JPS6125351B2 - - Google Patents
Info
- Publication number
- JPS6125351B2 JPS6125351B2 JP54100381A JP10038179A JPS6125351B2 JP S6125351 B2 JPS6125351 B2 JP S6125351B2 JP 54100381 A JP54100381 A JP 54100381A JP 10038179 A JP10038179 A JP 10038179A JP S6125351 B2 JPS6125351 B2 JP S6125351B2
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- refrigerant
- frozen
- tank
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 claims description 41
- 239000003507 refrigerant Substances 0.000 claims description 25
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 12
- 239000002245 particle Substances 0.000 claims description 12
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 239000011344 liquid material Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000007710 freezing Methods 0.000 claims description 4
- 230000008014 freezing Effects 0.000 claims description 4
- 238000005336 cracking Methods 0.000 claims 1
- 239000008187 granular material Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 239000012263 liquid product Substances 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 101100298225 Caenorhabditis elegans pot-2 gene Proteins 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25C—PRODUCING, WORKING OR HANDLING ICE
- F25C1/00—Producing ice
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Confectionery (AREA)
- Freezing, Cooling And Drying Of Foods (AREA)
Description
【発明の詳細な説明】
本発明は液状物から粒状形体の凍結物を製造す
る方法に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for producing a frozen product in granular form from a liquid product.
従来、粒状形体の凍結物を製造するには、原液
をまずブロツクに凍結し、ついでこの凍結物を破
砕機で破砕し、さらに得られる破砕物を選別する
ことにより所望範囲の大きさの粒状物を得るか、
又は原液を粒状の型へ注入したものを凍結するこ
とにより粒状物を得る手法が知られている。 Conventionally, in order to produce frozen products in granular form, the stock solution is first frozen into blocks, then the frozen products are crushed with a crusher, and the resulting crushed products are sorted to produce granules in the desired size range. or get
Alternatively, a method is known in which granules are obtained by injecting a stock solution into a granule mold and freezing it.
しかし、上記の前者の方法では作業工程が複雑
であるうえに、製品の収率低下が免れず、さらに
滑らかな表面を有する粒状凍結物を得ることが困
難である。また、後者の方法では作業が極めて非
能率的であつて工業的規模の製造には適さない。 However, in the former method, the working process is complicated, the yield of the product is inevitably reduced, and it is difficult to obtain frozen granules having a smooth surface. Furthermore, the latter method is extremely inefficient and is not suitable for industrial scale production.
本発明者は液状物を液体窒素のごとき液体冷媒
中へ適下方式で落下させて急速に凍結すると極め
て効率的に所望の大きさの粒状凍結物が得られる
こと、及びこの場合上記液体冷媒中に形成された
粒子をその全体の約60%が凍結した時点で冷媒か
ら取り出すと得られる粒状凍結物にヒビ割れが生
ぜず、表面が滑らかになることの知見を得て本発
明をなすに至つた。 The present inventor has discovered that if a liquid material is dropped into a liquid refrigerant such as liquid nitrogen using a dropwise method and rapidly frozen, a granular frozen material of a desired size can be obtained extremely efficiently, and in this case, the liquid material is dropped into a liquid refrigerant such as liquid nitrogen and frozen rapidly. The present invention was made based on the knowledge that if the particles formed in the above are removed from the refrigerant when approximately 60% of the particles are frozen, the resulting frozen granules do not have cracks and have a smooth surface. Ivy.
したがつて、本発明は所望の大きさを有し、か
つ表面の滑らかな粒状凍結物を大量生産方式で効
果的に製造し得る方法を提供することを目的とす
る。 Therefore, an object of the present invention is to provide a method for effectively producing frozen granules having a desired size and a smooth surface in a mass production manner.
以下本発明を詳しく説明する。 The present invention will be explained in detail below.
本発明において原料として使用する液状物は広
範囲なものを包含し得、例えば水、油類またはこ
れらに蛋白質、糖類、着色料、着香料、糊料なら
びに乳化剤などを適宜添加、混合して得られる水
性液もしくは油性液を例示し得る。特に、調合飲
料、果汁のごとき液状物は凍結物としての利用面
からみて好適な原料である。 The liquid materials used as raw materials in the present invention can include a wide range of materials, such as water, oils, or those obtained by adding and mixing proteins, sugars, colorants, flavorings, thickeners, emulsifiers, etc. to these as appropriate. Examples include aqueous liquids and oily liquids. In particular, liquid products such as mixed drinks and fruit juices are suitable raw materials from the viewpoint of use as frozen products.
本発明ではこれらの液状物を滴下方式で液体冷
媒中へ落下させることにより急速凍結させるもの
であるが、この滴下方式には種々の手法が利用し
得る。例えば、添附図面の第1図ならびに第2図
に例示したごとき装置を適用するとよい。第1図
の例示の装置は、底部に適当数個の孔を設けた固
定式円形盤1内に同じく底部に適当数個の孔を設
けた回転式摺動円盤2を嵌合させ、かつ該回転式
円盤の回転に伴つて両者の孔が間欠的に一致する
ごとく配置させてある原料液の滴下手段と、その
下方に配置した液体冷媒収容槽3とから構成され
ている。なお、図中4は上記収容槽3内に配設し
たスクリユーコンベアであつて該槽3内に形成さ
れた粒状凍結物を回収するためのものである。5
はスクリユーコンベアのモーターを示す。 In the present invention, these liquid substances are rapidly frozen by dropping them into a liquid refrigerant using a dropping method, but various methods can be used for this dropping method. For example, devices such as those illustrated in FIGS. 1 and 2 of the accompanying drawings may be applied. The illustrated device shown in FIG. 1 has a rotary sliding disc 2, which also has an appropriate number of holes in its bottom, fitted into a fixed circular disc 1, which also has an appropriate number of holes in its bottom. It consists of a raw material liquid dropping means arranged so that the holes of the two are intermittently aligned with each other as the rotary disk rotates, and a liquid refrigerant storage tank 3 arranged below the dropping means. In addition, 4 in the figure is a screw conveyor disposed in the storage tank 3, and is for collecting frozen granules formed in the tank 3. 5
indicates the screw conveyor motor.
また、第2図の例示の装置は、第1段階の液量
調整コツク2と滴下液量を調整するための第2段
階の液量調整コツク3を備えた原料液の滴下手段
1とその下方に配置した液体冷媒収容槽4とから
構成されている。なお、図中5および6は第1図
に例示したものと同様なスクリユーコンベアとそ
のモーターをそれぞれ示す。 In addition, the illustrated apparatus in FIG. 2 includes a raw material liquid dropping means 1 equipped with a first stage liquid volume adjustment pot 2 and a second stage liquid volume adjustment pot 3 for adjusting the dropped liquid volume, and a lower part thereof. It is composed of a liquid refrigerant storage tank 4 arranged in a. In the figure, numerals 5 and 6 respectively indicate a screw conveyor and its motor similar to the one illustrated in FIG.
上記例示の各装置において原料液状物をそれぞ
れの滴下手段に供給して、該手段の下方に配置し
た液体媒体の収容槽へ滴下すると液状物の滴は直
ちに液体冷媒と接触して該冷媒の冷熱により外部
より急速に凍結され粒状形体の固形物となる。こ
の際、滴下手段の孔の大きさ、原料液状物の粘稠
度ならびにその表面張力によつて凍結粒状物の粒
子の大きさを調整し得る。 In each of the above-mentioned devices, when the raw material liquid is supplied to the respective dripping means and dripped into the liquid medium storage tank disposed below the means, the droplets of the liquid immediately come into contact with the liquid refrigerant, and the cooling heat of the refrigerant is generated. It is rapidly frozen from the outside and becomes a granular solid. At this time, the particle size of the frozen granules can be adjusted by the size of the holes in the dropping means, the viscosity of the raw material liquid, and its surface tension.
なお、液状物の滴を液体冷媒中で粒状形体に凍
結する際形成粒子全体が完全に凍結するに至るま
で冷媒中に形成粒子を浸漬しておくと粒系全体に
著しいヒビ割れが生ずる傾向があるので、粒系全
体の約60%程度が凍結した時点で冷媒系から取り
出すように留意すべきである。この場合、冷媒か
ら取り出された未凍結部分は粒系が保有する冷熱
により経時的に凍結されるに至る。 Furthermore, when freezing droplets of a liquid substance into a granular form in a liquid refrigerant, if the formed particles are immersed in the refrigerant until the entire formed particle is completely frozen, significant cracks tend to occur in the entire particle system. Therefore, care should be taken to remove the particles from the refrigerant system when approximately 60% of the entire particle system has frozen. In this case, the unfrozen portion taken out from the refrigerant is frozen over time due to the cold energy possessed by the grain system.
上述したごとき凍結状態の調整は冷媒槽内に配
設したスクリユーコンベアの運搬速度、該槽内の
冷媒液面とスクリユーコンベアとの間隔などを調
整することにより行い得る。 The above-mentioned freezing state can be adjusted by adjusting the transport speed of the screw conveyor disposed in the refrigerant tank, the distance between the refrigerant liquid level in the tank and the screw conveyor, etc.
本発明で使用される液体冷媒は食品衛生上無害
であり、液状物の滴を急速凍結し得るものであれ
ばよく、液体窒素、液体空気、液体炭酸等を例示
し得るが、作業の安全性の観点から液体窒素が好
ましい。なお、実際の作業にあたつては液体冷媒
槽中の冷媒の逸散を防止すべくそれの装置上の工
夫が必要であるが密閉することは液体冷媒の気化
により槽内が高圧となるので危険である。 The liquid refrigerant used in the present invention may be any one as long as it is harmless in terms of food hygiene and can quickly freeze droplets of liquid material, and examples thereof include liquid nitrogen, liquid air, and liquid carbon dioxide. From this point of view, liquid nitrogen is preferable. In addition, during actual work, it is necessary to devise measures to prevent the refrigerant in the liquid refrigerant tank from escaping, but sealing the tank will cause high pressure inside the tank due to vaporization of the liquid refrigerant. It is a danger.
本発明によつて得られる粒状凍結物はその各粒
子表面が滑らかであつて恰かも宝石のごとき光択
を示し、加えて従来法により製造したものに比し
解けにくいので種々の面に利用し得る。 The granular frozen product obtained by the present invention has a smooth particle surface and exhibits a jewel-like appearance, and is also more difficult to melt than those produced by conventional methods, so it can be used for various purposes. obtain.
以下に実施例を例示する。 Examples are illustrated below.
実施例
飲料用水を5℃に冷却し、これを口径1.7m/
mのノズルより液体窒素中に滴下し、滴下してか
ら5〜30秒後に凍結物を、その全体の60%程度を
液体窒素槽内に配設してあるスクリユーコンベア
によりその運搬速度を調節して液体窒素中から取
り出して回収する。得られた凍結物は径が2〜
7m/mの粒状を呈し綺麗な光択を有する粒氷と
なる。なお得られる粒氷の収率は70%に達する。Example: Drinking water is cooled to 5℃, and it is heated to a diameter of 1.7m.
The frozen material is dropped into liquid nitrogen from the nozzle of m, and after 5 to 30 seconds after dropping, the transportation speed is adjusted by the screw conveyor, which has about 60% of the total frozen material inside the liquid nitrogen tank. Then, remove it from liquid nitrogen and collect it. The obtained frozen material has a diameter of 2~
The ice has a grain size of 7m/m and has a beautiful light selection. The yield of ice cubes obtained reaches 70%.
添附図面の第1図ならびに第2図は本発明の実
施に用いる装置をそれぞれ模式的に例示したもの
である。
第1図において、1…固定有孔定円盤、2…回
転式有孔摺動円盤、3…液体冷媒槽、
第2図において、1…液量調整コツクを備えた
原液滴下手段、4…液体冷媒槽。
FIGS. 1 and 2 of the accompanying drawings each schematically illustrate an apparatus used for carrying out the present invention. In FIG. 1, 1... fixed perforated constant disk, 2... rotating perforated sliding disk, 3... liquid refrigerant tank, in FIG. Refrigerant tank.
Claims (1)
て粒状形体の凍結物を製造する方法において、冷
媒槽内に配設したスクリユーコンベアの運搬速度
を調節することにより、冷媒中に形成された粒子
をその全体の約60%が凍結した時点で冷媒から取
り出すことを特徴とするヒビ割れの生じない粒状
形体の凍結物を製造する方法。 2 液状物が飲食用水性液である特許請求の範囲
第1項記載の方法。 3 液状物が飲食用油性液である特許請求の範囲
第1項記載の方法。 4 液体冷媒が液体窒素である特許請求の範囲第
1項記載の方法。[Scope of Claims] 1. In a method of manufacturing a granular frozen product by dropping a liquid material into a liquid refrigerant and rapidly freezing it, the transport speed of a screw conveyor disposed in a refrigerant tank is adjusted. A method for producing frozen particles in a granular form without cracking, characterized in that the particles formed in the refrigerant are removed from the refrigerant when about 60% of the entire particles are frozen. 2. The method according to claim 1, wherein the liquid is an edible aqueous liquid. 3. The method according to claim 1, wherein the liquid is an edible oily liquid. 4. The method according to claim 1, wherein the liquid refrigerant is liquid nitrogen.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP10038179A JPS5623882A (en) | 1979-08-07 | 1979-08-07 | Preparation of frozen material of granular shape |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP10038179A JPS5623882A (en) | 1979-08-07 | 1979-08-07 | Preparation of frozen material of granular shape |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5623882A JPS5623882A (en) | 1981-03-06 |
JPS6125351B2 true JPS6125351B2 (en) | 1986-06-14 |
Family
ID=14272427
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP10038179A Granted JPS5623882A (en) | 1979-08-07 | 1979-08-07 | Preparation of frozen material of granular shape |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5623882A (en) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58133582A (en) * | 1982-02-03 | 1983-08-09 | 石川島播磨重工業株式会社 | Device for manufacturing ice grain |
JPS5952521A (en) * | 1982-09-17 | 1984-03-27 | Tsukishima Kikai Co Ltd | Jet granulation method and apparatus |
JP2514263B2 (en) * | 1990-03-29 | 1996-07-10 | 株式会社テック | Handheld terminal |
JP2514264B2 (en) * | 1990-03-29 | 1996-07-10 | 株式会社テック | Handheld terminal |
DE4022648C2 (en) * | 1990-07-17 | 1994-01-27 | Nukem Gmbh | Method and device for producing spherical particles from a liquid phase |
JPH0441285U (en) * | 1990-08-03 | 1992-04-08 | ||
JPH0441286U (en) * | 1990-08-03 | 1992-04-08 | ||
JP2666884B2 (en) * | 1994-09-01 | 1997-10-22 | 工業技術院長 | Cold transport method and apparatus using anti-freeze protein |
JP6598429B2 (en) * | 2014-01-16 | 2019-10-30 | 江崎グリコ株式会社 | Ice grain group for cold liquid food with ice and method for producing the same, container with ice grain group, and cold liquid food with ice |
JP6461631B2 (en) * | 2015-02-06 | 2019-01-30 | 江崎グリコ株式会社 | Ice grain group for cold drink with fine ice and method for producing the same, container with ice grain group, cold drink with fine ice and method for preparing the same |
JP2016189722A (en) * | 2015-03-31 | 2016-11-10 | 大陽日酸株式会社 | Whipping cream granular freezing method |
-
1979
- 1979-08-07 JP JP10038179A patent/JPS5623882A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS5623882A (en) | 1981-03-06 |
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