JPS5871876A - Production of capsules including fluid food inside - Google Patents
Production of capsules including fluid food insideInfo
- Publication number
- JPS5871876A JPS5871876A JP56168808A JP16880881A JPS5871876A JP S5871876 A JPS5871876 A JP S5871876A JP 56168808 A JP56168808 A JP 56168808A JP 16880881 A JP16880881 A JP 16880881A JP S5871876 A JPS5871876 A JP S5871876A
- Authority
- JP
- Japan
- Prior art keywords
- calcium
- film
- liquid
- balls
- food
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000013305 food Nutrition 0.000 title claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 239000002775 capsule Substances 0.000 title abstract description 22
- 239000012530 fluid Substances 0.000 title description 4
- 239000007788 liquid Substances 0.000 claims abstract description 27
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 9
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 7
- 239000000661 sodium alginate Substances 0.000 claims abstract description 7
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 7
- 235000010443 alginic acid Nutrition 0.000 claims abstract description 3
- 239000000783 alginic acid Substances 0.000 claims abstract description 3
- 229960001126 alginic acid Drugs 0.000 claims abstract description 3
- 229920000615 alginic acid Polymers 0.000 claims abstract description 3
- 150000004781 alginic acids Chemical class 0.000 claims abstract description 3
- 235000010410 calcium alginate Nutrition 0.000 claims abstract description 3
- 239000000648 calcium alginate Substances 0.000 claims abstract description 3
- 229960002681 calcium alginate Drugs 0.000 claims abstract description 3
- OKHHGHGGPDJQHR-YMOPUZKJSA-L calcium;(2s,3s,4s,5s,6r)-6-[(2r,3s,4r,5s,6r)-2-carboxy-6-[(2r,3s,4r,5s,6r)-2-carboxylato-4,5,6-trihydroxyoxan-3-yl]oxy-4,5-dihydroxyoxan-3-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylate Chemical compound [Ca+2].O[C@@H]1[C@H](O)[C@H](O)O[C@@H](C([O-])=O)[C@H]1O[C@H]1[C@@H](O)[C@@H](O)[C@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@H](O2)C([O-])=O)O)[C@H](C(O)=O)O1 OKHHGHGGPDJQHR-YMOPUZKJSA-L 0.000 claims abstract description 3
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910001424 calcium ion Inorganic materials 0.000 claims abstract 2
- 239000003795 chemical substances by application Substances 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000000499 gel Substances 0.000 abstract description 6
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 abstract description 4
- 239000001527 calcium lactate Substances 0.000 abstract description 4
- 229960002401 calcium lactate Drugs 0.000 abstract description 4
- 235000011086 calcium lactate Nutrition 0.000 abstract description 4
- 235000016213 coffee Nutrition 0.000 abstract description 4
- 235000013353 coffee beverage Nutrition 0.000 abstract description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 3
- 229960005069 calcium Drugs 0.000 abstract description 3
- 229910052791 calcium Inorganic materials 0.000 abstract description 3
- 239000011575 calcium Substances 0.000 abstract description 3
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 abstract description 3
- 239000001639 calcium acetate Substances 0.000 abstract description 3
- 235000011092 calcium acetate Nutrition 0.000 abstract description 3
- 229960005147 calcium acetate Drugs 0.000 abstract description 3
- 235000015110 jellies Nutrition 0.000 abstract description 3
- 239000008274 jelly Substances 0.000 abstract description 3
- 235000015203 fruit juice Nutrition 0.000 abstract description 2
- 239000011248 coating agent Substances 0.000 abstract 2
- 238000000576 coating method Methods 0.000 abstract 2
- 239000003921 oil Substances 0.000 description 13
- 235000019198 oils Nutrition 0.000 description 13
- 239000002994 raw material Substances 0.000 description 13
- 239000000243 solution Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
- 239000007787 solid Substances 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 244000269722 Thea sinensis Species 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 235000006468 Thea sinensis Nutrition 0.000 description 4
- 235000020279 black tea Nutrition 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 108010010803 Gelatin Proteins 0.000 description 3
- 238000007710 freezing Methods 0.000 description 3
- 230000008014 freezing Effects 0.000 description 3
- 239000008273 gelatin Substances 0.000 description 3
- 229920000159 gelatin Polymers 0.000 description 3
- 235000019322 gelatine Nutrition 0.000 description 3
- 235000011852 gelatine desserts Nutrition 0.000 description 3
- 229920001817 Agar Polymers 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 240000004584 Tamarindus indica Species 0.000 description 2
- 235000004298 Tamarindus indica Nutrition 0.000 description 2
- 239000008272 agar Substances 0.000 description 2
- 239000001110 calcium chloride Substances 0.000 description 2
- 229910001628 calcium chloride Inorganic materials 0.000 description 2
- 235000011148 calcium chloride Nutrition 0.000 description 2
- -1 fatty acid esters Chemical class 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 235000011962 puddings Nutrition 0.000 description 2
- 239000003549 soybean oil Substances 0.000 description 2
- 235000012424 soybean oil Nutrition 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- 229920006051 Capron® Polymers 0.000 description 1
- 241001137251 Corvidae Species 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- 235000010418 carrageenan Nutrition 0.000 description 1
- 239000000679 carrageenan Substances 0.000 description 1
- 229920001525 carrageenan Polymers 0.000 description 1
- 229940113118 carrageenan Drugs 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 108010025899 gelatin film Proteins 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000004804 polysaccharides Chemical class 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 235000020183 skimmed milk Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000013616 tea Nutrition 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/256—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from seaweeds, e.g. alginates, agar or carrageenan
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- General Preparation And Processing Of Foods (AREA)
- Seeds, Soups, And Other Foods (AREA)
- Jellies, Jams, And Syrups (AREA)
- Formation And Processing Of Food Products (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
Description
【発明の詳細な説明】
この発#4は、常温で液状または柔かいゲル状の少量の
町*物の表面を比較的硬いゲル状皮膜で被優した粒状カ
プセル食品の製造方法に関する。DETAILED DESCRIPTION OF THE INVENTION This issue #4 relates to a method for producing a granular capsule food in which the surface of a small amount of food that is liquid or soft gel at room temperature is coated with a relatively hard gel film.
七り−やプリンのような常温で柔かいゲル状物やジエー
ス、コーヒーのような常温で液ないしゾル状の可食物を
内蔵したカプセル体を製造する方法としては、これらの
可食物原料中に造膜剤であるアルギン酸ソーダー等を少
竜含有させたものをカルシウム塩水I@液中に滴下し、
可食物の表面にアルギン酸カルシウムのゲル状カプセル
皮膜を形成させ″る方法や上記と反対に、可食物原料中
和カルシウム塩を含有させておき、これをアルギン酸ソ
ーダの水溶液中に滴下してFjL膜を形成させる方法な
どが優案されている。A method for producing capsule bodies containing gel-like substances that are soft at room temperature, such as naniri and pudding, or edible substances that are liquid or sol at room temperature, such as coffee, is to Drop a membrane agent containing sodium alginate etc. into the calcium salt solution I@ solution,
In contrast to the above method, a gel-like capsule film of calcium alginate is formed on the surface of an edible material, and a neutralized calcium salt is added to the edible material, and this is dropped into an aqueous solution of sodium alginate to form an FjL film. Several methods have been proposed for forming the .
上記滴下法は、ゼラチン等を冷加して常温ではaIKよ
る成形粒状化が可能な1lfKまでゲル化した可食物原
料で4.これに7JI+1!して一旦は液状としてから
滴下するといり機案がされるはと一般的なものと考えら
れている、
しかしながら、このような滴下法では、M下する液状物
と!!1膜剤含有液の造膜剤液槽中の液の表闇における
可*物原料粒の小滴化、上記造膜剤液中での可食物原料
粒の変形、相互付着などの境象が生じやすく、低能率で
、完全な球状力′プ七一体の収率が低(、満足な工業的
生ilK遍するまでに至らない。The above-mentioned dropping method uses an edible raw material such as gelatin that has been cooled and gelatinized to 1lfK, which can be formed into granules by aIK at room temperature. 7JI+1 for this! It is generally considered that a method is used in which the material is first made into a liquid state and then dripped. ! 1. Situations such as the formation of small droplets of edible raw material particles in the surface of the liquid in the film-forming agent liquid tank of the film-forming agent-containing liquid, deformation of the edible raw material particles in the film-forming agent liquid, and mutual adhesion are observed. It is easy to produce, has low efficiency, and the yield of complete spherical force is low (and does not reach a satisfactory industrial production level).
そこで、滴下法についての公知文献は多いが。Therefore, there are many known documents regarding the dropping method.
この方法により製造された常温で液状ないし柔かいゲル
状の可食物を内蔵するカプセル食品は、いまだ市場にあ
られれていない。Capsule foods produced by this method that contain edible liquid or gelatin at room temperature have not yet appeared on the market.
本発明は、上記の点にかんがみ研究開発されたもので、
その目的は、液状ないし柔かいゲル状町貢物を内蔵する
粒状カプセル食品ケ、従来の原料液滴の滴下という方法
によることなく、迅速(収4よく量産できる簡単な方法
を提供するにある。The present invention has been researched and developed in view of the above points,
The purpose is to provide a simple method for mass-producing granular capsule foods containing liquid or soft gel-like food products quickly (with good yield) without using the conventional method of dropping droplets of raw materials.
上記目的を達成するための本発明方法の要旨は。The gist of the method of the present invention for achieving the above object is as follows.
符許膚求の範囲に記載のとおりであって、これを蒙する
に、′W;温で液状ないし柔かいゲル状の可食物原料(
可食性カルシウム塩をカルシウムとして1.0重量暢ま
で含有させたものを、0℃以下の凍結温fを有する油の
少(とも一種以上″Ikθ℃以下の温度に保持した油液
中に分散滴下し冷却することKよって、上記可食物の球
形冷凍固結物v4゜この冷凍固繕物を5℃以上の造膜剤
水溶液中に投入して、固結物にカプセル皮膜を形成させ
ることを特徴としている。It is as described in the scope of the application, and in accordance with this, 'W; edible raw material in the form of liquid or soft gel at temperature (
An edible calcium salt containing up to 1.0% by weight of calcium is dispersed and dropped into an oil solution maintained at a temperature of at least one type of oil having a freezing temperature f of 0°C or lower (Ikθ°C or lower). The above-mentioned edible spherical frozen congealed product v4 is then cooled.The frozen congealed product is poured into an aqueous film-forming agent solution at 5°C or higher to form a capsule film on the condensed product. It is said that
つまり1本発明は、造膜剤水溶液中に可食物原料を液状
で滴下するのではなく、油液中(おいて、今却凍結され
た球形の固体の形で投入し、カプセル皮膜を形成させ、
皮膜が完成したころには皮膜で被覆されたor食物原料
を当初の液状ないし柔かいゲル状にもどすといつ点に%
黴があり、これによって、!@削金含有液中のカプセル
皮膜形成工程1に容易で能率よ(、製品収率の大宮いも
の圧している。In other words, in the present invention, the edible raw material is not dropped in a liquid form into an aqueous solution of a film-forming agent, but is added in the form of a frozen spherical solid to an oil solution to form a capsule film. ,
By the time the film is completed, the food material covered with the film can be returned to its original liquid or soft gel state.
There is mold and this causes it! @Process 1 of forming a capsule film in a solution containing cutting metal is easy and efficient (and the product yield is superior to that of Omiya Imo).
以下本発明について詳細に説明する。The present invention will be explained in detail below.
説明中の鴫は、すべて重量憾である。All of the crows being explained are heavy.
可食物原料は、多量の水分を含むもので、果汁。Edible raw materials contain a large amount of water, such as fruit juice.
紅茶、コーヒー、コーラ飲料などのほか、プリンやゼリ
ーのような柔かいゲル状のもので0℃ないし一5℃の範
囲で固結するものであれば何でもよい。これらは、or
賞物として適当な原料成分のほかに、乳酸カルシウム、
酢酸カルシウム、燐酸lカルシウム、塩化カルシウムな
どの可溶可食性カルシウム塩をカルシウムにして1.0
重量係までの通′ビの量添加してお(。できるだけ分子
責の大きいカルシウム塩が優の冷凍凝固工程を短かくす
るため好ましい。In addition to tea, coffee, and cola drinks, any soft gel-like substance such as pudding or jelly that solidifies in the range of 0°C to -5°C may be used. These are or
In addition to raw materials suitable for prizes, calcium lactate,
Soluble edible calcium salts such as calcium acetate, calcium phosphate, and calcium chloride are converted to calcium with a concentration of 1.0
Add the amount of sodium chloride up to the weight limit (. Calcium salts with as large a molecular weight as possible are preferred in order to shorten the freezing and coagulation process.
液状の可食物Ifj科を冷却同化するため和は一5℃で
凝固するリノール酸から一71℃で凝固するカブロン酸
メチルなどの脂肪酸エステルまでを含む谷檀の天然油お
よび精油を用いることができるが。In order to cool and assimilate liquid edible Ifj, natural oils and essential oils of Tanidan, including linoleic acid, which solidifies at 15°C, to fatty acid esters such as methyl cabronate, which solidifies at 171°C, can be used. but.
るアff二m、 同一8℃〜−2] Cの間にあるダイ
ズ油、同−I℃付近にある落花生油などが適当である。Suitable are soybean oil, which is between 8°C and -2°C, and peanut oil, which is around -1°C.
液状可食物原料にゼリー化剤を添刀口して、柔かいゲル
状にしたものを用い、その冷却固化する諷度が0℃tM
iえる場合には、0℃ないし一5℃で凝固するオリーブ
油やサラダ油を用いることもで律る。これらの油液は、
司貢物原#+を冷却して固化することができる程度の低
温に保持しておくこと1に!!する。A gelatinizing agent is added to the liquid edible raw material to form a soft gel, and the degree of solidification on cooling is 0°CtM.
If possible, use olive oil or salad oil that solidifies at 0°C to -5°C. These oils are
1. Keep the Sagibutsuhara #+ at a low temperature that allows it to cool and solidify! ! do.
可食物原料を冷却した油液の槽中和滴下するには、従来
滴下法用として知られている装置方法その他遍宜の装置
方法な選択採用すればよい。油液中への滴下、攪拌によ
って粒径2〜8絽程度の球形固結物を容易に得ることが
できる。To neutralize and drip the edible raw material into a tank of cooled oil, any device or method conventionally known for the dropping method or any other suitable device may be used. Spherical solids with a particle size of about 2 to 8 squares can be easily obtained by dropping the mixture into an oil solution and stirring.
この球形の固結物を造膜剤液と接舷させる(は。This spherical solidified material is brought into contact with the film-forming agent solution (ha.
通常の手段による投入で足りる。Input through normal means is sufficient.
41膜剤液中のアルギン散ソーダの製置は、0.5〜1
.5重量憾位がよいが、これに限定されない。41 The concentration of alginous soda in the membrane agent solution is 0.5 to 1
.. 5 weight is preferable, but is not limited to this.
造膜剤液中には、カプセル皮膜強化のため熱や酸で凝固
する蛋白類の#青か、カプセル皮膜の食感性向上のため
多糖類等適宜の成分ケ添加できる。!膜剤液の温度は、
常温から5℃までの間で選択するの
町*物原料の球形固結物は、造膜剤液中圧入ると、直ち
に表面から凝固が解は始め、含有されている遊−鳴ルシ
ウムイオンとf1膜剤販中のアルギン酸とが反応してカ
プセル皮膜が形成されてい(。Appropriate components such as proteins coagulated by heat or acid to strengthen the capsule film or polysaccharides to improve the texture of the capsule film can be added to the film forming agent solution. ! The temperature of the membrane agent solution is
When the spherical solidified material is selected between room temperature and 5℃, when it enters the pressure of the film-forming agent solution, it immediately begins to uncoagulate from the surface, and the free lucium ions contained therein begin to dissolve. The capsule film is formed by reacting with the alginic acid available in the f1 film formulation (.
その間球形固結物を4膜剤液中で常時攪拌しつつ。During this time, the spherical solids were constantly stirred in the 4-film agent solution.
順次移動させるのがよい1時間の経過とともに。It is best to move them sequentially over the course of an hour.
反応が進みカプセル皮膜厚が増大するが、これとともに
球形固結物の内部に解凝が徐々に進行する。As the reaction progresses, the capsule film thickness increases, but at the same time, deagglomeration gradually progresses inside the spherical solids.
その結果、可食物が液化し、その表面張力とm膜fi+
液中での運動によるMl俤で1粒形は球状化してい(。As a result, the edible material liquefies and its surface tension and m membrane fi+
Due to the movement of Ml in the liquid, the grain shape becomes spherical (.
概ね2〜5分を経過すると、カプセル皮膜は所望の強度
となる。これを増出して水洗し、必豊かあれは再度カル
シウム塩含有液に接触させて製品とする・
以下本発明を実施例に即して説明する。After about 2 to 5 minutes, the capsule film has the desired strength. The amount is increased and washed with water, and if necessary, it is brought into contact with a calcium salt-containing solution again to produce a product.The present invention will be explained below with reference to Examples.
実施例1
紅茶K O,9%の乳酸カルシウムのはか0.5優のフ
ァーモレ9フ、1畳のクエン酸およびtlp糖v加えB
x 6.2に調製した可食物原料vZIo熱殺劇しこの
0T食物原料液を予め1〜5℃に冷却してから。Example 1 Black tea K O, 9% calcium lactate, 0.5 ml of Farmole 9f, 1 tatami of citric acid and tlp sugar v added B
After heat killing the edible raw material vZIo prepared at
−加℃〜−切℃のカプロン絨メチル油中に滴下する1滴
下液量は径81uの球形カプセル体が形成可能なtKす
る。M下された液は油液の槽中で緩やかに攪拌V続ける
。(資)〜ω分経過すると紅茶は凍結して径gmの球形
冷凍固結物となる・これを油液槽から液出して−1[1
0℃の1.5僑アルギン酸ソーダ水浴液槽中に投入し、
5分間攪拌しつつ槽中に維持する。七〇fiJuζ、球
形に冷凍された可食物は解凍を進めつつ、tk狛の遊離
したカルシウムイオンが造g削液中のアルギン酸と反応
して力1セル皮、y1が形成され、町冑物内蔵球形カプ
セル食品となる。この内観食品を4勧化するには、さら
に0.2係のクエン酸と1憾の塩化カルシウムを含有さ
せた液で加熱する。これを流出させ。The amount of liquid dropped into Capron's methyl oil at temperatures ranging from -0.degree. The removed liquid is gently stirred in the oil tank. (Capital) After ~ω minutes, the black tea freezes and becomes a spherical frozen solid with a diameter gm. This is drained from the oil tank and -1[1
Pour 1.5 liters of sodium alginate into a water bath at 0°C,
Maintain in bath with stirring for 5 minutes. 70 fi Ju It becomes a spherical capsule food. To make this naikan food into 4 parts, it is further heated in a liquid containing 0.2 parts of citric acid and 1 part of calcium chloride. Let this flow out.
水洗して製品とする。4られた製品の内蔵可食物である
紅茶は液状ないしゼリー状をしており、カプセル皮膜の
強度も十分で大感性も丁ぐれている。Wash with water and use as a product. Black tea, which is a built-in edible product, is in the form of liquid or jelly, and the capsule film has sufficient strength and sensitivity.
実施例2
3011のゼラチン、13jlのタマリンド% 13O
Nのfllllj、310)寒天、5#のクエン酸、オ
レンジエツセンス少量、15Iの乳酸カルシウムに市販
の10憾オレンジジエースな添加溶解して100[1の
流動物1に4、減圧下で脱気してから、加熱膜−して常
温に冷却し柔かいゼリー状の可食物原料とする。Example 2 3011 gelatin, 13jl tamarind% 13O
N flllllj, 310) agar, 5 # citric acid, a small amount of orange essence, 15 I calcium lactate, add commercially available 10 orange extract, dissolve and dissolve in 100 [1 fluid 1:4] under reduced pressure. After drying, the mixture is heated and cooled to room temperature to form a soft jelly-like edible material.
これを凍結a度−21℃のダイズ油を−14℃に保つ1
こ槽中和滴下して5〜10分間攪拌してから取出しオレ
ンジジエースの球形#固体!得た。これを実施例IK述
べたと同様の造膜剤液中で同様に処理して1球形で径約
4〜5謹楊匿の粒状町食智内戚カプセル体食品を得た。This freezes soybean oil at -21°C and keeps it at -14°C1
Neutralize this tank, add it dropwise, stir for 5 to 10 minutes, and then take it out to form a spherical #solid orange ace! Obtained. This was treated in the same film-forming agent solution as described in Example IK to obtain a granular capsule food with a spherical shape and a diameter of about 4 to 5 mm.
このカプセルに内域されたジエースは凝固が解けて柔か
いゾル状となっており、カプセル皮膜tMfも十分で食
感性もよく、密封缶入り紅茶中に添加して用いることが
できる。The ACE contained in this capsule is uncoagulated and becomes a soft sol, and the capsule film tMf is sufficient and the texture is good, so it can be added to black tea in a sealed can.
実施例3
タマリンド13 i、カラギーナン51寒天2I初末脱
脂乳509.砂糖鉛1.酢酸カルシウムillに水″I
!を加えて100ONの流動物を得、脱気して可食qy
lJ原料とし、これy−27℃で凍結するアマニ油の一
14℃に保持された油液槽中に、滴下する。10−加分
間攪拌すると滴下された流曹体は径約7−の球形冷凍固
結物となる。これを取出して、i、o優のアルギン酸ソ
ーダと0.116のデンプンを加えた造ga中に投入し
、以優実厖例1のとおり処理して製品とする。得られた
カプセル賞品の内蔵液はコロイド状で1粒は球形であり
1缶入りコーヒーに添7Xlするものとして好適である
。Example 3 Tamarind 13i, carrageenan 51 agar 2I primary skim milk 509. Sugar lead 1. Calcium acetate ill water''I
! was added to obtain a 100ON fluid, which was degassed to give an edible qy
The raw material is linseed oil, which is frozen at -27°C, and is dropped into an oil bath maintained at 14°C. After stirring for 10 minutes, the dropped fluid becomes a spherical frozen solid having a diameter of about 7 mm. The product is taken out and put into a gelatinizer containing 1,00% sodium alginate and 0.116% starch, and processed as in Example 1 to obtain a product. The liquid contained in the obtained capsule prize is colloidal and each capsule is spherical, making it suitable for adding 7Xl to a can of coffee.
以上本発明の実施例数例について説明したが、本発明の
実mに当っては、上記実施例に限定されるものではなく
、特許請求の範囲の要件をみた丁限りで他の方法な用い
ることができる。Although several embodiments of the present invention have been described above, the actual implementation of the present invention is not limited to the above embodiments, and other methods may be used as long as the requirements of the claims are met. be able to.
本発明は、可食物原料をftm性のある状輯で造膜剤液
中に滴下するのではなく、固形物として投入するという
思春忙立脚しているが、と(K、多駿の水分1含む可食
物の組成にy#眼して、これを通常の冷蔵庫の冷?j[
m度程度の温度の油液中で凍結ないし凝固し1球形の固
結物とするので、冷凍に多少時間を4J!するけれど4
.可食物原料を超低温の液体中で凍結固化するのに比較
すると、装置に費用veせず、操作が簡単で特別の配m
v要することな(操業することができる。The present invention is based on the idea that the edible raw material is not dropped into the film-forming agent liquid in a state with ftm properties, but is added as a solid substance. Considering the composition of the edible food it contains, I put it in a normal refrigerator.
It freezes or solidifies in an oil liquid at a temperature of about m degrees and becomes a spherical solid, so it takes about 4J to freeze! I do but 4
.. Compared to freezing and solidifying edible ingredients in ultra-cold liquids, equipment costs less, are easier to operate, and require special arrangements.
v It is not necessary (it can be operated).
Claims (1)
にカルタδ五にして1.0重量部までの町m町食性カル
シウム塩な含有させた原%を、0℃することによって、
球状の冷凍固結智な得1次いで、この球状凍結11Fv
、 0.2〜2.0係までのアルギン酸ソーダを含有す
る5℃〜m℃の造膜剤水溶液中−投入攪拌して1球状凍
結智中のカルシウムイオンと造膜剤水溶液中のアルギン
酸との反応により1球状町食物の表面にアルギン酸カル
シウムを抱含するゲル状皮mt’形成させることV%做
とするfLWIJ食品内蔵球形カグ七ル食品の製造方法
。By containing up to 1.0 parts by weight of edible calcium salt in an edible liquid or gel that is soft and easily deformable at room temperature at 0°C,
Then, this spherical frozen 11Fv
, into a film-forming agent aqueous solution at 5°C to m°C containing sodium alginate with a concentration of 0.2 to 2.0, and stirring to combine the calcium ions in the spherical frozen particles with the alginic acid in the film-forming agent aqueous solution. A method for producing a spherical food containing fLWIJ food, which comprises forming a gel-like skin mt' containing calcium alginate on the surface of the spherical food by reaction.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56168808A JPS5871876A (en) | 1981-10-23 | 1981-10-23 | Production of capsules including fluid food inside |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56168808A JPS5871876A (en) | 1981-10-23 | 1981-10-23 | Production of capsules including fluid food inside |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5871876A true JPS5871876A (en) | 1983-04-28 |
JPS6129700B2 JPS6129700B2 (en) | 1986-07-08 |
Family
ID=15874870
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP56168808A Granted JPS5871876A (en) | 1981-10-23 | 1981-10-23 | Production of capsules including fluid food inside |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5871876A (en) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS63192352A (en) * | 1987-02-03 | 1988-08-09 | Nissin Food Prod Co Ltd | Production of fluid food of capsule type |
JPH04222562A (en) * | 1990-12-21 | 1992-08-12 | Ezaki Glico Co Ltd | Production of edible capsule |
WO2002071867A1 (en) * | 2001-03-08 | 2002-09-19 | Cargill Incorporated | Foodstuff for and method of feeding aquatic life |
JP2009165430A (en) * | 2008-01-18 | 2009-07-30 | Suntory Holdings Ltd | Jelly-containing beverage |
US7947305B2 (en) * | 2005-08-19 | 2011-05-24 | Riken Vitamin Co., Ltd. | Fat-soluble drug composition |
JP2013520203A (en) * | 2010-02-22 | 2013-06-06 | ル ラボグループ ソシエテ パール アクシオン サンプリフィエ | Contain materials in natural transportation systems |
CN103271424A (en) * | 2013-05-28 | 2013-09-04 | 上海交通大学 | Preparing method of fragrant microcapsule |
JP2019135945A (en) * | 2018-02-07 | 2019-08-22 | キユーピー株式会社 | Frozen spherical food and frozen spherical food production method |
JP2022504925A (en) * | 2018-10-29 | 2022-01-13 | ザ プロクター アンド ギャンブル カンパニー | Method for preparing the enclosed liquid composition |
-
1981
- 1981-10-23 JP JP56168808A patent/JPS5871876A/en active Granted
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS63192352A (en) * | 1987-02-03 | 1988-08-09 | Nissin Food Prod Co Ltd | Production of fluid food of capsule type |
JPH0441577B2 (en) * | 1987-02-03 | 1992-07-08 | Nissin Food Products Ltd | |
JPH04222562A (en) * | 1990-12-21 | 1992-08-12 | Ezaki Glico Co Ltd | Production of edible capsule |
WO2002071867A1 (en) * | 2001-03-08 | 2002-09-19 | Cargill Incorporated | Foodstuff for and method of feeding aquatic life |
US7947305B2 (en) * | 2005-08-19 | 2011-05-24 | Riken Vitamin Co., Ltd. | Fat-soluble drug composition |
JP2009165430A (en) * | 2008-01-18 | 2009-07-30 | Suntory Holdings Ltd | Jelly-containing beverage |
JP2013520203A (en) * | 2010-02-22 | 2013-06-06 | ル ラボグループ ソシエテ パール アクシオン サンプリフィエ | Contain materials in natural transportation systems |
JP2016104012A (en) * | 2010-02-22 | 2016-06-09 | ラブストアLabstore | Sealing of material to natural transport system |
US9795990B2 (en) | 2010-02-22 | 2017-10-24 | Incredible Foods, Inc. | Enclosing materials in natural transport systems |
CN103271424A (en) * | 2013-05-28 | 2013-09-04 | 上海交通大学 | Preparing method of fragrant microcapsule |
JP2019135945A (en) * | 2018-02-07 | 2019-08-22 | キユーピー株式会社 | Frozen spherical food and frozen spherical food production method |
JP2022504925A (en) * | 2018-10-29 | 2022-01-13 | ザ プロクター アンド ギャンブル カンパニー | Method for preparing the enclosed liquid composition |
Also Published As
Publication number | Publication date |
---|---|
JPS6129700B2 (en) | 1986-07-08 |
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