JPS5829648A - Inorganic fiber board and its manufacture - Google Patents

Inorganic fiber board and its manufacture

Info

Publication number
JPS5829648A
JPS5829648A JP12806081A JP12806081A JPS5829648A JP S5829648 A JPS5829648 A JP S5829648A JP 12806081 A JP12806081 A JP 12806081A JP 12806081 A JP12806081 A JP 12806081A JP S5829648 A JPS5829648 A JP S5829648A
Authority
JP
Japan
Prior art keywords
magnesium oxide
fibers
inorganic fiber
wool
mixed water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP12806081A
Other languages
Japanese (ja)
Inventor
Yoshihiro Yonemoto
米本 佳弘
Fujio Yamada
山田 冨士夫
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Sumitomo Metal Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Metal Industries Ltd filed Critical Sumitomo Metal Industries Ltd
Priority to JP12806081A priority Critical patent/JPS5829648A/en
Publication of JPS5829648A publication Critical patent/JPS5829648A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/10Lime cements or magnesium oxide cements
    • C04B28/105Magnesium oxide or magnesium carbonate cements

Abstract

PURPOSE:To obtain an inorganic fiber board having excellent fire proofness and excellent heat insulation property by a method in which a magnesium oxide mixed water is adhered to an inorganic fiber in static state while molding it into a plate form in such a way that the magnesium oxide is hardened and the fibers are bonded with one another without breaking the fibers. CONSTITUTION:For example, slug wool 1 oriented sidewards is set between metal nets 3 in a dipping tank 2 flled with a magnesium oxide mixed water 4 being circulated through a circulation pipe 5 with an opening at the bottom of the tank, a compounding tank 6, and a supply pipe 7. The slug wool 1 is brought into contact with the magnesium oxide mixed water 4 flowing, during which magnesium oxide in the mixed water 4 is adhered to the suface of the slug wool 1. Afterwards, the slug wool 1 is taken out and sent to a hot press molding machine for molding, where the magnesium oxide is hardened to bond the fibers of the slug wool 1 together. Thus, an objective inorganic fiber board can be obtained. EFFECT:Heat proofness and water resistance are excellent.

Description

【発明の詳細な説明】 この発明は無機質縁H,<1:ボード、すなわち岩綿、
製鉄時発生するスラグウールあるいはグラスウール等の
ボードおよびその製造法に関する。
DETAILED DESCRIPTION OF THE INVENTION This invention provides mineral edge H, <1: board, i.e., rock wool;
This article relates to boards made of slag wool or glass wool generated during steel manufacturing, and their manufacturing method.

その目的は、耐火、耐熱、耐水性が優れ、しかも断熱性
が高いボードを提案するにある。
The aim is to propose a board with excellent fire resistance, heat resistance, water resistance, and high heat insulation properties.

従来の無機質繊維ボード類は合成樹脂系あるいは澱粉系
等の接着剤をバインダーとして繊維間を結着し、同時に
板状に成形してなったものである。従って無機質繊組ケ
」、不燃であるが、バインダーが可燃性であるのでl1
火性が低Fする欠点があった。9また、澱゛粉系等のバ
インダーを用いた場合には耐水性も著しく低下した。丑
だ、ボードを製造するに当って、従来のバインダーは通
常粘度が1高いので、繊組゛間にバインダーを均一に含
浸させるためにに1:、繊維を攪拌する必要があり、こ
の・歴拌時にMl: fatが折れ細かいナリ状となシ
飛散して作隘環境が悪化し珪肺舌の原因ともなっている
1、 この発明は」−諸問題点に着II してなされたもので
、その要旨は無機質繊維がm互に、酸化マグネシウムを
バインダーとし結着していることを特徴とする無機質縁
、?f1ボードである3゜このボードは酸化マグネシラ
ノ・の(]ψ化物に」二り結着しているので、着火、燃
焼f1がなく、酸化マグネ/ラムの融点iJ: 280
0 ”C; Jソ上であり極めて旨い耐熱性をイJする
。、捷だ、、 +iil水1/1が];’F+く長時間
水中に浸漬してもバインダーが解体することはない。そ
して、結着してなった繊維間(寸多数の微#Iな解重空
気層を形成するので高い断熱性能をイ」与することがで
きる。
Conventional inorganic fiber boards are made by binding fibers together using a synthetic resin or starch adhesive as a binder, and at the same time forming them into a plate shape. Therefore, inorganic fibers are nonflammable, but since the binder is flammable, l1
It had the disadvantage of low flammability. 9 Furthermore, when a starch-based binder or the like was used, the water resistance was also significantly reduced. Unfortunately, when manufacturing boards, conventional binders usually have a high viscosity, so it is necessary to stir the fibers in order to uniformly impregnate the binder between the fibers. During stirring, the Ml: fat breaks off and scatters in small, nug-like shapes, deteriorating the cropping environment and causing silicosis. The gist is that an inorganic edge is characterized by inorganic fibers bound together using magnesium oxide as a binder. 3゜ which is an f1 board. Since this board is bonded to the (]ψ compound of magnesyrano oxide, there is no ignition or combustion f1, and the melting point of magne oxide / ram iJ: 280
0 ``C; It has excellent heat resistance and has excellent heat resistance.The binder does not disintegrate even if it is immersed in water for a long time. Since a large number of microscopic deagglomerated air layers are formed between the bound fibers, high heat insulation performance can be imparted.

このボードに用いる無機質繊維としては、岩綿、スラグ
ウール、グラスウール、炭素d1.ME等であり、岩綿
、グラスウールは耐熱性が高く酸化マグネシウムをバイ
ンダーとした場合極めて耐熱性が高いボードとすること
ができ、しかも低コストで好適である。酸化マグネシウ
ムは高純度、?a細粒子のものが好丑しいが、必ずしも
これに限定されるものではない。
Inorganic fibers used for this board include rock wool, slag wool, glass wool, carbon d1. Rock wool and glass wool have high heat resistance, and when magnesium oxide is used as a binder, it is possible to make a board with extremely high heat resistance, and it is suitable at low cost. Is magnesium oxide highly pure? A fine particles are preferable, but are not necessarily limited to this.

この無機質繊維ボードは結着した繊維間に微細な空気層
を有する多孔質構造であり、酸化マグネシウムバインダ
ー量、圧縮成形条件等により様々な空隙率、嵩密度とす
ることができる。
This inorganic fiber board has a porous structure with fine air layers between bound fibers, and can have various porosity and bulk density depending on the amount of magnesium oxide binder, compression molding conditions, etc.

高断熱性と実用強度を有するボードとするためには通常
嵩密度は600〜700 K47m”であり、5ooK
9/m”程度が好適である。
In order to make a board with high heat insulation properties and practical strength, the bulk density is usually 600 to 700K47m", and 5ooK
Approximately 9/m'' is suitable.

1ソ、下にこの無機質繊維ボードの製造法について図面
を1月い説明する。
Below, we will explain the manufacturing method of this inorganic fiber board with drawings.

第1図において略2次元的(+、17−カ向)に配向し
たスラグウール1を浸/11t槽2内企網3 、 :1
間に配置する1、浸ムIt槽2に酸化マグネ/ラム混合
水4を満たし−Cおき、この/lI′、合水4を4I1
11i底に開口する循環パイプ5.調合タンク(i 、
 イil、給・ぐイブ7を経て循環する6、グラスウー
ル+ (d’、 Mr、動する混合水4に接触し、混合
水/1中の酸比マグネシウムはグラスウール1表面に伺
オ”1する1、伺着量が適量となった時点で、スラグウ
ール1を取出し、次の加熱成形装置に移ず1.庁j、・
、第1図で8はバルブ、9はポンプ、10は酸化マグネ
/ラム原料タンクである1゜ 第2図の加熱成形装置IIにおいて、グラスウール1を
型枠12内に収納1〜、子方からジヤツキ13により昇
降する加、[[板14により圧定jIIめ−に胛圧し、
同時に型枠12内に加11水蒸気を吹込み高温高圧水蒸
気養生を行なう1.グラスウール1に付着した酸化マグ
ネンウj、0]硬化し、スラグウール1の・11」互繊
紺間は結着し板状fイ・に成形される。
In FIG. 1, slag wool 1 oriented approximately two-dimensionally (+, 17- directions) is immersed/11t tank 2 internal network 3:1
Fill the immersion tank 2 with magnesium oxide/ram mixed water 4 placed between -C, add this /lI' and the combined water 4 to 4I1
5. Circulation pipe opening at the bottom of 11i. Preparation tank (i,
6.Glass wool + (d', Mr.), which circulates through the supply pipe 7, contacts the moving mixed water 4, and the acid ratio magnesium in the mixed water/1 reaches the surface of the glass wool 1. 1. When the amount of slag wool reaches the appropriate amount, take out the slag wool 1 and do not move it to the next heat forming device.
In FIG. 1, 8 is a valve, 9 is a pump, and 10 is a magneto oxide/lamb raw material tank 1. In the thermoforming apparatus II shown in FIG. While being raised and lowered by the jack 13, the plate 14 presses to the desired position,
At the same time, additional steam is blown into the formwork 12 to perform high-temperature, high-pressure steam curing.1. The magnesium oxide adhering to the glass wool 1 is cured, and the 11" interlocking fibers of the slag wool 1 are bonded together and formed into a plate-like shape.

この製造法において、酸化マグネシウム混合水は酸fヒ
マグネシウム20〜30、水60〜90重量比の懸濁液
であって、流動性が良好であり、スラグウール間をよく
流れて循環し、静止状態にあるスラグウールに酸化マグ
ネシウムは均一に付着する。件だ、遊山((水分は容易
に分離され加熱成形によりボードとすることができる。
In this production method, the magnesium oxide mixed water is a suspension with a weight ratio of 20 to 30 percent magnesium oxide and 60 to 90 water, and has good fluidity, flows well between the slag wool, circulates, and stands still. Magnesium oxide adheres uniformly to the slag wool in this state. However, the moisture can be easily separated and it can be made into a board by heat molding.

従って製造の能率が高く、スラグウールを攪拌しないの
で、スラグウール細片が飛散することもなく製造の環境
が良好である。
Therefore, production efficiency is high, and since the slag wool is not stirred, the production environment is favorable without scattering of slag wool pieces.

水分を含んだ酸化マグネシウムは空気中で常温でも硬化
し繊維相互を結着してボードを形成することができる。
Magnesium oxide containing moisture can harden in the air at room temperature and bind fibers together to form a board.

しかし、短時間に強度を発現しボードとするためには、
加熱養生することが実際的であることは云うまでもない
。壕だ、このボードは表層部に酸化マグネシウム水のベ
ースト秋物等を塗着1〜で緻密な表皮層を形成し、内部
空隙を閉塞することもなる。このボードは流体を透過し
ないので耐火、耐熱、耐水性および断熱性が一層向士す
る1J 〔実施例〕 第1図、第2図の装置を用い、水21 K7に高純度、
微粒子酸化マグネシウム8.4 K7を混合した混合水
に、38.581(7のグラスウールを静置浸漬し、混
合水を循環移動して酸化マダイ、ンウムをスラグウール
表面に伺*’t 4−rしめた1、このスラグウールを
加熱成形装置1′1°C(移し、IOKり/(〃Iの飽
和水蒸気で養生し厚さ13 mm、  I O(フn×
90確のボード10枚をイqた。−、ボート1″l’+
i密度は略05Ky/儂3であった。
However, in order to develop strength in a short period of time and create a board,
Needless to say, heat curing is practical. Well, this board is coated with magnesium oxide water baset etc. on the surface layer to form a dense skin layer and close the internal voids. Since this board is impermeable to fluids, its fire resistance, heat resistance, water resistance, and heat insulation properties are further improved.
The glass wool of 38.581 (7) was immersed in the water mixed with fine particles of magnesium oxide 8.4 K7, and the mixed water was circulated to collect oxidized red sea bream and barley on the surface of the slag wool *'t 4-r 1. Transfer the slag wool to a heating molding device at 1'1°C and cure it with saturated steam to a thickness of 13 mm.
I got 10 boards with 90 accuracy. −, boat 1″l’+
The i-density was approximately 0.5 Ky/min.

このボードの性能は次の如くであつ/こ、。The performance of this board is as follows.

耐熱性:プロパンガスバーナー直1・850〜900”
cで一時間炎焼した結果、炎面多少変色するも形崩れな
し、裏面11゛・1常なし。
Heat resistance: Propane gas burner straight 1/850-900”
As a result of flame-grilling at c for one hour, the flame surface was slightly discolored but the shape remained intact, and the back side was 11゛.

吸湿性:室内放置で重:1;−変化なし3、耐水性:静
置水中浸漬24時間後、および振動水中浸漬5時間後、
τ]法変化なく、遊離水分を振切った状態で重U1;増
加d、認められなかった1゜ この発明は以上の通りであり、このボードは耐火、面1
熱、耐水性が優れ、しかも断熱性を備えている。また、
この製造法は能率よく作業環境を損なうことがない。
Hygroscopicity: Heavy when left indoors: 1; - No change 3; Water resistance: After 24 hours of immersion in static water and 5 hours of immersion in shaking water.
τ] No change in method, weight U1 after shaking off free moisture; increase d, not observed 1° This invention is as described above, and this board is fireproof, surface 1
It has excellent heat and water resistance, as well as insulation properties. Also,
This manufacturing method is efficient and does not harm the working environment.

【図面の簡単な説明】[Brief explanation of the drawing]

図面はこの発明のボードの製造過程を示すもので、第1
図は浸漬槽で酸化マグネシウムを付着せしめる工程の概
要を示す縦断面図、第2図−ニ加熱成形工程の概要を示
す縦断面図である。 1・・・・・スラグウール、2・・・・・・浸漬層、3
・・・・金網、イ・・・・・・酸化マグネシウム混合水
、5・・・・・循J)7パイプ、6・・・・・・調合タ
ンク、7・・・・・・供給パイプ、8・・・・・・バル
ブ、9・・・・・・ポンプ、10・・・・原オ′:1タ
ンク、11・・・・・・加熱成形装置、12・・・・・
型枠、13・・・・・・ジャツギ、14・・・・・加圧
板。 特許出願人  住友金属工業株式会社 (7) 第1図 第2図 283
The drawings show the manufacturing process of the board of this invention.
The figures are a vertical cross-sectional view showing an overview of the process of depositing magnesium oxide in a dipping tank, and a vertical cross-sectional view showing an overview of the heat forming process in FIG. 1... Slag wool, 2... Soaked layer, 3
... Wire mesh, A ... Magnesium oxide mixed water, 5 ... Circulation J) 7 pipe, 6 ... Mixing tank, 7 ... Supply pipe, 8... Valve, 9... Pump, 10... Geno': 1 tank, 11... Heat forming device, 12...
Formwork, 13... Jatsugi, 14... Pressure plate. Patent applicant: Sumitomo Metal Industries, Ltd. (7) Figure 1 Figure 2 283

Claims (2)

【特許請求の範囲】[Claims] (1)  無機質繊維が相互に酸化マグネシウムをバイ
ンダーとして結着してなったことを特徴とする無機質繊
維ボード。
(1) An inorganic fiber board characterized by inorganic fibers bound together using magnesium oxide as a binder.
(2)  解重状態の無機質繊維に酸化マグネシウム4
L合水を移動して接触させ、無機質繊維表面に酸化マグ
ネシウムを付着せしめ、板状に成形すると同時に付着し
た酸化マグネシウムを硬化して繊維相互間を結着するこ
とを特徴とする無機質繊維ボードの製造法。
(2) Magnesium oxide 4 in deweighted inorganic fibers
An inorganic fiber board characterized by moving and contacting L-water, adhering magnesium oxide to the surface of the inorganic fibers, forming it into a plate shape, and at the same time hardening the adhering magnesium oxide to bond the fibers together. Manufacturing method.
JP12806081A 1981-08-15 1981-08-15 Inorganic fiber board and its manufacture Pending JPS5829648A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP12806081A JPS5829648A (en) 1981-08-15 1981-08-15 Inorganic fiber board and its manufacture

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP12806081A JPS5829648A (en) 1981-08-15 1981-08-15 Inorganic fiber board and its manufacture

Publications (1)

Publication Number Publication Date
JPS5829648A true JPS5829648A (en) 1983-02-21

Family

ID=14975479

Family Applications (1)

Application Number Title Priority Date Filing Date
JP12806081A Pending JPS5829648A (en) 1981-08-15 1981-08-15 Inorganic fiber board and its manufacture

Country Status (1)

Country Link
JP (1) JPS5829648A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0473246A (en) * 1990-07-10 1992-03-09 Home Insaru Kk Inorganic fiber board having depressed hole in flat surface portion thereof and production thereof
US7255907B2 (en) 2005-01-31 2007-08-14 Michael E. Feigin Magnesium oxide-based construction board

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0473246A (en) * 1990-07-10 1992-03-09 Home Insaru Kk Inorganic fiber board having depressed hole in flat surface portion thereof and production thereof
US7255907B2 (en) 2005-01-31 2007-08-14 Michael E. Feigin Magnesium oxide-based construction board
US7867597B2 (en) 2005-01-31 2011-01-11 Jet Products, Llc Construction board with carbonate
US7998547B2 (en) 2005-01-31 2011-08-16 Jet Products, Llc Magnesium oxide-based construction board

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