する、（３）以上の（１
）と（２）の液を攪拌混合する、以上の工程により安定
で均一な本発明の不凍液を得ることができる。The method for producing the antifreeze of the present invention may be any method as long as the above components are mixed uniformly and a stable solution is formed. (1) Distilled water and glycerin fatty acid ester are rapidly stirred at room temperature or under heating. (2) Mix glycine, propylene glycol and a sweetener at room temperature or under heating, then add ethyl alcohol to this and rapidly stir and mix; (3) above (1);
The stable and uniform antifreeze solution of the present invention can be obtained through the above steps of stirring and mixing the liquids of ) and (2).
（実施例） 第１表に示す組成の不凍液を下記の手順で製造した。(Example) An antifreeze solution having the composition shown in Table 1 was manufactured according to the following procedure.
（１）ｓ溜水を２０℃の温度にコントロールし、これに
グリセリン脂肪酸エステルを急速に混合する、
（２）リンゴ酸ナトリウムとシリコン樹脂を１３℃〜１
５℃に加熱しながら混合する、
（３）常温でグリシン、プロピレングリコールおよびｄ
、Ｊ−リンゴ酸ナトリウムを混合する。(1) Control the temperature of the accumulated water at 20℃ and rapidly mix the glycerin fatty acid ester therein. (2) Add sodium malate and silicone resin to 13℃~1.
Mix while heating to 5℃. (3) Glycine, propylene glycol and d at room temperature.
, J-mix sodium malate.
（３）（２）の混合液にエチルアルコールを攪拌しなが
ら急速に混合する。(3) Rapidly mix ethyl alcohol into the mixture of (2) while stirring.
第１表
＊１ 東芝シリコーン ＴＳＡ７３７ （東芝シリコー
ン（株）の商品名、主成分はポリジメチルシロキサン）
＊２ 主成分はグリセリンモノカプリル酸エステルおよ
びグリセリンモノカプロン酸エステル
（発明の効果）
以上のようにして得られた不凍液は極めて安定であり、
−６０℃に冷却しても充分な流動性を有し、浸漬法によ
る急速瞬間冷凍の冷媒として充分使用できることが確認
された。本発明の不凍液は、冷凍時間が短く、数分間で
食品類を冷凍することができ、また解凍時間も短く、食
品の細胞を破壊することなく、味覚、栄養をほとんどそ
のまま保持することができる。このため、農水産物や加
工食品類の冷凍に最適である。Table 1 *1 Toshiba Silicone TSA737 (trade name of Toshiba Silicone Co., Ltd., the main component is polydimethylsiloxane) *2 The main components are glycerin monocaprylate and glycerin monocaproate (effects of the invention) The antifreeze obtained is extremely stable,
It was confirmed that it had sufficient fluidity even when cooled to -60°C and could be used satisfactorily as a refrigerant for rapid flash freezing using the immersion method. The antifreeze solution of the present invention has a short freezing time, can freeze foods in a few minutes, has a short thawing time, and can retain most of the taste and nutrition intact without destroying the cells of the food. Therefore, it is ideal for freezing agricultural and marine products and processed foods.
Claims (1)
５０重量部、シリコン樹脂０．１〜５重量部、プロピレ
ングリコール０．５〜１０重量部、グリセリン脂肪酸エ
ステル０．１〜５重量部、およびグリシン０．１〜５重
量部を含有することを特徴とする瞬間急速冷凍用不凍液
。(1) 30 to 60 parts by weight of ethyl alcohol, 30 to 60 parts by weight of pure water
50 parts by weight, 0.1 to 5 parts by weight of silicone resin, 0.5 to 10 parts by weight of propylene glycol, 0.1 to 5 parts by weight of glycerin fatty acid ester, and 0.1 to 5 parts by weight of glycine. Antifreeze for instant quick freezing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61060428A JPS62218472A (en) | 1986-03-18 | 1986-03-18 | Antifreeze for flash quick freezing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61060428A JPS62218472A (en) | 1986-03-18 | 1986-03-18 | Antifreeze for flash quick freezing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS62218472A true JPS62218472A (en) | 1987-09-25 |
Family
ID=13141949
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61060428A Pending JPS62218472A (en) | 1986-03-18 | 1986-03-18 | Antifreeze for flash quick freezing |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62218472A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7247254B1 (en) * | 2005-06-08 | 2007-07-24 | Camco Manufacturing, Inc. | Antifreeze composition and method |
| CN103087686A (en) * | 2013-02-04 | 2013-05-08 | 姜德富 | Automotive cooling fluid |
| CN103773323A (en) * | 2014-01-06 | 2014-05-07 | 沈阳化工大学 | Antifreezing fluid for automobile engine |
-
1986
- 1986-03-18 JP JP61060428A patent/JPS62218472A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7247254B1 (en) * | 2005-06-08 | 2007-07-24 | Camco Manufacturing, Inc. | Antifreeze composition and method |
| CN103087686A (en) * | 2013-02-04 | 2013-05-08 | 姜德富 | Automotive cooling fluid |
| CN103773323A (en) * | 2014-01-06 | 2014-05-07 | 沈阳化工大学 | Antifreezing fluid for automobile engine |
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