JPS62204833A - Method for blending multi-component liquid - Google Patents
Method for blending multi-component liquidInfo
- Publication number
- JPS62204833A JPS62204833A JP61047067A JP4706786A JPS62204833A JP S62204833 A JPS62204833 A JP S62204833A JP 61047067 A JP61047067 A JP 61047067A JP 4706786 A JP4706786 A JP 4706786A JP S62204833 A JPS62204833 A JP S62204833A
- Authority
- JP
- Japan
- Prior art keywords
- liquids
- mixing tank
- liquid supply
- supply ports
- component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 89
- 238000002156 mixing Methods 0.000 title claims abstract description 58
- 238000000034 method Methods 0.000 title claims description 22
- 238000003756 stirring Methods 0.000 claims abstract description 27
- 239000000203 mixture Substances 0.000 abstract description 17
- 238000013329 compounding Methods 0.000 abstract description 7
- 239000006185 dispersion Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Natural products OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000271 synthetic detergent Substances 0.000 description 2
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 1
- PXRKCOCTEMYUEG-UHFFFAOYSA-N 5-aminoisoindole-1,3-dione Chemical compound NC1=CC=C2C(=O)NC(=O)C2=C1 PXRKCOCTEMYUEG-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- MIVSDYNOAUEJHI-UHFFFAOYSA-N acetyl(trimethyl)azanium Chemical compound CC(=O)[N+](C)(C)C MIVSDYNOAUEJHI-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- 229960000541 cetyl alcohol Drugs 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- REZZEXDLIUJMMS-UHFFFAOYSA-M dimethyldioctadecylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC REZZEXDLIUJMMS-UHFFFAOYSA-M 0.000 description 1
- VTTZNHFOGZURNY-UHFFFAOYSA-L disodium;2-oct-1-enylbutanedioate Chemical compound [Na+].[Na+].CCCCCCC=CC(C([O-])=O)CC([O-])=O VTTZNHFOGZURNY-UHFFFAOYSA-L 0.000 description 1
- 239000004664 distearyldimethylammonium chloride (DHTDMAC) Substances 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 1
- 229960002216 methylparaben Drugs 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
- B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
- B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
- B29B7/40—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft
- B29B7/404—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft with feeding or valve actuating means, e.g. with cleaning means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Accessories For Mixers (AREA)
Abstract
Description
【発明の詳細な説明】
〔産業上の利用分野〕
本発明は、各種洗浄剤、仕上剤、化粧品、食品、化学薬
品等、成分の異なる複数種の液体を配合した多成分液体
からなる製品を製造するに際し、成分の異なる複数種の
液体を配合する方法に関するものである。[Detailed Description of the Invention] [Industrial Application Field] The present invention provides products made of multi-component liquids containing multiple types of liquids with different components, such as various cleaning agents, finishing agents, cosmetics, foods, and chemicals. It relates to a method of blending multiple types of liquids with different components during production.
成分の異なる複数種の液体を配合して多成分液体からな
る製品を製造するに際しては、成分の異なる複数種の液
体を配合槽の上部より順次投入し、撹拌して製品化する
回分式配合法や、配合物の循環系に成分の異なる複数種
の液体を供給し、ライン中又は配合槽で撹拌し製品化す
るか、或いはインラインミキサー（又はスタティックミ
キサー）の前にヘッダーを組んでここに成分の異なる複
数種の液体を供給してライン中で製品化する連続式（連
続系）配合法が採用されている。When manufacturing a product consisting of multi-component liquids by blending multiple types of liquids with different ingredients, a batch blending method is used in which multiple types of liquids with different ingredients are sequentially introduced from the top of the mixing tank and stirred to produce the product. Alternatively, you can supply multiple types of liquids with different components to the circulation system of the compound and mix them in the line or blending tank to produce the product, or you can install a header in front of the in-line mixer (or static mixer) and mix the ingredients here. A continuous compounding method is used in which multiple types of liquids with different values are supplied and manufactured into products in a line.
また、例えば合成洗剤の配合においては、特公昭５９−
１７１５９号公報に記載されているように、混合槽に外
部循環装置を設けると共に、滞留液量を比較的多くして
時間とともに組成が変動することを防止するのが一般的
である。In addition, for example, in the formulation of synthetic detergents,
As described in Japanese Patent No. 17159, it is common to provide an external circulation device in the mixing tank and to increase the amount of retained liquid to prevent the composition from changing over time.
しかしながら、上述の回分式配合法においては、大容量
の配合設備及び製品貯槽が必要である。However, the above-mentioned batch compounding method requires large-capacity compounding equipment and product storage tanks.
また、上述の連続式配合法においては、配合開始時に配
合系を水又は製品で充液する必要性、ヘソグ一部での滞
留時間の差によるタイミングのずれ等により、配合開始
（運転初期）時には規定の配合組成を得ることができず
、そのため、規格を満足する製品となるまでの端切りが
必要となり、製品ロスを伴うか、又はこの組成変動を緩
衝できる大容量の緩（ｈ系が必要である。In addition, in the above-mentioned continuous blending method, it is necessary to fill the blending system with water or product at the start of blending, and due to timing differences due to differences in residence time in some parts of the hesog, etc. It is not possible to obtain a specified composition, and therefore it is necessary to cut off the product until it meets the specifications, resulting in product loss. It is.
何れにしても、従来の方法においては、系内の組成（組
織）が均一化するのに時間がかかる（例えば、液体洗浄
剤の場合、３０分以上）ため、運転の初期から規定の配
合組成の製品を取出すことは極めて困難である等の問題
があった。In any case, in conventional methods, it takes time to homogenize the composition (structure) in the system (for example, 30 minutes or more in the case of liquid cleaning agents), so the prescribed composition is determined from the beginning of operation. There were problems such as it was extremely difficult to take out the product.
従って、本発明の目的は、運転初期から規定の配合組成
を得ることのできる新規な多成分液体の配合方法を提供
することにある。Accordingly, an object of the present invention is to provide a novel method for blending multi-component liquids that allows a prescribed blending composition to be obtained from the initial stage of operation.
本発明は、槽内の少なくとも下部に撹拌翼を有する混合
槽の下部側面又は底面に５個以上の液体供給口を設け、
それぞれ成分の異なる複数種の液体の供給を上記各供給
口から同時に開始し、供給′された複数種の液体を上記
撹拌翼で撹拌混合することにより、複数種の液体からな
る多成分液体が上記混合槽内に充満する以前に、該多成
分液体を均一化するようにしたことを特徴とする多成分
液体の配合方法を提供することよって上記の目的を達成
したもので、運転初期から規定の配合組成を得るように
したものである。勿論、本発明の方法は、運転を途中で
停止し、再スタートする場合にも有効で、再スタート後
直ちに均一な組成物を得ることができるものである。The present invention provides five or more liquid supply ports on the bottom side or bottom of a mixing tank having stirring blades at least at the bottom of the tank,
By simultaneously starting the supply of multiple types of liquids with different components from each of the above-mentioned supply ports, and stirring and mixing the supplied multiple types of liquids with the above-mentioned stirring blade, the multi-component liquid consisting of multiple types of liquids is The above object has been achieved by providing a method for blending multi-component liquids, which is characterized in that the multi-component liquids are homogenized before filling the mixing tank. It is designed to obtain a blended composition. Of course, the method of the present invention is also effective when the operation is stopped midway and restarted, and a uniform composition can be obtained immediately after restarting.
以下、本発明の多成分液体の配合方法を図面を参照しな
がら説明する。Hereinafter, a method for blending a multi-component liquid according to the present invention will be explained with reference to the drawings.
第１図〜第３図は本発明の多成分液体の配合方法に用い
る装置の一例の概略を示すもので、これらの図面におい
て、１は混合槽であり、混合槽１内には撹拌翼２，２．
・・を設け、混合槽１の下部側面には５個以上、通常５
〜２０個の液体供給口３．３．・・・を設け、混合槽１
の上部側面又は上部には多成分液体の取出し管４を設け
、混合槽ｌの底部にはドレン口５を設けである。液体供
給口３，３．・・・は、図示例の場合、鉛直位置を同じ
にして混合槽１の下部側面に放射状且つ等間隔で設けで
あるが、本発明の方法においては、混合槽１の下部側面
又は底面に設けてあれば良い。1 to 3 schematically show an example of an apparatus used in the method of blending multicomponent liquids of the present invention. In these drawings, 1 is a mixing tank, and inside the mixing tank 1 there are stirring blades 2. ,2.
..., and at least 5, usually 5, are installed on the bottom side of mixing tank 1.
~20 liquid supply ports 3.3. ... is installed, mixing tank 1
A multi-component liquid take-out pipe 4 is provided on the side or top of the mixing tank 1, and a drain port 5 is provided at the bottom of the mixing tank 1. Liquid supply port 3, 3. In the illustrated example, they are provided radially and at equal intervals on the lower side surface of the mixing tank 1 with the same vertical position, but in the method of the present invention, It is good if there is.
又、撹拌翼２．２．・・は、モーター６によって回転駆
動される回転軸７に上下方向に適宜間隔をあけて４箇所
に固定してあり、その内の下部の２箇所の撹拌１ｉｉ２
，２の間に、液体供給口３，３、・・・を臨ませである
が、本発明の方法を実施するための装置においては、液
体供給口から供給された複数種の液体が撹拌翼により直
ちに撹拌混合されるように、撹拌翼は、少なくとも槽内
の下部、即ち、液体供給口の位置に近接した位置に設け
てあれば良く、その固定箇所、数等は実施例に制限され
るものではない。又、８，８．・・・は、それぞれの液
体供給口３．３．・・に、それぞれ成分の異なる複数種
の液体を供給する原料供給管、９．９．・・・は、液体
供給口３，３．・・からの成分の異なる複数種の液体の
供給の開始及び停止を電磁弁又は流体による作動弁で同
時に行うようにしたアクチェーターである。Also, stirring blade 2.2. ... are fixed at four locations at appropriate intervals in the vertical direction on a rotating shaft 7 that is rotatably driven by a motor 6, of which the stirring shafts 1ii2 are located at the lower two locations.
, 2, the liquid supply ports 3, 3, ... are faced between the liquid supply ports 3, 3, . In order to immediately stir and mix the liquid, the stirring blades need only be provided at least at the bottom of the tank, that is, in a position close to the liquid supply port, and their fixing location, number, etc. are limited to the examples. It's not a thing. Also, 8,8. ... are the respective liquid supply ports 3.3. A raw material supply pipe for supplying multiple types of liquids each having different components to 9.9. ... are liquid supply ports 3, 3. This is an actuator that simultaneously starts and stops the supply of multiple types of liquids with different components from... using an electromagnetic valve or a fluid-operated valve.
而して、上述の装置を用いて本発明の多成分液体の配合
方法を実施するには、それぞれ成分の異なる複数種の液
体の混合槽ｌへの供給を、上記各供給口３，３．・・・
から同時に開始し、供給された複数種の液体を下部撹拌
翼２．２で撹拌混合すれば良く、その結果、複数種の液
体からなる多成分液体が、混合槽ｌ内に充満する以前に
均一化される。各供給口３，３．・・・からのそれぞれ
液体の供給量は、目的とする多成分液体の配合割合とす
ることは云う迄もない、尚、この際、少量成分及び固形
成分については、適宜な濃度の水溶液又は分散液として
供給する。又、目的に応じ、１つの液体供給口からは、
水のみを供給する場合もある。又、それぞれの供給口３
，３．・・・からは、それぞれ成分の異なる液体が供給
されるが、同一成分の液体であっても、全く同一ではな
いもの、例えば濃度が異なるものについては、異なる供
給口から供給することができる。In order to implement the multi-component liquid blending method of the present invention using the above-mentioned apparatus, a plurality of liquids having different components are supplied to the mixing tank l through the respective supply ports 3, 3, . ...
The supplied liquids can be stirred and mixed by the lower stirring blade 2.2 at the same time, and as a result, the multi-component liquid consisting of the plurality of liquids becomes homogeneous before it fills the mixing tank l. be converted into Each supply port 3, 3. Needless to say, the amount of each liquid supplied from Supplied as a liquid. Also, depending on the purpose, one liquid supply port can
In some cases, only water is supplied. Also, each supply port 3
,3. ... are supplied with different components, but even if the components are the same, liquids that are not exactly the same, for example, with different concentrations, can be supplied from different supply ports.
本発明の多成分液体の配合方法を、その好ましい一実施
態様について説明すると、目的とする多成分液体の処理
能力、種類、供給口の位置、サイズの差異等によっても
異なるが、混合槽としてはその容量が平均滞留時間１０
秒〜２０分、好ましくは２０秒〜５分のものを使用する
のが適当である。又、液体供給口は、混合槽の底部から
３０ｃｍ以内の高さに配置するのが好ましいが、特に混
合槽の下部側面に設ける場合には、高さを略同−にし略
等間隔で放射状に設けるのが更に好ましい。A preferred embodiment of the method for blending multi-component liquids of the present invention will be described. Although it varies depending on the processing capacity, type, position of the supply port, size, etc. of the target multi-component liquid, Its capacity has an average residence time of 10
It is appropriate to use a heating time of seconds to 20 minutes, preferably 20 seconds to 5 minutes. In addition, it is preferable that the liquid supply ports be placed at a height within 30 cm from the bottom of the mixing tank, but especially when they are provided on the bottom side of the mixing tank, they should be arranged at approximately the same height and radially spaced at approximately equal intervals. It is even more preferable to provide one.
又、液体供給口の直径、液体供給口からの液体供給圧力
等は、目的とする多成分液体の配合割合に応じて適宜選
択することができる。又、槽内に下部に設ける撹拌翼は
、液体供給口を下部側面に設けた場合には、液体供給口
に対して第２図に示す如き位置に配置するのが好ましく
、その場合、下方から１及び２番目の位置の撹拌翼の形
状は、ピッチドタービン又はディスパージョンタイプ又
はこれらの組合せとし、それ以外の撹拌翼の形状は、ビ
ソチドタービン又はプロペラ又はこれらの組合せとする
のが好ましい。又、その回転速度は、下部撹拌翼の先端
速度が２〜１５ｍ／ｓｅｃ、とするのが好ましい。Further, the diameter of the liquid supply port, the liquid supply pressure from the liquid supply port, etc. can be appropriately selected depending on the desired blending ratio of the multi-component liquid. In addition, when the liquid supply port is provided at the lower side of the tank, it is preferable that the stirring blades installed at the bottom of the tank be placed at the position shown in Fig. 2 with respect to the liquid supply port. The shapes of the stirring blades at the first and second positions are preferably pitched turbines, dispersion types, or a combination thereof, and the shapes of the other stirring blades are preferably bisotide turbines, propellers, or combinations thereof. Further, the rotation speed is preferably such that the tip speed of the lower stirring blade is 2 to 15 m/sec.
次に、実施例を挙げ、本発明の多成分液体の配合方法を
具体的に説明する。Next, examples will be given to specifically explain the method of blending the multi-component liquid of the present invention.
実施例１
第１〜第３図に示す如き構造の下記混合槽（但し、撹拌
翼の数は３枚とした）を用い、７つの液体供給口からそ
れぞれ成分の異なる液体を供給し、下記配合の多成分液
体からなる台所用液体合成洗剤を１００Ｋｇ／Ｈｒの割
合で連続的に製造した。Example 1 Using the following mixing tank with the structure shown in Figures 1 to 3 (however, the number of stirring blades was 3), liquids with different components were supplied from seven liquid supply ports, and the following composition was prepared. A kitchen liquid synthetic detergent consisting of a multi-component liquid was continuously produced at a rate of 100 Kg/Hr.
尚、少量成分及び固形成分については、適宜な濃度の水
溶液又は分散液として供給した。その結果を第４図に示
す。Incidentally, small amounts of components and solid components were supplied as aqueous solutions or dispersions of appropriate concentrations. The results are shown in FIG.
第４図の結果から、本発明の多成分液体の配合方法によ
れば、運転開始後僅か１分以内で規格通りのｐＨ及び粘
度ををする製品が得られることが判る。From the results shown in FIG. 4, it can be seen that according to the method of blending a multi-component liquid of the present invention, a product having a pH and viscosity within specifications can be obtained within just one minute after the start of operation.
尚、従来法によれば、運転開始後３０分以上経過しなけ
れば、規格通りのｐＨ及び粘度を有する製品を取り出せ
なかった。In addition, according to the conventional method, a product having a specified pH and viscosity could not be taken out until 30 minutes or more had passed after the start of operation.
（混合槽）
・混合槽の高さ：２８Ｃｒｎ
・混合槽の容量： ３．３ ｎ
・混合槽の下部の内径：２５０ｃｍ
・撹拌翼の形式及び設置位置（高さ）
・１番下；ピソチドタービン、混合槽の側面の最下部か
ら１．５ ｃｎの高さに設置・下から２番目；ディスパ
ージョンタイプ、１番下の撹拌翼から６ｃｍ上方に設置
・１番上；プロペラ
・撹拌翼の速度： １７５０ｒ、ｐ、ｍ。(Mixing tank) - Height of mixing tank: 28Crn - Capacity of mixing tank: 3.3 n - Inner diameter of lower part of mixing tank: 250cm - Type and installation position (height) of stirring blades - Bottom: Pisotide turbine, Installed at a height of 1.5 cm from the bottom of the side of the mixing tank ・Second from the bottom; dispersion type, installed 6 cm above the bottom stirring blade ・Top: propeller/stirring blade speed: 1750r, p, m.
・各液体供給口（の中心）の設置位５！（高さ）：混合
槽の側面の最下部から４
国上方
（多成分液体）
・アルキルエーテルサルフェート １８重量％・３級
アミンオキサイド ３重量％・ヤシ脂肪酸
ジェタノールアミド ３０重量％・パラトルエンスル
ホン酸ソーダ ２重量％・オクテニルコハク酸ソー
ダ ０．５ 重量％・エタノール
５ｆｆｌ量％・水
バランス実施例２
実施例１と同じ構造の混合槽を用い、９つの液体供給口
からそれぞれ成分の異なる液体を供給し、下記配合の多
成分液体からなるリンスをｌｏＯＫｇ／Ｈｒの割合で連
続的に製造した。尚、少量成分及び固形成分については
、適宜な濃度の水ｆ６液又は分散液として供給した。そ
の結果を第５図に示す。・Installation position 5 of each liquid supply port (center)! (Height): 4 points from the bottom of the side of the mixing tank Kunigami (multi-component liquid) - Alkyl ether sulfate 18% by weight - Tertiary amine oxide 3% by weight - Coconut fatty acid jetanolamide 30% by weight - Para-toluenesulfonic acid Soda 2% by weight, sodium octenylsuccinate 0.5% by weight, ethanol
5ffl amount%/water
Balance Example 2 Using a mixing tank with the same structure as Example 1, liquids with different components were supplied from nine liquid supply ports, and a rinse consisting of a multi-component liquid with the following composition was continuously applied at a rate of loOKg/Hr. Manufactured. Incidentally, small amounts of components and solid components were supplied as an aqueous F6 liquid or a dispersion at an appropriate concentration. The results are shown in FIG.
第５図の結果から、本発明の多成分液体の配合方法によ
れば、運転開始後僅か３分で規格通りの粘度を有する製
品が得られることが判る。From the results shown in FIG. 5, it can be seen that according to the multi-component liquid blending method of the present invention, a product having a viscosity meeting the specifications can be obtained in just 3 minutes after the start of operation.
尚、従来法（前もって系を製品で充液）によれば、運転
開始後１０分以上経過しなければ、規格通りの粘度を有
する製品を取り出せなかった。In addition, according to the conventional method (filling the system with the product in advance), it was not possible to take out the product having the viscosity according to the specifications until 10 minutes or more had passed after the start of operation.
（多成分液体）
・塩化ジステアリルジメチル
アンモニウム １重量％
・塩化アセチルトリメチル
アンモニウム ３重量％
・モノグリセライド １重量％・セタ
ノール ３重量％・プロピレ
ングリコール ５ｆｆｉｆｆ１％・ヒドロ
キシエチルセルロース ０．５重１％・クエン酸
０．１重量％・メチルパラベン
０．１ｍｆａ％・水
バランス〔発明の効果〕
本発明の多成分液体の配合方法は、成分の異なる５種類
以上の液体を同時供給且つ瞬時混合することができるた
め、運転初期から規定の配合組成を得ることができ、そ
のため、端切りが不要で緩衝系を極小化でき且つ貯槽も
不要とするすることができ、更には、配合設備を小型化
し、配合設備の設置面積を小さくすることができ、加え
て、配合設備の極小化及びシンプル化により品種切替時
のコンタミ量の減少をを図ることができる効果を奏する
もので、原料ヘッダーを省略でき、又混合槽内の滞留量
を極小化できるため減菌作業を容易に行うことができる
等の他の効果と相俟ち、その価値の極めて高いものであ
る。(Multi-component liquid) ・Distearyldimethylammonium chloride 1% by weight ・Acetyltrimethylammonium chloride 3% by weight ・Monoglyceride 1% by weight ・Cetanol 3% by weight ・Propylene glycol 5ffiff1% ・Hydroxyethyl cellulose 0.5% by weight 1% ・Citric acid
0.1% by weight・Methylparaben 0.1mfa%・Water
Balance [Effect of the Invention] The multi-component liquid blending method of the present invention can simultaneously supply and instantaneously mix five or more types of liquids with different components, so it is possible to obtain a specified blending composition from the initial stage of operation. Therefore, the buffer system can be minimized without the need for edge cutting, and the storage tank can also be eliminated.Furthermore, the compounding equipment can be downsized and the installation area of the compounding equipment can be reduced; This has the effect of reducing the amount of contamination when changing types by minimizing and simplifying the process.The raw material header can be omitted, and the amount of retention in the mixing tank can be minimized, making sterilization work easier. Coupled with other effects such as being able to do this, it is of extremely high value.
第１図は本発明の実施に用いる装置の一例の概略を示す
側面図、第２図はその要部の概略を示す拡大図、第３図
は第１図の要部の概略を示す拡大平面図、第４図は本発
明の一実施例の結果を示すグラフ、第５図は本発明の別
の実施例の結果を示すグラフである。
１・・・混合槽
２・・・撹拌翼
３・・・液体供給口
Ｊ！１私綺閉（ｍｉｎ、）
第５図
道私ｍ関（ｍｉｎ、）
手続補正書
昭和６１年 ３月２６日
１、事件の表示
特願昭６１−４７０６７号
２、発明の名称
多成分液体の配合方法
３、補正をする者
事件との関係 特許出願人
（０９１）花 王 株式会社
４、代理人
東京都港区赤坂九丁目６番２９号
パシフィソク乃木坂６０１号
（１）第９頁１２行のｒ２５０ｃｍＪをｒ１３．４ｃｍ
Ｊと補正。
（２）第１０頁６行の「３０重量％」を「３重量％」と
補正。
（３）第１２頁６行の「減少をを」を「減少を」と補正
。
以上FIG. 1 is a side view schematically showing an example of an apparatus used for carrying out the present invention, FIG. 2 is an enlarged view schematically showing the main parts thereof, and FIG. 3 is an enlarged plan view schematically showing the main parts of FIG. 4 is a graph showing the results of one embodiment of the present invention, and FIG. 5 is a graph showing the results of another embodiment of the present invention. 1... Mixing tank 2... Stirring blade 3... Liquid supply port J! 1 Private closing (min,) Figure 5 Road private security (min,) Procedural amendment March 26, 1985 1. Indication of the case Patent application No. 1983-47067 2. Name of the invention Multi-component liquid Compounding method 3, relationship with the case of the person making the amendment Patent applicant (091) Kao Co., Ltd. 4, Agent No. 601 Nogizaka, Pacific, 9-6-29 Akasaka, Minato-ku, Tokyo (1), page 9, line 12 r250cmJ to r13.4cm
J and correction. (2) Corrected "30% by weight" in line 6 of page 10 to "3% by weight." (3) On page 12, line 6, "decrease" was corrected to "decrease". that's all
Claims (3)
下部側面又は底面に５個以上の液体供給口を設け、それ
ぞれ成分の異なる複数種の液体の供給を上記各供給口か
ら同時に開始し、供給された複数種の液体を上記撹拌翼
で撹拌混合することにより、複数種の液体からなる多成
分液体が上記混合槽内に充満する以前に、該多成分液体
を均一化するようにしたことを特徴とする多成分液体の
配合方法。(1) Five or more liquid supply ports are provided on the bottom side or bottom of a mixing tank that has stirring blades at least at the bottom of the tank, and the supply of multiple types of liquids with different components is started simultaneously from each of the above-mentioned supply ports. By stirring and mixing the supplied plural types of liquids with the stirring blade, the multi-component liquid made of the plural types of liquids is homogenized before the multi-component liquid is filled in the mixing tank. A method for blending multi-component liquids characterized by the following.
れている、特許請求の範囲第（１）項記載の多成分液体
の配合方法。(2) The method for blending a multi-component liquid according to claim (1), wherein the liquid supply ports are provided radially on the lower side surface of the mixing tank.
を電磁弁又は流体による作動弁で同時に行うようにした
、特許請求の範囲第（１）項又は第（２）項記載の多成
分液体の配合方法。(3) The multi-component according to claim (1) or (2), wherein the supply of a plurality of liquids having different components is simultaneously started and stopped by a solenoid valve or a fluid-operated valve. How to mix liquids.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61047067A JPS62204833A (en) | 1986-03-04 | 1986-03-04 | Method for blending multi-component liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61047067A JPS62204833A (en) | 1986-03-04 | 1986-03-04 | Method for blending multi-component liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62204833A true JPS62204833A (en) | 1987-09-09 |
| JPH0242534B2 JPH0242534B2 (en) | 1990-09-25 |
Family
ID=12764813
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61047067A Granted JPS62204833A (en) | 1986-03-04 | 1986-03-04 | Method for blending multi-component liquid |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62204833A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0856571A3 (en) * | 1997-01-31 | 1998-09-30 | Showa Denko Kabushiki Kaisha | Process for producing mixed refrigerants |
| WO2006094039A1 (en) * | 2005-02-28 | 2006-09-08 | Honeywell International Inc. | Improved process for blending refrigerants |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51137759U (en) * | 1975-04-30 | 1976-11-06 |
-
1986
- 1986-03-04 JP JP61047067A patent/JPS62204833A/en active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51137759U (en) * | 1975-04-30 | 1976-11-06 |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0856571A3 (en) * | 1997-01-31 | 1998-09-30 | Showa Denko Kabushiki Kaisha | Process for producing mixed refrigerants |
| WO2006094039A1 (en) * | 2005-02-28 | 2006-09-08 | Honeywell International Inc. | Improved process for blending refrigerants |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0242534B2 (en) | 1990-09-25 |
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