JPS5941457A - Heat treatment method - Google Patents

Heat treatment method

Info

Publication number
JPS5941457A
JPS5941457A JP15101282A JP15101282A JPS5941457A JP S5941457 A JPS5941457 A JP S5941457A JP 15101282 A JP15101282 A JP 15101282A JP 15101282 A JP15101282 A JP 15101282A JP S5941457 A JPS5941457 A JP S5941457A
Authority
JP
Japan
Prior art keywords
heat treatment
amorphous material
subjected
present
corrosion resistance
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP15101282A
Other languages
Japanese (ja)
Inventor
Ryozo Sawada
沢田 良三
Katsuto Yoshizawa
克仁 吉沢
Ryoichi Shibata
良一 柴田
Yasuo Arai
新井 保夫
Shunsuke Arakawa
俊介 荒川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Proterial Ltd
Original Assignee
Hitachi Metals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Metals Ltd filed Critical Hitachi Metals Ltd
Priority to JP15101282A priority Critical patent/JPS5941457A/en
Publication of JPS5941457A publication Critical patent/JPS5941457A/en
Pending legal-status Critical Current

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  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

PURPOSE:To apply stable heat treatment without generating irregularity in characteristics, by a method wherein an amorphous material is immersed in a selected resin liquid to be held at a high temp. CONSTITUTION:A material to be subjected to heat treatment being an amorphous material is immersed in a liquid prepared by using resins having a b.p. higher than 100 deg.C and held at 60 deg.C or more to be subjected to heat treatment. By this method, the amorphous material can be subjected to heat treatment without generating irregularity in magnetic properties, strength or the like and unstability from the point of view of corrosion resistance. In this case, if treatment is performed at a temp. lower than 60 deg.C, corrosion resistant stability becomes poor.

Description

【発明の詳細な説明】 本発明はアモルファス4Δ料の熱処理法に関するもので
ある。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for heat treating an amorphous 4Δ material.

従来、アモルファス材料はA r雰囲気中等の不活性ガ
スにて熱処理していた。。しかし、一般に、アモルファ
ス材料の熱処理温度は低く、このため均一な温度分布に
なるまでの時間が永くかかり、焼鈍むらを生じて、部分
的な焼鈍不足あるいは部分的な過焼鈍の状態になる欠点
がめった。また、たとえば磁性コアの場合など、磁性の
バラツキばかりでなく機械的強度の不足を生じるケース
が発生し、さらにまた、耐蝕材料9強度材料の場合には
耐蝕性のむら、あるいは強度−Lのバラツキを生ずるケ
ース等も多々あった。
Conventionally, amorphous materials have been heat treated in an inert gas such as an Ar atmosphere. . However, the heat treatment temperature for amorphous materials is generally low, so it takes a long time to achieve a uniform temperature distribution, resulting in uneven annealing and partial under-annealing or partial over-annealing. Rarely. In addition, for example, in the case of a magnetic core, there are cases where not only the magnetism varies but also the mechanical strength is insufficient.Furthermore, in the case of corrosion-resistant materials with 9 strength materials, there may be unevenness in corrosion resistance or variations in strength -L. There were many cases where this occurred.

本発明は従来方式のこれら欠点を除去し、アモルファス
材料を安定に熱処理できる新しい方法を提供するもので
ある。
The present invention eliminates these drawbacks of the conventional methods and provides a new method capable of stably heat treating amorphous materials.

すなわち、本発明は沸点が100℃より高い樹脂類を用
い、60°Cよりも高い温度に保持した中へ被熱処理体
を浸漬して行うことを特徴とするアモルファス材料の熱
処理法である。
That is, the present invention is a method for heat treatment of an amorphous material, which is characterized by using a resin having a boiling point higher than 100°C and immersing the object to be heat-treated in a resin maintained at a temperature higher than 60°C.

本発明によれば、従来磁性バラツキ、強度バラツギおよ
び耐蝕性上の不安定性等多々発生していた1〜ラブルも
ほとんど皆無に出来るものである。
According to the present invention, it is possible to almost completely eliminate the 1 to 1 to 1 rubs that have conventionally occurred frequently, such as magnetic variations, strength variations, and corrosion resistance instability.

本発明において、沸点が100 ’Cよりも高い樹脂類
を用いて熱処理する理由は、経験的に、このよ°うな樹
脂を用いた場合、とくにアモルファス材料における熱処
理後の耐蝕性安定性が良くなったからである。また、6
0℃よりも高い温度域での熱処理に限定したのは、同様
にしてそれよりも低い湿度域で熱処理した場合に、とく
に耐蝕安z性が悪くなり本発明の効果が出ない場合があ
るからである。
In the present invention, the reason why resins with a boiling point higher than 100'C are used for heat treatment is that when such resins are used, the corrosion resistance stability after heat treatment is improved, especially in amorphous materials. This is because the. Also, 6
The reason why heat treatment is limited to a temperature range higher than 0°C is because if heat treatment is similarly performed at a humidity range lower than 0°C, the corrosion resistance and stability may deteriorate and the effects of the present invention may not be achieved. It is.

以下に本発明を一゛εの実施例に基づいて説明する。The present invention will be explained below based on an embodiment of 1.epsilon.

実施例1 resiB系アモルファス材別を用い、250℃で11
1rの熱処理を施すに当り、本発明に基づいてそれそ′
れ磁性リング状わ1を10回づつ焼鈍を行ったところ、
同様にしてΔ1゛ガス雰囲気中で行ったものに比”<I
f性バラツキ、機械特性バラツキが第1表に示す如く著
しく少ない効果が得られた。
Example 1 11 at 250°C using resiB amorphous material
When performing heat treatment for 1r, it is based on the present invention.
When the magnetic ring shape 1 was annealed 10 times,
Similarly, compared to that conducted in a Δ1゛ gas atmosphere, “<I”
As shown in Table 1, the effect of significantly reducing variation in f properties and mechanical properties was obtained.

第1表 実施例2 CO[e M I)S I B系アモルファス材料にお
いて、120°Cにて磁性安定熱処理を2hr行うに当
り、本発明による方式どN2 ガス中にお【ノる熱処理
とを、イれぞれリング状試片等を用いて10回づつ行っ
たところ第2表に示す如く、磁性、耐蝕性が異り、本発
明の方式が優れていることが判明した。
Table 1 Example 2 When performing magnetic stability heat treatment at 120°C for 2 hours on a CO[e M I) S I B based amorphous material, the method according to the present invention was conducted in N2 gas. The tests were conducted 10 times using ring-shaped specimens, etc., respectively, and as shown in Table 2, the magnetism and corrosion resistance were different, and it was found that the method of the present invention was superior.

第2表 *耐蝕性は大気中暴露試験による錆発生の度数以上の実
施例から判るように、本発明はでの効果大きく、工業的
価値大きいものである。
Table 2 *Corrosion resistance: As can be seen from the examples showing the frequency of rust occurrence in the atmospheric exposure test, the present invention has great effects and is of great industrial value.

手続補正書(方式) %式% 発明の名称 熱6.方法 補正をする者 と、 相  +5os1F−l立金属株式会社代ノ・者
河野 兵火 代   理   人 居  i’17    東京都千代111区丸の内÷下
目1番2シツ?10 11−  の  文・j  象明
細書 補正の内容 明細書の浦41(内容に変更なし)
Procedural amendment (method) % formula % Title of invention Heat 6. The person who corrects the method, Ai +5os1F-l Ritsu Kinzoku Co., Ltd., Mr. Kono, Hyoukayo, Osamu, Hitori i'17 Marunouchi, 111-ku, Chiyo, Tokyo ÷ Lower 1st and 2nd Shitsu? 10 11- Sentence/j Ura 41 of the description of contents of the amendment to the description (no change in contents)

Claims (1)

【特許請求の範囲】[Claims] アモルファス材料を熱処理するに当り、沸点が100℃
よりも高い油脂類を用い、60℃Jス上の温度いしてイ
の中へ被熱処理体を浸漬して行うことを特徴とするアモ
ルファス材料の熱処理方法。
When heat treating amorphous materials, the boiling point is 100℃
1. A method for heat treatment of an amorphous material, characterized in that the heat treatment is carried out by immersing the object to be heat treated in a bath at a temperature of 60° C. or above using oils and fats higher than 60° C.
JP15101282A 1982-08-31 1982-08-31 Heat treatment method Pending JPS5941457A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP15101282A JPS5941457A (en) 1982-08-31 1982-08-31 Heat treatment method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP15101282A JPS5941457A (en) 1982-08-31 1982-08-31 Heat treatment method

Publications (1)

Publication Number Publication Date
JPS5941457A true JPS5941457A (en) 1984-03-07

Family

ID=15509362

Family Applications (1)

Application Number Title Priority Date Filing Date
JP15101282A Pending JPS5941457A (en) 1982-08-31 1982-08-31 Heat treatment method

Country Status (1)

Country Link
JP (1) JPS5941457A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4668309A (en) * 1986-06-09 1987-05-26 Allied Corporation Rapid magnetic annealing of amorphous metal in molten tin
US4877464A (en) * 1986-06-09 1989-10-31 Allied-Signal Inc. Rapid magnetic annealing of amorphous metal in molten tin

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4668309A (en) * 1986-06-09 1987-05-26 Allied Corporation Rapid magnetic annealing of amorphous metal in molten tin
US4877464A (en) * 1986-06-09 1989-10-31 Allied-Signal Inc. Rapid magnetic annealing of amorphous metal in molten tin

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