JPS62115266A - Thermally sterilized food and production thereof - Google Patents

Thermally sterilized food and production thereof

Info

Publication number
JPS62115266A
JPS62115266A JP25336485A JP25336485A JPS62115266A JP S62115266 A JPS62115266 A JP S62115266A JP 25336485 A JP25336485 A JP 25336485A JP 25336485 A JP25336485 A JP 25336485A JP S62115266 A JPS62115266 A JP S62115266A
Authority
JP
Japan
Prior art keywords
food
fatty acid
heat
foods
sterilized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP25336485A
Other languages
Japanese (ja)
Inventor
Hironobu Nanbu
宏暢 南部
Masatsugu Yamashita
政続 山下
Fumitaka Takeuchi
竹内 文香
Noriaki Kadota
門田 則昭
Yoshiro Toda
戸田 義郎
Nagataka Yamazaki
山崎 長孝
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Taiyo Kagaku KK
Original Assignee
Taiyo Kagaku KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Taiyo Kagaku KK filed Critical Taiyo Kagaku KK
Priority to JP25336485A priority Critical patent/JPS62115266A/en
Publication of JPS62115266A publication Critical patent/JPS62115266A/en
Pending legal-status Critical Current

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  • Food Preservation Except Freezing, Refrigeration, And Drying (AREA)

Abstract

PURPOSE:To suppress the germination and propagation of heat-resistant bacterial spores during preservation at high temperatures, by adding a polyglycerol ester of a fatty acid to a food, hermetically sealing the food in a container and sterilizing the food while heating. CONSTITUTION:A polyglycerol ester of a fatty acid is added to a food or retort food to be canned or bottled, etc. The resultant food is hermetically sealed in a container and sterilized while heating. The polyglycerol ester of the fatty acid is an ester of polyglycerol having >=6 average polymerization degree of >=970 hydroxyl value, e.g. hexaglycerol, etc., with a fatty acid, e.g. 14-24C fatty acid such as myristic acid, etc. The amount thereof to be added is 0.001-5wt%, preferably 0.01-0.3wt% based on the food.

Description

【発明の詳細な説明】 本発明は加熱滅菌食品およびその製造法に関する。詳し
くは罐詰食品、びん詰食品またはレトルト食品などの保
存食品およびその製造法に関するものである。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a heat sterilized food and a method for producing the same. More specifically, it relates to preserved foods such as canned foods, bottled foods, and retort foods, and their manufacturing methods.

(産業上の利用分野) 本発明の加熱滅菌食品およびその製造法は、人間の食生
活において加熱滅菌食品を長期に保存しいつでも、どこ
でも簡便に衛生的に食べることができ、かつ経済的に製
造する場合に有用なものである。ポリグリセリン脂肪酸
エステルは使用制限のない食品添加物として強力なO/
W、W10乳化系を作り耐塩性、耐酸性に優れた特徴を
持つ非常に重要な乳化剤である。
(Industrial Application Field) The heat-sterilized food of the present invention and its production method enable heat-sterilized food to be preserved for a long period of time in the human diet, to be eaten conveniently and hygienically anytime and anywhere, and to be produced economically. It is useful when Polyglycerin fatty acid ester is a powerful O/
It is a very important emulsifier that creates a W, W10 emulsion system and has excellent salt resistance and acid resistance.

(従来の技術) 罐詰食品、びん詰食品またはレトルト食品などの保存食
品は食品を容器に詰めて加熱滅菌し微生物の増殖を抑制
するものであるが、一般に行なわれている滅菌処理は商
業的滅菌であって、完全な無菌処理にはいたっていない
。すなわち、市販されている罐詰食品、びん詰食品また
はレトルト食品などは、通常の保存条件では腐敗変質を
おこさず消費者の健康に有害な作用を示さない程度に加
熱滅菌されたものである。しかし、このような滅菌条件
下では耐熱性細菌胞子がある程度の確率で残存している
ものである。この耐熱性細菌胞子は、普通の保存条件下
では発芽したり増殖したりすることは極めて稀であるた
め、備品食品、びん詰食品またはレトルト食品などに変
質をもたらすことは非常に少ない。しかしながら備品食
品などが自動販売機の中で、加温、販売されている条件
下では、備品食品などに残存した耐熱性細菌胞子は発芽
、増殖して食品を腐敗変質させてしまう。
(Prior art) Preserved foods such as canned foods, bottled foods, and retort foods are packaged in containers and heat sterilized to inhibit the growth of microorganisms. Although it is sterilized, it has not been completely sterilized. That is, commercially available canned foods, bottled foods, retort foods, etc. have been heat sterilized to the extent that they do not deteriorate under normal storage conditions and do not exhibit harmful effects on the health of consumers. However, under such sterilization conditions, there is a certain probability that heat-resistant bacterial spores remain. Since these heat-resistant bacterial spores rarely germinate or multiply under normal storage conditions, they are very unlikely to cause deterioration in food supplies, bottled foods, retort foods, etc. However, under conditions where food supplies and the like are heated and sold in vending machines, heat-resistant bacterial spores remaining in the food supplies germinate and multiply, causing the food to deteriorate.

このような現象はぼ酸飲料のような高酸性の食品には比
較的少ないが、中性または弱酸性の食品などは、40〜
70”Cの高温に長期間保存しておくと、滅菌されずに
残存していた耐熱性細菌胞子が発芽増殖して食品の品質
を劣化させてしまう。
This phenomenon is relatively rare for highly acidic foods such as boric acid drinks, but for neutral or weakly acidic foods,
If food is stored at a high temperature of 70"C for a long period of time, heat-resistant bacterial spores that remain without being sterilized will germinate and proliferate, degrading the quality of the food.

このような耐熱性細菌胞子を死滅させるために、滅菌温
度をあげて行なう方法があるが、この方法は食品の物理
的、化学的性質に悪影響を与えてしまい、食品としての
価値が減少してしまうため滅菌温度を一定温度以上に上
げることはできない。
In order to kill these heat-resistant bacterial spores, there is a method of raising the sterilization temperature, but this method has a negative effect on the physical and chemical properties of the food, reducing its value as a food. The sterilization temperature cannot be raised above a certain temperature because it will be stored away.

(発明が解決しようとする問題点) このようなことから、滅菌温度条件を上昇させずに備品
食品、びん詰食品またはレトルト食品などに残存する耐
熱性細菌胞子の死滅率を向上させたり、あるいは滅菌し
た備品食品などを高温に保存しても耐熱性細菌胞子の発
芽、増殖を抑制する方法の開発が望まれていた。
(Problems to be Solved by the Invention) For these reasons, it is possible to improve the killing rate of heat-resistant bacterial spores remaining in stock foods, bottled foods, retort foods, etc. without increasing the sterilization temperature conditions, or There has been a desire to develop a method that suppresses the germination and proliferation of heat-resistant bacterial spores even when sterilized food supplies are stored at high temperatures.

本発明は備品食品、びん詰食品またはレトルト食品など
を商業的滅菌して食品を製造し、高温保存中において耐
熱性細菌胞子の発芽、増殖を抑制し製品の品質を長期に
わたって一定に保つ方法を提供するものである。
The present invention provides a method for manufacturing foods by commercially sterilizing supplies, bottled foods, retort foods, etc., and suppressing the germination and proliferation of heat-resistant bacterial spores during high-temperature storage to maintain constant product quality over a long period of time. This is what we provide.

(問題を解決するための手段) 本発明者らは、備品食品、びん詰食品またはレトルト食
品などの高温における長期間保存中に耐熱性細菌胞子の
発芽、増殖を抑制する食品およびその製−法を開発する
目的で、鋭意研究を行なった結果、ポリグリセリン脂肪
酸エステルを食品に添加してなる保存食品の製造法を発
明した。
(Means for Solving the Problems) The present inventors have proposed a food product that suppresses the germination and proliferation of heat-resistant bacterial spores during long-term storage at high temperatures of food supplies, bottled food products, retort food products, etc., and a method for producing the same. As a result of intensive research, we invented a method for producing preserved foods by adding polyglycerin fatty acid esters to foods.

すなわち、本発明は安全性の高く使用制限のない食品添
加物であるポリグリセリン脂肪酸エステルを食品に添加
し、容器に密封して加熱滅菌することを特徴とする加熱
滅菌食品の製造法である。
That is, the present invention is a method for producing a heat-sterilized food, which is characterized by adding polyglycerol fatty acid ester, which is a highly safe food additive with no restrictions on use, to the food, sealing the container in a container, and heat-sterilizing the food.

本発明において用いられる食品としては、コーヒー飲料
、ココア飲料、チョコレート飲料、紅茶飲料、しるこ、
ゆであずき、その他の農畜産加工性食品などの他、スー
プ、カレー、シチュー、ハヤシ、ミートソースなどのレ
トルトソースおよびレトルト食品などがあげられる。
Foods used in the present invention include coffee drinks, cocoa drinks, chocolate drinks, black tea drinks, Shiruko,
Examples include boiled azuki beans and other agricultural and livestock processed foods, as well as retort sauces and retort foods such as soups, curries, stews, hash, and meat sauces.

本発明に用いられるポリグリセリン脂肪酸エステルは、
ヘキサグリセリン、オクタグリセリン、デカグリセリン
、エイコサグリセリン、トリアコンタグリセリンなど平
均重合度6以上、または水酸基価970以下のポリグリ
セリンの脂肪酸エステルである。ポリグリセリン脂肪酸
エステルに用いられる脂肪酸は、ミリスチン酸、パルミ
チン酸ステアリン酸、ベヘニン酸、オレイン酸などの天
然系、合成系の戻素数14〜24の飽和または不飽和の
、直鎖または分峡鎖脂肪酸であり、なかでも炭素数16
〜1Bの飽和または不飽和の脂肪酸が望ましい。これら
の脂肪酸は、単独またはその混合物でもよい。
The polyglycerol fatty acid ester used in the present invention is
It is a fatty acid ester of polyglycerin having an average degree of polymerization of 6 or more or a hydroxyl value of 970 or less, such as hexaglycerin, octaglycerin, decaglycerin, eicosaglycerin, and triacontaglycerin. The fatty acids used in the polyglycerin fatty acid ester include natural and synthetic saturated or unsaturated straight-chain or split-chain fatty acids with a return prime number of 14 to 24, such as myristic acid, palmitic acid, stearic acid, behenic acid, and oleic acid. Among them, the carbon number is 16
~1B saturated or unsaturated fatty acids are preferred. These fatty acids may be used alone or in mixtures thereof.

本発明のポリグリセリン脂肪酸エステルは、平均重合度
6以上、または水酸基価970以下のポリグリセリンの
モノ、ジ、トリ、テトラ、ペンタの脂肪酸エステルであ
り、なかでもモノ、ジ、トリの脂肪酸エステルが望まし
く、これらは単独またはその混合物で用いることができ
る。
The polyglycerin fatty acid ester of the present invention is a mono-, di-, tri-, tetra-, or penta-fatty acid ester of polyglycerin with an average degree of polymerization of 6 or more or a hydroxyl value of 970 or less, and among them, mono-, di-, or tri-fatty acid esters are used. Desirably, these can be used alone or in mixtures thereof.

本発明に用いられるポリグリセリン脂肪酸エステルは食
品に対して、0.001%〜5%(重量部)添加する。
The polyglycerol fatty acid ester used in the present invention is added in an amount of 0.001% to 5% (parts by weight) to the food.

好ましくは食品に対して0.01〜0.3%(重量部)
する。0.001%の添加量では本発明の効果がなく、
5%以−Lの添加ではポリグリセリン脂肪酸エステルが
食品の風味に影響を与え、更に経済的にも高価になり望
ましくない。
Preferably 0.01 to 0.3% (parts by weight) based on food
do. If the amount added is 0.001%, there is no effect of the present invention,
Addition of 5% or more of the polyglycerol fatty acid ester affects the flavor of the food, and is also undesirable because it becomes economically expensive.

(作用) 本発明のポリグリセリン脂肪酸エステルは非常に親水性
が強く、HLB値が大きい界面活性剤であるために、耐
熱性細菌胞子の表面に作用して耐熱性細菌胞子の発芽、
増殖を抑制するものと推定される。
(Action) Since the polyglycerol fatty acid ester of the present invention is a surfactant with very strong hydrophilicity and a large HLB value, it acts on the surface of heat-resistant bacterial spores, causing germination of heat-resistant bacterial spores.
It is presumed to suppress proliferation.

次に本発明を実施例によって説明する。Next, the present invention will be explained by examples.

実施例1 1000mN当り、L−シスチン0.5g、ブドウ糖5
.0g、酵母エキス5.0g、トリプトン15.0 g
 、チオグリコール酸ナトリウム0.5g、塩化ナトリ
ウム2.5g、寒天15.0gを含む水溶液に、デカグ
リセリンモノステアリン酸エステル(Q−18U、太陽
化学■製)を加えそれぞれ、0.01.0.02.0.
03.0.05゜0.10重量%の濃度と成るように調
製し、121”C,20分間高圧加熱殺菌を行ない、試
験培地を作成した。
Example 1 Per 1000 mN, L-cystine 0.5 g, glucose 5
.. 0g, yeast extract 5.0g, tryptone 15.0g
Decaglycerin monostearate (Q-18U, manufactured by Taiyo Kagaku ■) was added to an aqueous solution containing 0.5 g of sodium thioglycolate, 2.5 g of sodium chloride, and 15.0 g of agar to give 0.01.0 g of sodium thioglycolate, respectively. 02.0.
A test medium was prepared by adjusting the concentration to a concentration of 0.03.0.05°0.10% by weight and sterilizing it by high-pressure heating at 121"C for 20 minutes.

嫌気性耐熱性細菌、バチルス・コーギュランス(Bac
illus  coagulans)及びバチルス・ス
テアロサーモフィラス(Bacillus  stea
rothermophilus)を液体培地(チオグリ
コール酸培地■“栄研。
The anaerobic heat-resistant bacterium Bacillus cogulans (Bacillus
illus coagulans) and Bacillus stearothermophilus (Bacillus stea
thermophilus) in a liquid medium (thioglycolic acid medium ■“Eiken.

、栄研化学■製)中で、55°C110日間振盪培養し
た後、培養液を121°C115分間高圧加熱殺菌を行
ない、104個/ m lの芽胞溶液を調製= 7− 表1抗菌性試験結果 し、上記の試験培地毎に0.1mlを接種して、55℃
、7日間嫌気培養を行なった。
After culturing with shaking for 110 days at 55°C in a spore solution (manufactured by Eiken Chemical Co., Ltd.), the culture solution was sterilized by high-pressure heating at 121°C for 115 minutes to prepare a spore solution containing 104 spores/ml. As a result, 0.1 ml of each of the above test media was inoculated and incubated at 55°C.
, anaerobic culture was performed for 7 days.

培養後の上記嫌気性耐熱性細菌2種の検出結果を表1及
び2に示す。
Tables 1 and 2 show the detection results of the two types of anaerobic heat-resistant bacteria after culturing.

実施例2 コーヒー豆抽出液4.5kg、インスタントコーヒー粉
末20g、牛乳1.0kg、砂糖800g。
Example 2 Coffee bean extract 4.5 kg, instant coffee powder 20 g, milk 1.0 kg, sugar 800 g.

水3.67kgを配合した後、デカグリセリンモノステ
アリン酸エステル(Q−18U、太陽化学■製)10g
を添加してコーヒー飲料(pH6,9)を調製し、10
mj!毎に試験管に分注して、121”C、20分間高
圧加熱殺菌して液体培地を作製する。これに、上記で調
製した嫌気性耐熱性細菌芽胞溶液(B、coagula
ns、菌数104/m1)10μ!を接種した後、滅菌
流動パラフィンを重層して密封し、55°C110日間
嫌気培養する。培養後、各試料液について顕微鏡観察を
行ない、嫌気性耐熱性細菌の検出率を求めた結果、10
00検体中において3件に嫌気性耐熱性細菌が認められ
、検出率は0.3%となった。
After blending 3.67 kg of water, 10 g of decaglycerin monostearate (Q-18U, manufactured by Taiyo Kagaku ■)
A coffee beverage (pH 6,9) was prepared by adding 10
mj! Dispense each sample into test tubes and sterilize them by high-pressure heating at 121"C for 20 minutes to prepare a liquid medium. To this, add the anaerobic heat-resistant bacterial spore solution (B, coagula) prepared above.
ns, bacterial count 104/m1) 10μ! After inoculation, the cells were sealed with a layer of sterilized liquid paraffin and cultured anaerobically at 55°C for 110 days. After culturing, each sample solution was observed under a microscope and the detection rate of anaerobic heat-resistant bacteria was determined to be 10.
Anaerobic heat-resistant bacteria were found in 3 out of 00 samples, resulting in a detection rate of 0.3%.

表2 抗菌性試験結果 (本発明の効果) 本発明のポリグリセリン脂肪酸エステルを添加した食品
は実施例の結果から明らかなように、自動販売機などで
加温販売される食品中で、耐熱性細菌胞子が発芽、増殖
するのを抑制する。そのため、食品を製造するに際して
特別の装置を必要としない。また食品の腐敗変質を防止
して長期間保存できるので、食品に゛よる中毒を防止し
、食品衛生上においても有用なものである。
Table 2 Antibacterial test results (effects of the present invention) As is clear from the results of the examples, the food to which the polyglycerol fatty acid ester of the present invention has been added has high heat resistance in foods sold heated in vending machines, etc. Inhibits germination and proliferation of bacterial spores. Therefore, no special equipment is required when producing food. Furthermore, since food can be stored for a long period of time by preventing spoilage and deterioration, it prevents food poisoning and is also useful in terms of food hygiene.

Claims (3)

【特許請求の範囲】[Claims] (1)ポリグリセリン脂肪酸エステルを食品に添加し容
器に密封して加熱滅菌することを特徴とする加熱滅菌食
品およびその製造法
(1) A heat-sterilized food and its manufacturing method characterized by adding polyglycerol fatty acid ester to food, sealing it in a container, and heat-sterilizing it.
(2)ポリグリセリン脂肪酸エステルのポリグリセリン
が平均重合度6以上または水酸基価970以下である特
許請求の範囲第1項記載の加熱滅菌食品およびその製造
(2) The heat-sterilized food according to claim 1, wherein the polyglycerin of the polyglycerin fatty acid ester has an average degree of polymerization of 6 or more or a hydroxyl value of 970 or less, and the method for producing the same.
(3)ポリグリセリン脂肪酸エステルの脂肪酸が炭素数
14以上である特許請求の範囲第1項記載の加熱滅菌食
品およびその製造法
(3) The heat-sterilized food according to claim 1, wherein the fatty acid of the polyglycerol fatty acid ester has 14 or more carbon atoms, and the method for producing the same.
JP25336485A 1985-11-12 1985-11-12 Thermally sterilized food and production thereof Pending JPS62115266A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP25336485A JPS62115266A (en) 1985-11-12 1985-11-12 Thermally sterilized food and production thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP25336485A JPS62115266A (en) 1985-11-12 1985-11-12 Thermally sterilized food and production thereof

Publications (1)

Publication Number Publication Date
JPS62115266A true JPS62115266A (en) 1987-05-26

Family

ID=17250318

Family Applications (1)

Application Number Title Priority Date Filing Date
JP25336485A Pending JPS62115266A (en) 1985-11-12 1985-11-12 Thermally sterilized food and production thereof

Country Status (1)

Country Link
JP (1) JPS62115266A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6355448B1 (en) 1998-06-02 2002-03-12 3M Innovative Properties Company Sterilization indicator with chemically stabilized enzyme
US7045343B2 (en) 1998-06-02 2006-05-16 3M Innovative Properties Company Sterilization indicator test packs
US7150893B1 (en) 1999-03-24 2006-12-19 Mitsubishi Chemical Corporation Milk beverage

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6355448B1 (en) 1998-06-02 2002-03-12 3M Innovative Properties Company Sterilization indicator with chemically stabilized enzyme
US6897059B2 (en) 1998-06-02 2005-05-24 3M Innovative Properties Company Sterilization indicator with chemically stabilized enzyme
US7045343B2 (en) 1998-06-02 2006-05-16 3M Innovative Properties Company Sterilization indicator test packs
US7150893B1 (en) 1999-03-24 2006-12-19 Mitsubishi Chemical Corporation Milk beverage

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