JPS6022088B2 - Dry fine powder raw material production equipment containing short carbon fibers - Google Patents

Dry fine powder raw material production equipment containing short carbon fibers

Info

Publication number
JPS6022088B2
JPS6022088B2 JP20454882A JP20454882A JPS6022088B2 JP S6022088 B2 JPS6022088 B2 JP S6022088B2 JP 20454882 A JP20454882 A JP 20454882A JP 20454882 A JP20454882 A JP 20454882A JP S6022088 B2 JPS6022088 B2 JP S6022088B2
Authority
JP
Japan
Prior art keywords
short carbon
carbon fibers
raw material
pair
rotating bodies
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP20454882A
Other languages
Japanese (ja)
Other versions
JPS59100720A (en
Inventor
謙三 入江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IRIE HEKIZAI KK
Original Assignee
IRIE HEKIZAI KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IRIE HEKIZAI KK filed Critical IRIE HEKIZAI KK
Priority to JP20454882A priority Critical patent/JPS6022088B2/en
Publication of JPS59100720A publication Critical patent/JPS59100720A/en
Publication of JPS6022088B2 publication Critical patent/JPS6022088B2/en
Expired legal-status Critical Current

Links

Description

【発明の詳細な説明】 (技術分野) 本発明はカーボン短繊維が単繊維状に均一に分繊混合し
たカーボン短繊維入り乾式微粉体原材料製造装置に関す
るものである。
DETAILED DESCRIPTION OF THE INVENTION (Technical Field) The present invention relates to an apparatus for producing a dry fine powder raw material containing short carbon fibers in which short carbon fibers are uniformly split and mixed into single fibers.

(従釆技術) ピッチ等の原料から作られた蓬約5r〜20仏程度のカ
ーボン繊維及びこの繊維を10仇舷程度までの各種の長
さに切断した短繊維は公知である。
(Subsidiary technology) Carbon fibers made from raw materials such as pitch and having a length of about 5 to 20 mm, and short fibers obtained by cutting these fibers into various lengths of about 10 mm are well known.

また、上記カーボン短繊維を均一に分散混合して賦形し
た各種モルタル、コンクリート、ガラス、金属、樹脂等
の成形品ないし部材が耐熱性や化学的安定性を損うこと
なく機械的強度を著しく増大することも公知である。し
かし、この種製品を作るための賦形前の粉粒ないし流動
状原料に、カーボン短繊維を均一に分散させるには大き
な困難がある。
In addition, molded products or parts such as various mortars, concrete, glass, metals, resins, etc., made by uniformly dispersing and mixing the above-mentioned short carbon fibers, have significantly increased mechanical strength without impairing heat resistance or chemical stability. It is also known to increase. However, there are great difficulties in uniformly dispersing short carbon fibers in powder or fluid raw materials before shaping to produce this type of product.

すなわち、カーボン短繊維は、多数集合した状態におい
ては、多少の振動、震蟹、鷹梓その他の力が加わること
によって、あたかも短い細毛を掃き寄せたりしたときの
ように、隣り合った短繊維同士が互いに交叉し重なり合
って、柔かく綿状の4・塊状の凝集体をつくる倭向があ
る。
In other words, when a large number of short carbon fibers are aggregated, when some force is applied such as vibration, vibration, or other force, the adjacent short fibers can move together, just like when short fine hairs are swept together. They intersect and overlap each other to form soft, cotton-like aggregates.

この凝集体における各短綾相互間の付着結合は大して強
いものではないが、手指では容易にもみほぐせないもの
である。しかし、カーボン短繊維の上述のような性質は
、これを成形品の賭形前における粉状または流動状の原
料中に添加し均一に分散混合させようとするとき大きな
欠点となる。なぜなら、カーボン短繊維を前述のような
多数の小塊状の凝集体を含んだ集合物の状態のままで成
形品原料に混入すると、この凝集塊状物は、その後の原
料の蝿拝、濠練その他の尋常の分散手段によっては単繊
維ごとに分離されず、かえって、一旦分離したカーボン
短繊維ですら成形品原料中でづ・球状に再凝集してしま
い、したがって原料中にカーボン短繊維が相互に分離し
た単繊維として均一分散した状態のものを得られないか
らである。
Although the adhesive bond between each short twill in this aggregate is not very strong, it cannot be easily loosened with fingers. However, the above-mentioned properties of short carbon fibers are a major drawback when they are added to a powdered or fluid raw material before being formed into a molded article and uniformly dispersed and mixed. This is because when short carbon fibers are mixed into the raw material for a molded product in the form of an aggregate containing many small aggregates as described above, these aggregates are likely to cause damage to the raw material in subsequent processes such as mixing, drilling, etc. Even with ordinary dispersion methods, the single fibers cannot be separated, and even the once separated short carbon fibers re-agglomerate into a spherical shape in the raw material for the molded product. This is because it is not possible to obtain separated single fibers in a uniformly dispersed state.

そのため、前述したカーボン短繊維を均一に混入したモ
ルタルやスレート板又はコンクリート成形品打設物等の
原料を得るには極めて繁雑な方法を用いなければならな
い。
Therefore, extremely complicated methods must be used to obtain raw materials for mortar, slate plates, cast concrete molded products, etc. in which the short carbon fibers described above are uniformly mixed.

すなわち、カーボン短繊維の集合物をセメントと混練す
べき水等の適当な液状物又はセメントを含む流動状態の
原料中に投入し、特殊のミキサー等によって少量ずつ燈
拝し、流動状の均一分散固液混合物とする操作を経るこ
とが必要となるのである。湿式法とでもいうべき上記方
法が非能率的で迂遠であることは言うをまたない。
That is, an aggregate of short carbon fibers is put into a suitable liquid material such as water to be mixed with cement, or into a fluidized raw material containing cement, and is mixed little by little with a special mixer, etc., to uniformly disperse it in a fluid state. It is necessary to undergo an operation to form a solid-liquid mixture. It goes without saying that the above method, which can be called a wet method, is inefficient and roundabout.

近時この種の成形材料は各種の固形材料添加物を混合し
たものをワン・パッケージにして流通させ、必要に応じ
て水等と混練すれば、それだけでモルタルを形成するよ
うになっている。
Recently, this type of molding material has come to be distributed as a single package containing a mixture of various solid material additives, and if necessary, it can be kneaded with water or the like to form mortar.

いわゆる複合材料のプレミツクス品である。ところが、
前述した問題があるので、カーボン短繊維を添加した固
形粉粒状複合材料のワン・パッケージ製品を作ることは
できず、仮に作っても時間の経過とともにカーボン短繊
維が凝集するので使用に供し得なくなる。
This is a so-called premixed composite product. However,
Due to the above-mentioned problems, it is not possible to create a one-package product of solid powder/granular composite material with added short carbon fibers, and even if it were made, the short carbon fibers would aggregate over time, making it unusable. .

これは極めて不便であり、時代の趨勢に合わない。以上
のような次第で、カーボン短繊維混入モルタル、スレー
ト板、セメント瓦ないしコンクリ−ト成形品については
、その優れた特性に着目した大きな期待と需要があるの
に、その現実の実施は微々たるものであるという現状で
ある。
This is extremely inconvenient and does not match the trends of the times. As described above, although there are great expectations and demands for mortar containing short carbon fibers, slate boards, cement tiles, and concrete molded products due to their excellent properties, there is very little actual implementation of these products. The current situation is that it is a thing.

そこで、上記セメント粉末等を含む粉粒状固形原料中に
乾状態で始めからカーボン短繊維の各単繊総が相互に比
較的十分に分離し分散混在した複合セメントを得ること
ができれば好都合である。
Therefore, it would be advantageous if a composite cement could be obtained in which all the short carbon fibers are relatively sufficiently separated and dispersed from the beginning in a dry state in a granular solid raw material containing the above-mentioned cement powder.

また、同様に、各種の溶融ガラス、溶融樹脂や未硬化樹
脂原料中に上記のような乾状態でカーボン短繊維を単繊
総に解綴して混入することができれば益するところは大
である。そのためには、集合し凝集したカーボン短繊維
の塊を液状煤質を用いず、機械的に、いわば乾式法によ
り単繊維ごとに分離し、又は凝集傾向を阻止して、分離
した単機縦の状態のまま原料に投入する必要がある。
Similarly, it would be of great benefit if short carbon fibers could be dissolved into single fibers and mixed into various molten glasses, molten resins, and uncured resin raw materials in a dry state as described above. . In order to do this, it is necessary to mechanically separate the aggregated aggregated short carbon fibers into single fibers by a so-called dry method without using liquid soot, or to prevent the agglomeration tendency and separate the single fibers into a vertical state. It is necessary to add it to the raw material as is.

ところがこのようなカーボン短繊維乾式法による解繊は
従来から大企業が試みながら遂に成功した例をさかない
。(目 的) 本発明はカーボン短繊維を単繊維状に分散混合した乾式
微粉体原材料を得る製造装置を提供することを目的とし
ている。
However, there have been no examples of large companies attempting to defibrate short carbon fibers using the dry process and finally succeeding. (Objective) The object of the present invention is to provide a manufacturing apparatus for obtaining a dry fine powder raw material in which short carbon fibers are dispersed and mixed in the form of single fibers.

(構 成) 本発明は上記目的を達成するため、表面に多数の細突起
が小間隔で立設された1対の回転体を両突起先端が僅か
の間隙で相対連動する如く対向設置し、上方にカーボン
短繊維凝集体供給装置を鞄設し、1対の回転体下方に夫
々談回転体周面には付着して回転しようとする短繊維の
移動を阻止するスイーパロールを設け、該1対のスイー
パロール対向部を優の間隙で相対運動する如く対向設置
し、1対の回転体及び1対のスィーパロール間を通過し
て分織されたカーボン短繊維を徴粉体原材料と混合する
手段を備えたことを特徴とするものである。
(Structure) In order to achieve the above-mentioned object, the present invention includes a pair of rotating bodies each having a large number of thin protrusions erected at small intervals on its surface, which are disposed opposite to each other so that the tips of both protrusions are relatively interlocked with a small gap. A short carbon fiber aggregate supply device is installed above the bag, and a sweeper roll is installed below the pair of rotating bodies to prevent the short fibers from moving by adhering to the circumferential surface of each rotating body and attempting to rotate. The opposing parts of the pair of sweeper rolls are placed opposite each other so as to move relative to each other with a large gap, and the separated short carbon fibers are mixed with the fine powder raw material by passing between the pair of rotating bodies and the pair of sweeper rolls. It is characterized by having means.

以下実施例に基づいて具体的に説明する。1は肉厚スチ
ール製円筒形回転体で外径40仇、幅8ルホであり、2
は同様の回転体で外径20仇、幅80仇である。
Hereinafter, a detailed explanation will be given based on an example. 1 is a thick-walled steel cylindrical rotating body with an outer diameter of 40mm and a width of 8mm;
is a similar rotating body with an outer diameter of 20 mm and a width of 80 mm.

いずれの回転体も表面に約3肋の間隔で円周方向に伸び
る溝がラセン状に刻設している。この溝中には糸鋸歯状
に細突起を列設した鉄製綿状体が細突起を上にして埋込
まれ固定されている。この細突起は、先端が尖鋭三角状
でピッチ3帆、高さ6肌である。円筒形回転体1と回転
体2とは、両円周面の細突起3,4の先端が接触するこ
となく数〆距たった間隔で対向するよう所定間隔をおい
て固定されている。図示しないモータ及び変速機によっ
て回転体1,2は図面上反時計方向に回転可能なように
鞠支されている。この例では、回転体1の周面の一部に
スィーパロール5,6が接触しており、同様に、回転体
2の周面にもスイーパロール7,8が接触している。回
転体1,2の中央上方にはカーボン短繊維凝集体11の
ホツパー9が固定配置されている。10はセメントモル
タル、コンクリートの材料又は混和剤等の各種原材料を
投入した蝿梓装置である。
Each of the rotating bodies has grooves extending in the circumferential direction at intervals of about three ribs in a helical pattern on the surface. In this groove, an iron cotton-like body having thin protrusions arranged in a serrated manner is embedded and fixed with the thin protrusions facing upward. These thin processes have a pointed triangular tip, a pitch of 3 sails, and a height of 6 skins. The cylindrical rotating body 1 and the rotating body 2 are fixed at a predetermined interval so that the tips of the thin protrusions 3 and 4 on both circumferential surfaces face each other several distances apart without contacting each other. The rotating bodies 1 and 2 are supported by a motor and a transmission (not shown) so that they can rotate counterclockwise in the drawing. In this example, sweeper rolls 5 and 6 are in contact with a portion of the circumferential surface of the rotating body 1, and sweeper rolls 7 and 8 are also in contact with the circumferential surface of the rotating body 2. A hopper 9 for carbon short fiber aggregates 11 is fixedly arranged above the center of the rotating bodies 1 and 2. Reference numeral 10 denotes a flywheel device into which various raw materials such as cement mortar, concrete materials, or admixtures are input.

次に作用について説明する。ホッパー9内には平均蓬約
15〃、平均長さ約3.伍皿のカーボン短繊維凝集体1
1が入れられており、これは大部分が凝集して大小不揃
いの綿状の小塊状となっている。このカーボン短繊維凝
集体1 1は、ホッパー9を振動させることによって下
方の供給口から回転体1,2の周面対向部の上部に供給
される。この時回転体1は反時計方向に毎分400回転
の速度で回転し、回転体2は反時計方向に毎分20回転
の速度で回転している。そこで、供給されたカーボン短
繊維凝集体11は、その各所に両回転体の表面に立設さ
れた各細突起によって係止され、上下反対方向に引張ら
れ、殆んど大部分が回転体1の回転にしたがい下方に移
動する。その間に上記カーボン短繊維凝集体11は、そ
の単繊維が殆んど一本づつに分離し、更にスィーパロー
ル5,7の周面の間隙から下方に落下する。この場合、
回転体1,2の周面に付着して回転しようとする単繊縦
はスィーパロール5,7によって移動を阻止される。こ
のようにして、スイーパロール5,7の間隙から下方に
落下する間にカーボン短繊維は驚くほど完全に単繊維一
本ずつに分離される。
Next, the effect will be explained. The average length of the hopper 9 is approximately 15 mm, and the average length is approximately 3 mm. Gosara short carbon fiber aggregate 1
1 is contained, and most of this aggregates into cotton-like small lumps of irregular size. This short carbon fiber aggregate 11 is supplied from the lower supply port to the upper portions of the opposing peripheral surfaces of the rotating bodies 1 and 2 by vibrating the hopper 9. At this time, the rotating body 1 is rotating counterclockwise at a speed of 400 revolutions per minute, and the rotating body 2 is rotating counterclockwise at a speed of 20 revolutions per minute. Therefore, the supplied short carbon fiber aggregates 11 are stopped by the thin protrusions erected on the surfaces of the two rotating bodies at various locations, and are pulled in opposite directions, and almost all of the short carbon fiber aggregates 11 are It moves downward according to the rotation of . During this time, most of the single fibers of the carbon short fiber aggregate 11 are separated one by one, and further fall downward through the gap between the peripheral surfaces of the sweeper rolls 5 and 7. in this case,
The single fibers attached to the circumferential surfaces of the rotating bodies 1 and 2 and attempting to rotate are prevented from moving by the sweeper rolls 5 and 7. In this way, the short carbon fibers are surprisingly completely separated into individual fibers while falling downward from the gap between the sweeper rolls 5 and 7.

落下した繊維を顕微鏡で観察したところによれば、各単
綴総の表面には殆んど損傷がなく、又切損したものも僅
少である。そして完全に単繊維一本ずつに分緩されたカ
ーボン短繊維は縄梓装置10内に落下し、縄梓装置10
内に投入されてるセメントモルタル、コンクリートの材
料又は混和剤等の各種徴粉体原材料中に均一に損梓混合
される。
When the fallen fibers were observed under a microscope, there was almost no damage to the surface of each single binding, and only a few were cut. Then, the short carbon fibers that have been completely loosened into single fibers fall into the rope sanding device 10, and the rope sanding device 10
The powder is uniformly mixed into various powdered raw materials such as cement mortar, concrete materials, or admixtures.

該各種徴粉体原材料中で一本ずつに分織されたカーボン
短繊維は再凝集することがない。(効 果) 本発明によると表面に多数の細突起が小間隔で立設され
た1対の回転体を両突起先端が値の間隙で相対運動する
如く対向設置し、上方にカーボン短繊維凝集体供給装置
を配設し、1対の回転体下方に夫々該回転体周面には付
着して回転しようとする短繊維の移動を阻止するスィー
パロールを設け、該1対のスィーパロール対向部を億の
間隙で相対運動する如く対向設置し、1対の回転体び1
対のスィーパロール間を通過して分緩されたカーボン短
繊維を各種徴粉体原材料と混合する手段を備えているの
でカーボン短繊維を単繊維状に分散混合した乾式微粉体
原材料を得ることができる。
The short carbon fibers that are individually woven in the various powder raw materials do not re-agglomerate. (Effects) According to the present invention, a pair of rotating bodies each having a large number of fine protrusions erected at small intervals on the surface are placed facing each other so that the tips of both protrusions move relative to each other with a gap of a certain value, and the short carbon fibers are aggregated upward. A collection supply device is disposed, and a sweeper roll is provided below the pair of rotating bodies to prevent movement of short fibers that adhere to the circumferential surface of the rotating bodies and try to rotate, and the pair of sweeper rolls face each other. A pair of rotating bodies and a
Since it is equipped with a means for mixing the short carbon fibers that have been loosened by passing between a pair of sweeper rolls with various powder raw materials, it is possible to obtain a dry fine powder raw material in which the short carbon fibers are dispersed and mixed in the form of single fibers. can.

【図面の簡単な説明】[Brief explanation of the drawing]

図は本発明の一実施例正面図である。 1,2…・・・回転体、3,4・・・・・・細突起、5
,7……スイーパロール、9……ホツパー、10……濃
洋装層、11・・・・・・カーボン短繊維凝集体。
The figure is a front view of one embodiment of the present invention. 1, 2...Rotating body, 3, 4...Thin protrusions, 5
, 7...Sweeper roll, 9...Hopper, 10...Dense clothing layer, 11...Carbon short fiber aggregate.

Claims (1)

【特許請求の範囲】[Claims] 1 表面に多数の細突起が小間隔で立設された1対の回
転体を両突起先端が僅の間隙で相対運動する如く対向設
置し、上方にカーボン短繊維凝集体供給装置を配設し、
1対の回転体下方に夫々該回転体周面には付着して回転
しようとする短繊維の移動を阻止するスイーパロールを
設け、該1対のスイーパロール対向部を僅の間隙で相対
運動する如く対向設置し、1対の回転体及び1対のスイ
ーパロール間を通過して分繊されたカーボン短繊維を微
粉体原材料と混合する手段を備えたカーボン短繊維入り
乾式微粉体原材料製造装置。
1. A pair of rotating bodies each having a large number of thin protrusions erected at small intervals on the surface thereof are placed facing each other so that the tips of both protrusions move relative to each other with a small gap, and a carbon short fiber aggregate supply device is arranged above. ,
Sweeper rolls are provided below the pair of rotating bodies to prevent the movement of short fibers that adhere to the circumferential surfaces of the rotating bodies and attempt to rotate, and the opposing parts of the pair of sweeper rolls are moved relative to each other with a small gap. A dry-type fine powder raw material production device containing carbon short fibers is provided with means for mixing carbon short fibers separated by passing between a pair of rotating bodies and a pair of sweeper rolls with a fine powder raw material.
JP20454882A 1982-11-24 1982-11-24 Dry fine powder raw material production equipment containing short carbon fibers Expired JPS6022088B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP20454882A JPS6022088B2 (en) 1982-11-24 1982-11-24 Dry fine powder raw material production equipment containing short carbon fibers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP20454882A JPS6022088B2 (en) 1982-11-24 1982-11-24 Dry fine powder raw material production equipment containing short carbon fibers

Publications (2)

Publication Number Publication Date
JPS59100720A JPS59100720A (en) 1984-06-11
JPS6022088B2 true JPS6022088B2 (en) 1985-05-31

Family

ID=16492327

Family Applications (1)

Application Number Title Priority Date Filing Date
JP20454882A Expired JPS6022088B2 (en) 1982-11-24 1982-11-24 Dry fine powder raw material production equipment containing short carbon fibers

Country Status (1)

Country Link
JP (1) JPS6022088B2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6630991B2 (en) 2017-05-17 2020-01-15 株式会社新菱 Method for producing recycled carbon fiber bundle, recycled carbon fiber, milled recycled carbon fiber, apparatus for producing recycled carbon fiber bundle, method for producing carbon fiber reinforced resin, and method for producing carbon fiber reinforced resin pellet

Also Published As

Publication number Publication date
JPS59100720A (en) 1984-06-11

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