JPS5954005B2 - Continuous kneading machine - Google Patents

Continuous kneading machine

Info

Publication number
JPS5954005B2
JPS5954005B2 JP382780A JP382780A JPS5954005B2 JP S5954005 B2 JPS5954005 B2 JP S5954005B2 JP 382780 A JP382780 A JP 382780A JP 382780 A JP382780 A JP 382780A JP S5954005 B2 JPS5954005 B2 JP S5954005B2
Authority
JP
Japan
Prior art keywords
kneading
chamber
discharge
chambers
section
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP382780A
Other languages
Japanese (ja)
Other versions
JPS56101811A (en
Inventor
慎治 橋爪
伸一 福水
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kobe Steel Ltd
Original Assignee
Kobe Steel Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kobe Steel Ltd filed Critical Kobe Steel Ltd
Priority to JP382780A priority Critical patent/JPS5954005B2/en
Priority to GB8100984A priority patent/GB2069354B/en
Priority to IT8119156A priority patent/IT1135054B/en
Priority to FR8100669A priority patent/FR2473352A1/en
Priority to DE3101083A priority patent/DE3101083C2/en
Priority to US06/225,774 priority patent/US4380397A/en
Publication of JPS56101811A publication Critical patent/JPS56101811A/en
Publication of JPS5954005B2 publication Critical patent/JPS5954005B2/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/30Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/46Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/465Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft each shaft comprising rotor parts of the Banbury type in addition to screw parts

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Description

【発明の詳細な説明】 本発明は、均一な混練が得られる連続式混練機に関する
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a continuous kneader that can provide uniform kneading.

一般に合成樹脂等の高分子物質を混練する場合、混練
時間を短縮して生産性を向上させるために、材料の供給
、混練、排出を連続的に行い得る連続式混練機が用いら
れている。なかても二軸型の連続式混練機は、単軸型に
比べてせん断熱による溶融効果が高く、混練効率を高め
る一とができるので、好評を得ている。ところで、この
二軸型の連続式混練機を用いた場合、材料の種類や混合
比によつては材料の一部がほとんどせん新作用を受けず
に混練部を通過する所謂ショートバス現象が生じる場合
があり、これによつて混練の均一性を阻害し、製品の品
質を劣化させるおそれがあつた。
Generally, when kneading polymeric substances such as synthetic resins, a continuous kneader that can continuously supply, knead, and discharge materials is used in order to shorten kneading time and improve productivity. In particular, twin-screw continuous kneaders are popular because they have a higher melting effect due to shear heat than single-screw kneaders and can improve kneading efficiency. By the way, when this twin-screw type continuous kneading machine is used, a so-called short bath phenomenon occurs in which a part of the material passes through the kneading section with almost no shearing action, depending on the type of material and the mixing ratio. In some cases, this may impede the uniformity of kneading and deteriorate the quality of the product.

本発明は、このような事情に鑑み、二軸型の連続式混練
機の効果を保持しながら、ショートバス現象を防止して
混練の均一化を図り、製品の品質を向上べきるようにす
ることを目的とするものである。
In view of these circumstances, the present invention aims to improve the quality of products by preventing the short bath phenomenon and ensuring uniform kneading while maintaining the effects of a two-screw continuous kneading machine. The purpose is to

本発明は、一端に材料供給口を、他端に吐出圧調整用絞
り機構を有する吐出口を備えたチャンバー内に2本の混
練軸を平行に配置し、各混練軸にそれぞれフィード部、
混練部およびディスチャージ部を設けてなる連続式混練
機において、チャンバー内で各混練軸のディスチャージ
部に対応する室の底部内面にそれぞれ円孤状の堰を互い
に連続するように突設し、混練部により混練された材料
Jがこの堰を乗り越えて送り出されるようにし、以つて
、ショートバスを防止して混練の均一化を可能にしたも
のである。
In the present invention, two kneading shafts are arranged in parallel in a chamber equipped with a material supply port at one end and a discharge port having a throttle mechanism for adjusting discharge pressure at the other end, and each kneading shaft has a feed section and a
In a continuous kneading machine having a kneading section and a discharge section, arc-shaped weirs are protruded continuously from the bottom inner surface of the chamber corresponding to the discharge section of each kneading shaft in the chamber. The kneaded material J is sent out over this weir, thereby preventing short baths and making it possible to make the kneading uniform.

以下、本発明の実施例を図によつて説明する。Embodiments of the present invention will be described below with reference to the drawings.

1はチャンバーで、一端に材料供給口2を、他丁端に吐
出口3を有していると共に、内部に断面眼鏡の空洞部を
有し、その中に2本の混練軸4、4’を平行に配置して
いる。
Reference numeral 1 denotes a chamber, which has a material supply port 2 at one end and a discharge port 3 at the other end, and has a hollow section shaped like a cross-section glass inside, and two kneading shafts 4, 4' are installed in the chamber. are arranged in parallel.

混練軸4、4’は、材料供給端から順に、フィード部4
1、41′と、混練部42、42’と、デθイスチヤー
ジ部43、43’を備えている。
The kneading shafts 4, 4' are connected to the feed section 4 in order from the material supply end.
1 and 41', kneading sections 42 and 42', and discharge θ discharge sections 43 and 43'.

フィード部41、41’はスクリュー形状をなし、混練
部42、42’は、断面オーバル形状の翼が、その始端
側から中間部まで順ねじ方向にねじれ、ついでその先か
ら終端側に逆ねじ方向にねじれた■5状態で連続して形
成されてなり、ディスチャージ部43、43’は、混練
部42、42′と同一断面のストレートな翼で形成され
ている。そして、これら各部に対応してチヤンバ一1内
の空洞部に、フイード室11,11″と、混練室12,
12″と、デイスチヤージ室13,13″が形成され、
これら各室は軸方向に連続し、かつ横断面において左右
に隣接する各室が互いに連通している。
The feed sections 41, 41' have a screw shape, and the kneading sections 42, 42' have blades with an oval cross section twisted in a normal thread direction from the starting end side to the middle part, and then twisted in a counter thread direction from the tip to the terminal side. The discharge parts 43, 43' are formed of straight blades having the same cross section as the kneading parts 42, 42'. Corresponding to these parts, feed chambers 11, 11'', kneading chambers 12,
12'' and discharge chambers 13, 13'' are formed,
These chambers are continuous in the axial direction, and adjacent chambers on the left and right in the cross section communicate with each other.

なお、吐出口3には吐出圧調整用絞り機構として開度調
節可能なオリフイス5を設けている。このような連続式
混練機において、本発明ではどくにチヤンバ一1内でデ
イスチヤージ室13,13″の底部内面に堰6,6″を
突設したのである。
Note that the discharge port 3 is provided with an orifice 5 whose opening degree can be adjusted as a throttle mechanism for adjusting the discharge pressure. In such a continuous kneading machine, the present invention specifically provides weirs 6, 6'' projecting from the bottom inner surface of the discharge chambers 13, 13'' within the chamber 11.

堰6,6″は、断面形状が山形で、前記室13,13″
の底面の周方向に沿つて円孤状に形成し、かつ、左右の
堰6,6″が互に連続するように形成する。該堰6,6
″は、チヤンバ一1の室13,13″の内面に一体に突
設してもよいし、別体のものをボルト等の取付手段によ
り着脱自在に取付けて一体化してもよい。一方、混練軸
4,4″のデイスチヤージ部43,43″において、前
記堰6,6″に対向する部分に凹部44,44″を形成
し、混練軸4,4″が支障なく回転できるようにする。
The weirs 6, 6'' have a chevron-shaped cross section, and the chambers 13, 13''
It is formed into a circular arc shape along the circumferential direction of the bottom surface, and the left and right weirs 6, 6'' are formed to be continuous with each other. The weirs 6, 6
'' may be provided integrally protruding from the inner surfaces of the chambers 13, 13'' of the chamber 11, or may be separate pieces that are removably attached using attachment means such as bolts and integrated. On the other hand, in the discharge parts 43, 43'' of the kneading shafts 4, 4'', recesses 44, 44'' are formed in the portions facing the weirs 6, 6'', so that the kneading shafts 4, 4'' can rotate without hindrance. do.

また、チヤンバー1は少なくとも堰6,6″に対応する
部分、実施例では混練室12,12″とデイスチヤージ
室13,13″を上下にニツ割に形成し、混練軸4,4
″をチヤンバ一1から抜取る際に堰6,6″が邪魔にな
らないようにする。次に、当該混練機の作用について説
明する。
Further, the chamber 1 has at least a portion corresponding to the weirs 6, 6'', in the embodiment, the kneading chambers 12, 12'' and the discharge chambers 13, 13'' are vertically divided, and the kneading shafts 4, 4
To prevent the weirs 6, 6'' from getting in the way when extracting the material from the chamber 11. Next, the operation of the kneader will be explained.

チヤンバ一1の供給口2から投入されたペレツト状もし
くはパウダー状の被混線材料Aは、混練軸4,4″のフ
イード部41,41゛により前方の混練室12,12″
に送られ、この混練室12,12″内において、次のよ
うな混練作用を受ける。すなわち、材料Aは第4図に示
すように、混練・部42,42/の回転前方にあつて矢
印イ,イ彷向に回転され(その回転中に材料Aの一部が
混練部42,42″の先端チツプランド42a,42b
,42a″, 42″bと混練室12,12″内面のク
リアランスを通過し、この間にせん断熱を受けqて昇温
し、溶融される。
The pellet-like or powder-like mixed material A introduced from the supply port 2 of the chamber 1 is fed into the kneading chambers 12, 12'' in the front by the feed portions 41, 41' of the kneading shafts 4, 4''.
In the kneading chambers 12, 12'', the material A is subjected to the following kneading action.As shown in FIG. (during the rotation, part of the material A is rotated in the opposite direction of the kneading section 42, 42'')
, 42a'', 42''b and the inner surfaces of the kneading chambers 12, 12'', during which time they are subjected to shear heat q, heated up, and melted.

一方、混練部12,12″の回転前方には未溶融材料が
あり、さらにその上層には先のチツプランド等のせん断
作用等によつて溶融された材料があり、この溶融材料と
未溶融材料の層の境界部で溶融材料が未溶融材料中に進
入すると共に、この間に熱の伝達が行なわれ、溶融、混
練される。この場合、混練軸4,4″が一回転する間に
前記クリアランスを通過する材料は全材料Aのうちの一
部であり、他の大部分の材料は混練部42,42″の回
転前方にある。
On the other hand, there is an unmelted material in front of the rotation of the kneading section 12, 12'', and further above that there is a material that has been melted by the shearing action of the chip land, etc., and this molten material and unmelted material are separated. The molten material enters the unmelted material at the boundary between the layers, and during this time heat is transferred, melting and kneading.In this case, the above-mentioned clearance is maintained during one rotation of the kneading shafts 4, 4''. The material passing through is a part of the total material A, and most of the other material is in front of the rotation of the kneading sections 42, 42''.

そして、混練部42,42″の回転によつて、前記チツ
プランドが混練室12,12″の上壁交点12aを通過
するときフに、前記溶融材料と未溶融材料およびそれら
の一部混合材料とが入り混つて混練部42,42″間の
中心空間Cに放出され、然る後、混練室12,12″の
底壁交点12bによつて左右の混練室12,12″に振
り分けられ、以下、上記作用を繰・り返すことによつて
前記材料Aが次第に溶融、混練されながらフイード室1
1,1「から送り込まれる後続の材料に押されてデイス
チヤージ室13,13″側に送り出される。このような
混線状態において、混練室12,1ノ2″の中間部もし
くは終端部近くでは、前記の如く混練部42,42″の
回転によつて中心空間Cに放出される材料の一部が底壁
頂点12bによつて左右の混練室12,12″に振り分
けられる前にデイスチヤージ室13,13″に飛び込も
うとし、あるいは振り分けられた直後にデイスチヤージ
室13,13″に流出しようとする傾向がある。
By the rotation of the kneading parts 42, 42'', when the chips pass through the upper wall intersection 12a of the kneading chambers 12, 12'', the molten material, unmelted material, and a part of the mixed material are mixed together. are mixed and discharged into the central space C between the kneading sections 42, 42'', and then distributed to the left and right kneading chambers 12, 12'' by the bottom wall intersection 12b of the kneading chambers 12, 12'', and the following By repeating the above action, the material A is gradually melted and kneaded, and then the material A is transferred to the feed chamber 1.
It is pushed by the subsequent material fed in from 1, 1'' and is sent to the discharge chamber 13, 13'' side. In such a mixed line state, a part of the material discharged into the central space C by the rotation of the kneading sections 42, 42'' as described above is in the middle part or near the end of the kneading chambers 12, 1 and 2''. There is a tendency for the mixture to jump into the discharge chambers 13, 13'' before being distributed to the left and right kneading chambers 12, 12'' by the bottom wall apex 12b, or to flow out to the discharge chambers 13, 13'' immediately after being distributed. .

この場合、従来のようにチヤンバ一内壁面とくに底部に
何ら障害物がなく、混練室とデイスチヤージ室が均一断
面形状であると、前記の如く混練室の中間部もしくは終
端部近くからデイスチヤージ室に飛び込み、あるいは流
出しようとした材料が何の抵抗もなくそのま・飛び込み
、あるいは流出してしまう。
In this case, if there are no obstacles on the inner wall surface of the chamber, particularly the bottom, and the kneading chamber and the de-staging chamber have uniform cross-sectional shapes, as in the past, water will jump into the de-staging chamber from the middle or near the end of the kneading chamber. , or the material that was about to flow out will simply jump in or flow out without any resistance.

これがいわゆるシヨートパス現象であり、このシヨート
パスした材料の中には未溶融材料が含まれている。なお
、こうしてデイスチヤージ室に送り込まれた材料はデイ
スチヤージ部により吐出口を経て機外に吐出されるが、
こ・では積極的な混練作用は受けず、ほとんどそのま・
で送り出される。従つて、従来の混練機では、未溶融材
料が含まれたま・機外に送り出されることになり、これ
が製品の品質を劣下する要因となつていた。然るに、本
発明によれば、デイスチヤージ室13,13″に円孤状
の堰6,6″を互いに連続して突設してあるので、前記
混練室12,12″の中間部もしくは終端部近くからデ
イスチヤージ室13,13″に飛び込もうとし、あるい
は流出しようとした材料は、堰6,6″に当つて混練室
12,12″に戻され、同室12,12″で再び前記同
様のせん断、溶融、混練作用を受ける。
This is the so-called short pass phenomenon, and the short pass material contains unmelted material. The material fed into the discharge chamber in this way is discharged outside the machine through the discharge port by the discharge section.
In this case, there is no active kneading effect, and the product is processed almost as is.
sent out. Therefore, in conventional kneading machines, the unmelted material is sent out of the kneading machine, which is a factor in degrading the quality of the product. However, according to the present invention, since the circular arc-shaped weirs 6, 6'' are continuously protruded from the discharge chambers 13, 13'', the discharging chambers 13, 13'' are provided with circular weirs 6, 6'' that protrude continuously from each other. The material that was about to jump into or flow out from the discharge chamber 13, 13'' hits the weir 6, 6'' and is returned to the kneading chamber 12, 12'', where it is again subjected to the same shearing and melting as described above. , subjected to kneading action.

これによつて、従来のようなシヨートパスが生じること
を防止できると共に、混練室12,12″内の材料の滞
溜時間分布(時間差)を短くでき、滞溜時1間を均一化
でき、かつ、せん断作用を受ける度数、すなわちシャー
レート値を高くでき、溶融、混練効率を高め、充分に混
練させることができる。さらにこの場合、混練室12,
12″の底部とくに両室12,12″間の中心空間Cで
シヨートパスが生じやすいので、堰6,6″を第5図お
よび第6図に示すように形成するのが効果的である。
This makes it possible to prevent the occurrence of shot passes as in the conventional case, shorten the residence time distribution (time difference) of the materials in the kneading chambers 12 and 12'', and make the residence time 1 hour uniform. , the frequency of shearing action, that is, the shear rate value, can be increased, the melting and kneading efficiency can be increased, and sufficient kneading can be achieved.Furthermore, in this case, the kneading chamber 12,
Since short passes are likely to occur at the bottom of the chambers 12'', particularly in the central space C between the two chambers 12, 12'', it is effective to form the weirs 6, 6'' as shown in FIGS. 5 and 6.

すなわち、チヤンバ一1の軸方向に対して直交する断面
において、室13,13″を横方向の中心線xと縦方向
の中心線Y,Y″によつてそれぞれ第1〜第4象限〜I
に区画して説明すると、一方の堰6は室13の第2象限
11内に位置した中心点0を中心として円孤状に形成し
、他方の堰6″は室13″の第1象限1内に位置した中
心点0″を中心として円孤状に形成し、両堰6,6″の
連続部の頂部6aが中心線xより上方に位置し、その反
対側の端部6b,6b″に適当な丸味をもたせるように
する。こうすれば、中心空間Cで起りやすいシヨートパ
ス現象を一層確実に防止でき、前記溶融、混練効率を一
層高め、より完全に混練させることができる。混練室1
2,12″で完全に溶融、混練された材料は、フイード
室11,1「から送り込まれる後続の材料に押され、前
記堰6,6″をオーバーフローしてデイスチヤージ室1
3,13″に流入し、デイスチヤージ部43,43″に
より吐出口3から機外に吐出される。
That is, in a cross section perpendicular to the axial direction of the chamber 1, the chambers 13, 13'' are divided into the first to fourth quadrants to I by the horizontal center line x and the vertical center line Y, Y'', respectively.
One weir 6 is formed in an arc shape centered on the center point 0 located in the second quadrant 11 of the chamber 13, and the other weir 6'' is formed in the first quadrant 1 of the chamber 13''. The apex 6a of the continuous part of both weirs 6, 6'' is located above the center line x, and the opposite ends 6b, 6b'' By doing so, the short pass phenomenon that tends to occur in the center space C can be more reliably prevented, the melting and kneading efficiency can be further increased, and the kneading can be performed more completely.Kneading chamber 1
The material completely melted and kneaded in the feed chambers 11 and 12'' is pushed by the subsequent material fed from the feed chambers 11 and 1'', overflows the weirs 6 and 6'' and flows into the discharge chamber 1.
3, 13'', and is discharged outside the machine from the discharge port 3 by the discharge portions 43, 43''.

以上説明したように、本発明によればデイスチヤージ室
に設けた円孤状で互いに連続した堰によつて、シヨート
パス現象を防止でき、混練室における材料の滞溜時間を
均一化し、混練度のばらつきを小さくし、製品の品質を
格段に向上することができる。
As explained above, according to the present invention, the short pass phenomenon can be prevented by the arc-shaped and mutually continuous weir provided in the discharging chamber, and the residence time of the material in the kneading chamber is made uniform, resulting in variations in the degree of kneading. can be made smaller and the quality of the product can be significantly improved.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本発明の連続式混練機の実施例を示す縦断正面
図、第2図はその横断平面図、第3図はそのデイスチヤ
ージ室の縦断側面図、第4図は混線状態を示す同機混練
室の縦断側面図、第5図は別の実施例を示すデイスチヤ
ージ室の縦断側面図、第6図はその堰の縦断正面図であ
る。 1・・・チヤンバ一、2・・・材料供給口、3・・・吐
出口、4,4″・・・混練軸、5・・・オリフイス、6
,6″・・・堰、11,1「・・・フイード室、12,
12Z・・混練室、13,13″・・・デイスチヤージ
室、41,4「・・・フイード部、42,42″・・・
混練部、43,43″・・・デイスチヤージ部。
Fig. 1 is a longitudinal sectional front view showing an embodiment of the continuous kneading machine of the present invention, Fig. 2 is a cross-sectional plan view thereof, Fig. 3 is a longitudinal sectional side view of the discharging chamber, and Fig. 4 is the same machine showing a mixed line state. FIG. 5 is a vertical side view of the discharge chamber showing another embodiment, and FIG. 6 is a vertical front view of the weir. DESCRIPTION OF SYMBOLS 1...Chamber 1, 2...Material supply port, 3...Discharge port, 4,4''...Kneading shaft, 5...Orifice, 6
,6"...Weir, 11,1"...Feed chamber, 12,
12Z...kneading chamber, 13,13''...discharge chamber, 41,4''...feed section, 42,42''...
Kneading section, 43, 43''... discharging section.

Claims (1)

【特許請求の範囲】[Claims] 1 一端に材料供給口を、他端に吐出圧調整用絞り機構
を有する吐出口を備えたチャンバー内に2本の混練軸を
平行に配置し、各混練軸にそれぞれフィード部、混練部
、ディスチャージ部を設けてなる二軸型連続式混練機に
おいて、チャンバー内で各混練軸のディスチャージ部に
対応する室のの底部内面にそれぞれ円孤状の堰を互いに
連続するように突窃したことを特徴とする連続式混練機
1 Two kneading shafts are arranged in parallel in a chamber equipped with a material supply port at one end and a discharge port with a throttle mechanism for adjusting discharge pressure at the other end, and each kneading shaft has a feed section, a kneading section, and a discharge section. A two-shaft continuous kneading machine having two shafts is characterized in that arc-shaped weirs are continuous with each other on the inner surface of the bottom of the chamber corresponding to the discharge part of each kneading shaft in the chamber. Continuous kneading machine.
JP382780A 1980-01-16 1980-01-16 Continuous kneading machine Expired JPS5954005B2 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP382780A JPS5954005B2 (en) 1980-01-16 1980-01-16 Continuous kneading machine
GB8100984A GB2069354B (en) 1980-01-16 1981-01-13 Continuous mixing
IT8119156A IT1135054B (en) 1980-01-16 1981-01-15 DOUBLE TYPE CONTINUOUS MIXER
FR8100669A FR2473352A1 (en) 1980-01-16 1981-01-15 CONTINUOUS MIXER
DE3101083A DE3101083C2 (en) 1980-01-16 1981-01-15 Continuously working mixer with two parallel mixing chambers
US06/225,774 US4380397A (en) 1980-01-16 1981-01-16 Duplex type continuous mixer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP382780A JPS5954005B2 (en) 1980-01-16 1980-01-16 Continuous kneading machine

Publications (2)

Publication Number Publication Date
JPS56101811A JPS56101811A (en) 1981-08-14
JPS5954005B2 true JPS5954005B2 (en) 1984-12-27

Family

ID=11568024

Family Applications (1)

Application Number Title Priority Date Filing Date
JP382780A Expired JPS5954005B2 (en) 1980-01-16 1980-01-16 Continuous kneading machine

Country Status (1)

Country Link
JP (1) JPS5954005B2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5175822B2 (en) * 2009-10-22 2013-04-03 株式会社神戸製鋼所 Kneading equipment

Also Published As

Publication number Publication date
JPS56101811A (en) 1981-08-14

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