JPS6174723A - Tungsten wire rod and its production - Google Patents

Tungsten wire rod and its production

Info

Publication number
JPS6174723A
JPS6174723A JP19397384A JP19397384A JPS6174723A JP S6174723 A JPS6174723 A JP S6174723A JP 19397384 A JP19397384 A JP 19397384A JP 19397384 A JP19397384 A JP 19397384A JP S6174723 A JPS6174723 A JP S6174723A
Authority
JP
Japan
Prior art keywords
wire
tungsten
tungsten wire
hardness
fiber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP19397384A
Other languages
Japanese (ja)
Inventor
Kuninari Kimura
木村 邦成
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tokyo Tungsten Co Ltd
Original Assignee
Tokyo Tungsten Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tokyo Tungsten Co Ltd filed Critical Tokyo Tungsten Co Ltd
Priority to JP19397384A priority Critical patent/JPS6174723A/en
Publication of JPS6174723A publication Critical patent/JPS6174723A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE:To improve a wear resistance and break resistance by forming the fiber organizations more than the specified number on the unit length which is at right angles with the longitudinal direction of a wire rod. CONSTITUTION:The wear resistance and break resistance of a tungsten wire rod are much concerned with the hardness and bend fatigue strength of a wire rod. The tungsten blank material having the prescribed wire diameter is subjected to a wire drawing work at >=99.6% work rate, after performing forging and medium heat treatment. The hardness of >=650 Vickers is obtd. due to the forging being reduced while wire drawing work being increased. With said wire drawing work the fiber organizations in the 100mum unit length which is at right angles with the longitudinal direction can be formed in numbers of >=10<5>. By the achievement in the number of said fiber organizations, the break resistance is improved to at least >=five times. Consequently with >=99.6% wire drawing work, the prescribed hardness is obtd. and wear resistance and break resistance are improved.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明はタングステン線材及びその製造方法に関し、特
に、ドツトプリンタ用ワイヤとして用いられるタングス
テン線材及びその製造方法に関する。
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to a tungsten wire and a method for manufacturing the same, and particularly to a tungsten wire used as a wire for a dot printer and a method for manufacturing the same.

〔従来技術〕[Prior art]

一般にドツトプリンタ用ワイヤとしてはタングステン線
が多く用いられている。ところでドツトプリンタ用ワイ
ヤは繰り返しの印字による摩耗。
Generally, tungsten wire is often used as wire for dot printers. By the way, dot printer wires wear out due to repeated printing.

折損を防止する上から一定値以上の機械的強度が要求さ
れる。
Mechanical strength above a certain value is required to prevent breakage.

タングステン線材の耐摩耗性及び耐折損性はそれぞれ、
前者に関してはタングステン線材の硬度。
The wear resistance and breakage resistance of tungsten wire are as follows:
Regarding the former, it is the hardness of the tungsten wire.

後者に関してはタングステン線材の折シ曲げ疲労強度及
び内部欠陥が関係する。
The latter concerns the bending fatigue strength and internal defects of the tungsten wire.

上述したタングステン線材の硬度ハビッカース硬度計で
測定され、耐摩耗性のためにはビッカース硬度(Hv)
650以上が必要である。また折シ曲げ疲労強度につい
ては、第1図に示すようにタングステン線材1の半径但
)のAの半径(−!−R〕で形成された一対の角を付す
る治具2でタングステン線材を挾み左右に90度繰り返
し、折シ曲げを行う。耐折損性のためには折り曲げ強度
が第1図に示す試験方法によって5回以上耐えることが
必要である。
The hardness of the tungsten wire mentioned above is measured using a Havickers hardness tester, and the Vickers hardness (Hv) is used for wear resistance.
650 or more is required. Regarding the bending fatigue strength, as shown in Fig. 1, the tungsten wire is held in a jig 2 with a pair of corners formed by the radius (-!-R) of the tungsten wire 1. The product is sandwiched and bent 90 degrees from side to side repeatedly.For breakage resistance, the bending strength must be able to withstand 5 or more times according to the test method shown in Figure 1.

従来のタングステン線材の製造方法においては。In the conventional manufacturing method of tungsten wire.

転打加工と中間熱処理を施した後、中間熱処理により再
結晶された結晶が線引きに耐えられる結晶状態になるま
で転打加工を続ける。転打終了後の線径は2.0〜3.
0順程度となる。その後、超硬ダイスを用いてガスによ
って加熱しながら線引きを行い、所定の線径に仕上げる
After rolling and intermediate heat treatment, rolling is continued until the crystals recrystallized by the intermediate heat treatment reach a crystalline state that can withstand wire drawing. The wire diameter after rolling is 2.0 to 3.
It will be about 0 order. Thereafter, wire is drawn using a carbide die while being heated with gas, and the wire is finished to a predetermined diameter.

ところが、一般にタングステン線材ではHv=600以
上になると、加工歪が飽和状態となって線材((亀裂(
クラック)が発生しやすくなり、また折り曲げ強度が低
下してしまうという問題点があり、著しく歩留を低下さ
せてしまう。
However, in general, for tungsten wires, when Hv=600 or more, the processing strain reaches a saturated state and the wire ((cracks)
There are problems in that cracks are likely to occur and the bending strength is reduced, resulting in a significant decrease in yield.

〔発明の目的〕[Purpose of the invention]

本発明の目的は十分な硬度及び折)曲げ疲労強度が得ら
れ、しかも亀裂(クラ、り)の発生することのないタン
グステン線材を提供することである。
An object of the present invention is to provide a tungsten wire that has sufficient hardness and bending fatigue strength and does not cause cracks.

本発明の他の目的は十分な硬度及び折シ曲げ疲労強度が
得られ、しかも亀裂(クラック)が発生することのない
タングステン線材の製造方法を提供することである。
Another object of the present invention is to provide a method for manufacturing a tungsten wire that provides sufficient hardness and bending fatigue strength and does not generate cracks.

〔発明の構成〕[Structure of the invention]

本発明によれば、タングステン線材の長さ方向に延びる
億維組織の数が、この長さ方向に平行な断面において、
繊維組織の長さ方向に対して直角な単位長さ100μm
中にIO以上存在することを特徴とするタングステン線
材が得られ、このタングステン線材は線引による加工率
を99.6%以上とすることによって得られる。
According to the present invention, the number of fiber structures extending in the length direction of the tungsten wire is as follows in a cross section parallel to the length direction.
Unit length perpendicular to the length direction of the fiber structure: 100 μm
A tungsten wire characterized by the presence of IO or more in the wire is obtained, and this tungsten wire is obtained by increasing the processing rate by drawing to 99.6% or more.

〔発明の実施例〕[Embodiments of the invention]

以下本発明について実施例によって説明する。 The present invention will be explained below with reference to Examples.

所定の線径を有するタングステン素材を準備し。Prepare a tungsten material with a predetermined wire diameter.

前述したように転打加工及び中間熱処理を施して。As mentioned above, it was subjected to rolling processing and intermediate heat treatment.

線径(φ)6閤及び3順のタングステン素材とした。A tungsten material with a wire diameter (φ) of 6 mm and a wire diameter of 3 was used.

これら線年6酎及び3頗のタングステン素材を超硬ダイ
スを用いて線引きを行い、それぞれを最終的に線径0.
35 tmとした。また上記線引きの途中で線径l瓢、
0,8酬、0.6鴎、0,4隠のタングステン線材も作
製した。
These 6- and 3-year tungsten materials are drawn into wire using a carbide die, and each is finally made into a wire with a wire diameter of 0.
35 tm. Also, in the middle of the above line drawing, the wire diameter is 1,
Tungsten wires of 0.8, 0.6, and 0.4 were also produced.

上述した線引き後の線径が1 mn 、 0.8 x 
、 0.6調、0・1m及び0.35m+++のタング
ステン線材の加工率(線引き前と線引き後のタングステ
ン線材の断面積減少率をいう。)、ピッカス硬度(荷重
は500Iとした。)、繊維度(タングステン線材の長
さ方向に平行な断面において、この長さ方向に直角な単
位長さ100μm中の繊維組織の数)及び折シ曲げ回数
について試験した。この結果を第2図に示す。なおこの
試験にあたってはそれぞれの線径のタングステン線材を
10本用意し、第2図には10本のタングステン線材の
平均値を示す。
The wire diameter after drawing as described above is 1 mn, 0.8 x
, Processing rate of 0.6 tone, 0.1 m and 0.35 m+++ tungsten wire (referring to the cross-sectional area reduction rate of tungsten wire before and after drawing), Pickus hardness (load was 500 I), fiber Tests were conducted on the degree of bending (the number of fiber structures in a unit length of 100 μm perpendicular to the length direction in a cross section parallel to the length direction of the tungsten wire) and the number of bends. The results are shown in FIG. In this test, 10 tungsten wires of each diameter were prepared, and FIG. 2 shows the average value of the 10 tungsten wires.

第2図に示すように、線引き加工率が高くなるに従って
ビッカース硬度、繊維度及び折り曲げ回数ともに増加す
ることがわかる。前述したようにドツトプリンタ用ワイ
ヤとして用いられるタングステン線材においては、耐摩
耗性の上からはビッカース硬度が650以上である必要
がある。第2図から明らかなように650以上のビッカ
ース硬度を得るためには線引き加工率を99.6%以上
とすればよいことがわかる。
As shown in FIG. 2, it can be seen that as the wire drawing rate increases, the Vickers hardness, fiber content, and number of bends increase. As mentioned above, the tungsten wire used as the wire for dot printers needs to have a Vickers hardness of 650 or higher in order to have good wear resistance. As is clear from FIG. 2, in order to obtain a Vickers hardness of 650 or more, the wire drawing rate should be 99.6% or more.

第3図乃至第5図には第2図に示された数値を用いてそ
れぞれ折り曲げ回数と繊維度、線径と折9曲げ回数及び
線径とビッカース硬度との関係を示す。なお、第3図に
示す一点鎖線は転打加工及び中間熱処理を行った後の線
径が6訓及び3填のタングステン素材を線引きしたタン
グステン線材を表わす。第4図及び第5図に示す実線及
び破線はそれぞれ転打加工及び中間熱処理を行った後の
線径が6IIIII+及び3閣のタングステン素材を腺
引きしたタングステン線材を表わす。
3 to 5 show the relationships between the number of bends and fiber content, the wire diameter and the number of bends, and the wire diameter and Vickers hardness using the numerical values shown in FIG. 2, respectively. Incidentally, the dashed-dotted line shown in FIG. 3 represents a tungsten wire drawn from a tungsten material having a diameter of 6 and 3 after rolling and intermediate heat treatment. The solid lines and broken lines shown in FIGS. 4 and 5 represent tungsten wire rods obtained by drawing tungsten materials having wire diameters of 6III+ and 3 mm after rolling and intermediate heat treatment, respectively.

第3図から明らかなように折シ曲げ回数が増えるど繊維
度が急激に増加することがわかる。前述したようにドツ
トプリンタ用ワイヤに用いられるタングステン線材は耐
折損性の上から5回以上の折り曲げ強度を有することが
必要であるが、第3図に示すようにタングステン線材の
繊維度が105個/100μm以上であればこの折り曲
げ強度が得られることがわかる。また第11図及び第5
図から線径が細くなるに従って、即ち線引加工率が高く
なると折シ曲げ回数及びビッカース硬度ともに増加する
ことがわかる。特に線径6酬のタングステン素材を線引
きしたタングステン線材(実線)では最終線引後のタン
グステン線材(線径0.35 m。
As is clear from FIG. 3, the fiber content increases rapidly as the number of folds increases. As mentioned above, the tungsten wire used in the wire for dot printers must have a bending strength of 5 times or more from the viewpoint of breakage resistance. It can be seen that this bending strength can be obtained if the thickness is 100 μm or more. Also, Figures 11 and 5
It can be seen from the figure that as the wire diameter decreases, that is, as the wire drawing rate increases, both the number of bends and the Vickers hardness increase. In particular, for the tungsten wire (solid line) drawn from a tungsten material with a wire diameter of 6, the tungsten wire after the final drawing (wire diameter 0.35 m).

線引加工率99.6%)に2いては10回の折り曲げ強
度を示し、その時のビッカース強度はHv=692を示
した。また線径6閣及び3簡のタングステン線材を線引
きしたタングステン線材ともに内部亀裂(クラック)は
生じていなかった。
At a wire-drawing rate of 99.6%, the wire showed a bending strength of 10 times, and the Vickers strength at that time was Hv=692. In addition, no internal cracks were found in the tungsten wires drawn from tungsten wires with wire diameters of 6 and 3.

このように9本発明では中間熱処理後の転打加工の割合
を縮めて巌引工程の割合を多くしている。
As described above, in the present invention, the ratio of the rolling process after the intermediate heat treatment is reduced and the ratio of the rolling process is increased.

即ち線引工程での加工率を上げている。In other words, the processing rate in the wire drawing process is increased.

転打加工は高温における鍛造加工であるため。Rolling is a forging process at high temperatures.

転打加工の割合が多いと、繊維組織の発達が遅れ。If the ratio of rolling processing is high, the development of the fiber structure will be delayed.

しかも繊維組織が不揃いとなって不均一な残留歪が生じ
易く、一方線引加工の場合は均一な歪がかかり、しかも
繊維組織は著しく長手になシかつ細粒となる。
Furthermore, the fiber structure tends to be irregular and non-uniform residual strain is likely to occur.On the other hand, in the case of wire drawing, uniform strain is applied, and the fiber structure becomes extremely elongated and fine grained.

〔発明の効果〕〔Effect of the invention〕

以上説明したように本発明によれば耐摩耗性及び耐折性
の高いタングステン線材及びその製造方法が得られる。
As explained above, according to the present invention, a tungsten wire with high wear resistance and folding resistance and a method for manufacturing the same can be obtained.

また本発明によるタングステン線材の製造方法では転打
加工における加工率を減少させ、線引工程における力(
ビ[率を増加させているので新たな設備を必要とするこ
となく、実用化が容易であシ、線引き加工では1通過当
シの減面率を転打加工よりも約3()〜・10%多くす
ることが可能であるためコスト的にも優位な製造方法で
ある。
In addition, in the method for manufacturing tungsten wire according to the present invention, the processing rate in the rolling process is reduced, and the force (
Since the wire drawing rate is increased, it is easy to put it into practical use without requiring new equipment, and the area reduction rate for one pass in wire drawing is approximately 3() ~ . Since it is possible to increase the amount by 10%, it is also an advantageous manufacturing method in terms of cost.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図はタングステン線1オの折り曲げ強度試験の方法
を示すための図、第2図は線引き後のタン、ゲステン線
材の加−ロ率、ビッカース硬度、繊維度及び折シ曲げ回
数を示すだめの図、第3図は折シ曲げ回数と鐵維度との
関係に示すための図、第4図は線径と折シ曲げ回教との
関係を示すための図。 第5図は線径とビッカース硬度との関係を示すための図
である。 第3図 折り凹lフ回数C回) 線 イ+(mm ) 腺 任(mm)
Figure 1 is a diagram showing the method for testing the bending strength of tungsten wire 1. Figure 2 is a diagram showing the tungsten wire after drawing, the loading rate of the Gesten wire, the Vickers hardness, the fiber degree, and the number of folds. FIG. 3 is a diagram showing the relationship between the number of bends and the steel strength, and FIG. 4 is a diagram showing the relationship between the wire diameter and the bending rate. FIG. 5 is a diagram showing the relationship between wire diameter and Vickers hardness. Figure 3 Folding concave number C times) Line + (mm) Gland length (mm)

Claims (1)

【特許請求の範囲】 1、タングステン線材の長さ方向に延びる繊維組織の数
が、該長さ方向に平行な断面において、前記繊維組織の
長さ方向に対して直角な単位長さ100μm中に10^
5以上存在することを特徴とするタングステン線材。 2、タングステン線材を製造する方法において、線引き
による加工率を99.6パーセント以上とすることを特
徴とするタングステン線材の製造方法。
[Claims] 1. The number of fiber structures extending in the length direction of the tungsten wire is such that the number of fiber structures extending in the length direction of the tungsten wire is within a unit length of 100 μm perpendicular to the length direction of the fiber structures in a cross section parallel to the length direction. 10^
A tungsten wire material characterized by the presence of 5 or more tungsten wires. 2. A method for producing a tungsten wire, characterized in that the processing rate by drawing is 99.6% or more.
JP19397384A 1984-09-18 1984-09-18 Tungsten wire rod and its production Pending JPS6174723A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP19397384A JPS6174723A (en) 1984-09-18 1984-09-18 Tungsten wire rod and its production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP19397384A JPS6174723A (en) 1984-09-18 1984-09-18 Tungsten wire rod and its production

Publications (1)

Publication Number Publication Date
JPS6174723A true JPS6174723A (en) 1986-04-17

Family

ID=16316851

Family Applications (1)

Application Number Title Priority Date Filing Date
JP19397384A Pending JPS6174723A (en) 1984-09-18 1984-09-18 Tungsten wire rod and its production

Country Status (1)

Country Link
JP (1) JPS6174723A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20230050851A (en) * 2021-10-08 2023-04-17 한국생명공학연구원 Surface-enhanced Raman Scattering (SERS)-based immunoassay for virus

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20230050851A (en) * 2021-10-08 2023-04-17 한국생명공학연구원 Surface-enhanced Raman Scattering (SERS)-based immunoassay for virus

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