JPS58167947A - Spinner of nuclear magnetic resonance device - Google Patents

Spinner of nuclear magnetic resonance device

Info

Publication number
JPS58167947A
JPS58167947A JP57049071A JP4907182A JPS58167947A JP S58167947 A JPS58167947 A JP S58167947A JP 57049071 A JP57049071 A JP 57049071A JP 4907182 A JP4907182 A JP 4907182A JP S58167947 A JPS58167947 A JP S58167947A
Authority
JP
Japan
Prior art keywords
ceramics
spinner
spectrum
caused
glass ceramics
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP57049071A
Other languages
Japanese (ja)
Inventor
Susumu Tsujiku
Yasuo Hiyoshi
Ataru Yokono
Masao Goto
Shinichi Uematsu
Masahiro Hatano
Yasunori Nozawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Ltd
Original Assignee
Hitachi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Ltd filed Critical Hitachi Ltd
Priority to JP57049071A priority Critical patent/JPS58167947A/en
Publication of JPS58167947A publication Critical patent/JPS58167947A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/20Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/307Sample handling arrangements, e.g. sample cells, spinning mechanisms specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer

Abstract

PURPOSE:To remove absorption spectrum (background spectrum) caused by a spinner itself by manufacturing a rotor with ceramics or glass ceramics. CONSTITUTION:As the base material of a spinner 2 to be used in the magic angle spinning method wherein a solid specimen 6 is caused to rotate around a shaft tilted by an angle of 54.7 deg. (magic angle) from the direction of magnetic field at a high speed of several kHz and by this, a sharp NMR spectrum can be obtained, a kind of ceramics or that of glass ceramics is used. The ceramics is the sinter of a composition consists of 30-96wt% of boron nitride and 70- 4wt% of a ceramics other than boron nitride, and the glass ceramics is such a substance containing fine crystals of synthetic mica which is known by the trade name of MAKORU. By the use of a spinner made of such materials, it is possible to easily obtain C13NMR spectrum of a solid specimen free from background spectrum caused by the spinner itself.
JP57049071A 1982-03-29 1982-03-29 Spinner of nuclear magnetic resonance device Pending JPS58167947A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP57049071A JPS58167947A (en) 1982-03-29 1982-03-29 Spinner of nuclear magnetic resonance device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP57049071A JPS58167947A (en) 1982-03-29 1982-03-29 Spinner of nuclear magnetic resonance device

Publications (1)

Publication Number Publication Date
JPS58167947A true JPS58167947A (en) 1983-10-04

Family

ID=12820843

Family Applications (1)

Application Number Title Priority Date Filing Date
JP57049071A Pending JPS58167947A (en) 1982-03-29 1982-03-29 Spinner of nuclear magnetic resonance device

Country Status (1)

Country Link
JP (1) JPS58167947A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007218697A (en) * 2006-02-15 2007-08-30 Sumitomo Rubber Ind Ltd Rubber specimen tension tool, molecular structure/molecular motility property analyzer for rubber specimen in stretched state, and analysis method
JP2008014651A (en) * 2006-07-03 2008-01-24 National Institute For Materials Science Mas probe apparatus for solid-state nmr
US7482810B2 (en) 2004-11-26 2009-01-27 National University Corporation Tokyo University Of Agriculture And Technology Sample tube for solid-state nuclear magnetic resonance apparatus magic angle high-speed rotation method and method for measuring nuclear magnetic resonance absorption spectrum employing it
WO2012082204A1 (en) * 2010-12-13 2012-06-21 Battelle Memorial Institute Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
JP2012247442A (en) * 2012-09-21 2012-12-13 National Institute For Materials Science Mas probe apparatus for solid-state nmr

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5417796A (en) * 1977-06-03 1979-02-09 Inst Kiberunechiki Akademii Na Sensor for generating nuclear magnetic resonance

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5417796A (en) * 1977-06-03 1979-02-09 Inst Kiberunechiki Akademii Na Sensor for generating nuclear magnetic resonance

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7482810B2 (en) 2004-11-26 2009-01-27 National University Corporation Tokyo University Of Agriculture And Technology Sample tube for solid-state nuclear magnetic resonance apparatus magic angle high-speed rotation method and method for measuring nuclear magnetic resonance absorption spectrum employing it
JP2007218697A (en) * 2006-02-15 2007-08-30 Sumitomo Rubber Ind Ltd Rubber specimen tension tool, molecular structure/molecular motility property analyzer for rubber specimen in stretched state, and analysis method
JP2008014651A (en) * 2006-07-03 2008-01-24 National Institute For Materials Science Mas probe apparatus for solid-state nmr
WO2012082204A1 (en) * 2010-12-13 2012-06-21 Battelle Memorial Institute Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
US8692548B2 (en) 2010-12-13 2014-04-08 Battelle Memorial Institute Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
US9835698B2 (en) 2010-12-13 2017-12-05 Battelle Memorial Institute Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
JP2012247442A (en) * 2012-09-21 2012-12-13 National Institute For Materials Science Mas probe apparatus for solid-state nmr

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