JPS58143237A - Method for measuring moisture content of sample - Google Patents

Method for measuring moisture content of sample

Info

Publication number
JPS58143237A
JPS58143237A JP2662582A JP2662582A JPS58143237A JP S58143237 A JPS58143237 A JP S58143237A JP 2662582 A JP2662582 A JP 2662582A JP 2662582 A JP2662582 A JP 2662582A JP S58143237 A JPS58143237 A JP S58143237A
Authority
JP
Japan
Prior art keywords
arm
moisture content
sample
tool
hanging
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2662582A
Other languages
Japanese (ja)
Inventor
Yoshinobu Oda
小田 義宣
Takeo Kawakita
川北 丈夫
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Gunze Ltd
Original Assignee
Gunze Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Gunze Ltd filed Critical Gunze Ltd
Priority to JP2662582A priority Critical patent/JPS58143237A/en
Publication of JPS58143237A publication Critical patent/JPS58143237A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

PURPOSE:To measure moisture content simply and quickly in high accuracy, by providing an arm descendable its tip end freely in a box which is capable of humidifying and drying, hanging a sample hanging tool to this arm and carrying out weighing in the state released from hanging the tool. CONSTITUTION:An arm 4 which is supported by a turnable shaft 5 as a fulcrum and is descendable its tip end through a spring 6 is provided in a box 1 which is capable of humidifying and drying and a sample hanging tool 3 is hung on the arm 4 and, a sample is hung on a needle 14. At the time of measuring the moisture content, a hanging state from the arm 4 is released by pushing down the arm 4 by an outside knob through a pressing tool 7 and placing the tool 3 in a groove 12 of a sample stand 11 of a weighing device 21 and it is weighed. The weight of the sample is obtained by subtracting the weight of the tool 3 from the weight at that time and the moisture content is obtained by subtracting moreover absolutely dried weight. Hereby, the moisture content is measured simply and quickly in high accuracy.

Description

【発明の詳細な説明】 本発明は簡便にして迅速に資料中の水分率を測定可能な
らしめた質料の水分率測定方法に関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for measuring the moisture content of materials that allows the moisture content of materials to be measured easily and quickly.

従来、資料中の水分率はa1々の方法で測定さrlてい
たが、各社各様の方式で行ってυす、一般には試験ホッ
クス中しで資料を吊り下け、一定条件後、その資料を取
り出し迅速に測定して水分率を求めるという原始的な方
法によっていた、ところがこ扛ら従前の方法では試料を
外部にノ1?i2 出す必要があり、このため外部条件に左右さ扛て測定誤
差が出やすく問題であった。例えば資料を取出すときボ
ックス内の温湿度が変化したり、取出した質料が外部の
温湿度により変化したり、ホックス内の駅気が例へ強制
的に循環され°Cいたとしても、ボックス内の温湿度を
全く均一にするこはできず、場所&−一よる温度差斑は
避けらnない等の神々の間廟点があった。
Conventionally, the moisture content in materials has been measured using various methods, but each company uses its own method.Generally, the materials are suspended in a test hook, and after certain conditions, the materials are measured. The previous method used a primitive method of taking out the sample and quickly measuring it to determine the moisture content. i2, which was a problem because it was dependent on external conditions and measurement errors were likely to occur. For example, when taking out materials, the temperature and humidity inside the box may change, the material taken out may change due to the outside temperature and humidity, or even if the air inside the box is forcibly circulated to °C, the temperature inside the box may change. There were temples of the gods where it was impossible to make the temperature and humidity completely uniform, and variations in temperature depending on the location were unavoidable.

そこで本発明者らは試料を外部に持ち出すことがなく、
しかも迅速に資料中の水分率を泪1j定すべく神々の方
法を検t・1シた結果、ついに本発明に到達した。即ち
本発明の特徴とするところは、加湿及び乾燥自在なホッ
クス内に[al動、停止自在かつ降下自在なアームを設
けると共に、前記アームに餘料吊下具vf−垂下せしめ
停止中のアームを降下せしめて、61j記吊下其の垂下
を解除せしめ、しかる後秤を器で計賞してなる加湿、乾
燥水分率の測定方法を提供せんとした点にある。
Therefore, the inventors did not take the sample outside,
Moreover, as a result of testing countless divine methods to quickly determine the moisture content in materials, we finally arrived at the present invention. That is, the characteristics of the present invention are that an arm that can be moved, stopped, and lowered is provided in a hook that can be humidified and dried, and that a food hanging tool VF is attached to the arm while the arm is suspended. The object of the present invention is to provide a method for measuring humidification and dry moisture content by lowering the suspension, releasing the sagging of the suspension described in 61j, and then measuring it with a scale.

次に本発明を実施するための装置の実施例を第1〜3図
により詣1明しつ一1本発明の構成を述べA3 ることにする。
Next, we will explain an embodiment of the apparatus for carrying out the present invention with reference to FIGS. 1 to 3, and then describe the structure of the present invention.

資料(省略)は資料吊下具(3)V″CS−いて例えぽ
釦(14)により吊り下をすら1.るもので、資料吊下
具(3)はアーム(4)に通常垂下され、すり止め具(
16)により前後動かしないようになっている。このア
ーム(4)は少なくとも吊下具を吊り下げる位置で降下
できるように心棒(5)に、心棒(5)を支点として取
り付けらt1降下後元に戻すため、スプリング+61が
付設さ扛ている。アーム(4)は本例では左右に2本付
いているが、こnは4本で吃8木でも適宜でよい。アー
ム(4)を降下せしめるためにパー(2)に押え具(7
)が相段されており、こ、の押え具(7)は取り手(8
)を第1図矢印の方に持ち上けることによりスプリング
(9)が伸び、第2図の如き状態となって押え具(7)
がアーム14)を押し、アーム(41の少なくとも吊下
具の吊下位置は降下する。この時、資料吊下具(3)の
プレー)(131が秤量器(10)に通ずる資料台(1
1)の@(121に入り込み状に載置臼\アーム(4)
からの吊下げ状態が解除jflで吊り下げ先端(15)
がアームから浮きフリー状態となる。この時、秤量器(
lO)には資料吊下具(3)と資料(省略)の車量が表
示されるのである、あと資料吊下具の重量を引いておけ
は資料のA(都−が計量さn、ることになる。しかる後
、取り手(8)ケになすとスプリング(9)の作用で押
え具(71が11−1位に戻り、と同時にアーム(4)
もスプリング(6)の作用で11:1位に戻る。アーム
(4)は回動自在で、必要な時に前記の操作を行ない資
料の重量を測定すn trotよいようになっている3
以上の装置はボックス(1)内に付設さ71.ており、
第3図に示すように正面にのぞき愈(段があって、この
窓より中の状態を見つ(必すな時、例えばホックス(1
)外に取り付けた収り手(8)を操作す扛ばよい。ボッ
クス(1)は加湿、乾燥自社に設計さn、ており、こオ
′1.により加湿状態、乾燥状態をチェックしつ!、必
要時に資料N量を測定して資料中の水分率を求めtばよ
い。この際、アームを回動自在とすることにより資料中
の加湿、乾燥斑を防止でき、また加l昆、乾燥げ湿風、
冷熱風の夫々発生装置により、血止にコントロールさn
たエアーとして強制吹込み、循環を行なえはよく、秤量
中はエアーの吹込み、循環をストップすb5 jばよい。ボックスは断熱状態G401とし、高温、高
湿状態において露結が生じないようになっており、これ
により長時間の安定計測が可能である。秤量器は適宜で
よいが例えば0.01〜Q、OO1gr単位の自動重子
天秤(21)を用いると効果的で、ボックス外から計量
できるようにボックス(1)に資料台0])の径よりや
!大きな径を有するBいていて、接触しないようになっ
ており、こ!から資料台(Illのみがボックス内に通
じている、従って計量は外部で可能なわけであり、また
アーム(4)の降下は人為的に行なうも機械的に行なう
もよい。心棒(5)はモーター07)により定速で回転
しており、必要時に例えば計量器の資料台の真上でスト
ップできるようになっている。
The material (omitted) is a material hanging tool (3) V"CS-, and the material hanging tool (3) is normally hung from the arm (4). , anti-slip tool (
16) prevents it from moving back and forth. This arm (4) is attached to the mandrel (5) using the mandrel (5) as a fulcrum so that it can be lowered at least to the position where the hanging tool is suspended, and a spring +61 is attached to it to return it to its original position after descending at t1. . In this example, there are two arms (4) on the left and right sides, but there may be four arms (4) and eight arms (8 arms) as appropriate. In order to lower the arm (4), a presser (7) is attached to the par (2).
) are arranged in parallel, and the presser foot (7) is connected to the handle (8).
) in the direction of the arrow in Figure 1, the spring (9) will stretch, and the presser (7) will be in the state shown in Figure 2.
presses the arm 14), and at least the hanging position of the hanging tool of the arm (41) is lowered.
1) @ (121) Place the mortar in a recessed manner @ Arm (4)
The hanging state is released from jfl and the hanging tip (15)
floats off the arm and becomes free. At this time, use a weighing device (
1O) displays the vehicle weight of the material hanging tool (3) and the material (omitted).Also, subtract the weight of the material hanging tool. After that, when it is placed on the handle (8), the presser (71) returns to the 11-1 position due to the action of the spring (9), and at the same time, the arm (4)
The ratio returns to 11:1 due to the action of the spring (6). The arm (4) is rotatable, making it easy to carry out the above operations and measure the weight of materials when necessary.
The above devices are attached to the box (1) 71. and
As shown in Figure 3, there is a peephole (step) in front of the window.
) All you have to do is operate the handle (8) attached to the outside. Box (1) is designed in-house for humidification and drying. Check the humidification and dryness conditions! , just measure the amount of material N and find the moisture content in the material when necessary. At this time, by making the arm freely rotatable, it is possible to prevent humidification and dry spots in the material, and also to prevent humidification, dryness, dampness, etc.
Hemostasis can be controlled by each generator of cold and hot air.
It is best to forcefully blow in and circulate the air, or just stop the air blowing and circulation during weighing. The box is in an insulated state G401 to prevent dew condensation from occurring in high temperature and high humidity conditions, allowing stable measurement over a long period of time. Any weighing device may be used, but for example, it is effective to use an automatic weight balance (21) with a unit of 0.01 to Q, OO1gr. or! B has a large diameter so that they do not come into contact with each other. Only the data table (Ill) is connected to the inside of the box, so weighing can be done externally, and the arm (4) can be lowered manually or mechanically.The mandrel (5) It is rotated at a constant speed by a motor 07), and can be stopped, for example, right above the data table of a weighing instrument when necessary.

以上は本発明を実施するための好適なl実施例であり、
本発明は斯る実施例に制限を受けることなく、1内室の
実施態様をとることが可酢でめる。
The above are preferred embodiments for carrying out the present invention,
The present invention is not limited to such embodiments, and can be implemented in one-chamber embodiments.

本発明に係るボックスとは適宜でよく、加温乾燥機構が
そなわっていn、ば特に制限はない。
The box according to the present invention may be any suitable box, and is not particularly limited as long as it is equipped with a heating and drying mechanism.

−また、降下自在なアームの降下機構についてもlfh
 6 人為的、機械的を問わすJ−宜でよい。アームの回転、
停止についても人為的、機械的を問わず適宜でよく、電
気回路を組み込んで必要時に秤量場所で停止できる機構
とするとより好ましい。資料吊下具についてはアームか
らの垂下f:解除するためには個室に行なえばよく、機
械的に自動で行なうことも当然用油である。秤量器につ
いてもJ円宜でよいが精度を商めるならば、より精密な
大びん等を使用すれはよい。
-Also, regarding the lowering mechanism of the arm that can be lowered freely, lfh
6 Artificial or mechanical J-Anything is fine. rotation of the arm,
Stopping may be done either manually or mechanically, and it is more preferable to incorporate an electric circuit into a mechanism that allows stopping at the weighing location when necessary. As for the document hanging tool, it can be removed from the arm in a private room, and of course it can be done mechanically and automatically. As for the weighing device, J-yen scale is fine, but if you value accuracy, it is better to use a more precise large bottle or the like.

本発明は第4図の如き実施態様を取ることもできる。即
ち第4図における資料吊下具(3)がアーム(4)によ
り垂下さnている状態は第1図と同様であるが、アーム
(4)が82図の如く降下して鎖線位置にきた時、上部
から下ってきているカギ部材(24)により、吊下具(
3)の先端(15)が保持さA2ることになる。このカ
ギ部材がボックス外部の秤量器と直結している場合、資
料(略)と資料吊下具の重量が秤量器によって計量さn
ること番でなり、以下前述の実施例同様に質量の重量が
外部から知ることができ、とnにより質料の水分率が簡
単に71111定できlん7 ることになる。
The present invention can also be implemented as shown in FIG. In other words, the state in which the material hanging tool (3) is suspended by the arm (4) in Fig. 4 is the same as in Fig. 1, but the arm (4) has descended to the chain line position as shown in Fig. 82. When the hanging tool (
The tip (15) of 3) will be held A2. If this key member is directly connected to a scale outside the box, the weight of the material (omitted) and the material hanging tool will be measured by the scale.
As in the previous embodiment, the weight of the mass can be known from the outside, and the moisture content of the material can be easily determined by n.

この際、カギ部材(24)は資料吊下具(3)を吊り下
げる件・造のものならば、】画室でよいことは勿論であ
る。尚、資料中の水分率を求めるには、例えば絶乾状態
の重量(A−)と加湿時の隼t (B)とを求め次式に
よn、ばよい。
In this case, it goes without saying that the key member (24) may be used in the gallery as long as it is made to hang the document hanging tool (3). In order to determine the moisture content in the material, for example, the weight (A-) in an absolutely dry state and the weight (B) in a humidified state may be calculated using the following formula.

−A 水分率= □  X  I OO(%)この際、本発明
の方法により例えばボックス内rM7F20℃、114
 yt 11 S’ 40 v)11.)f IfCテ
、水分率300%に湿潤した綿布を乾燥した時の経時に
おける水分率の変化を第5図に示し、またボックス内温
度30°C1相対湿度80%)1.[−1に”C5乾燥
さtた締布を吸湿させた時の経時における水分率の変化
を第6図にボした。
-A Moisture content = □ X I OO (%) At this time, by the method of the present invention,
yt 11 S' 40 v)11. Figure 5 shows the change in moisture content over time when a cotton cloth moistened to a moisture content of 300% is dried. Figure 6 shows the change in moisture content over time when the tightening cloth that had been dried to [-1] was allowed to absorb moisture.

貼る例の妬く本発明の方法によると水分率曲線も碓めて
迅速に不めることができる。
According to the method of the present invention, the moisture content curve can also be improved and quickly improved.

本発明に係る資料としではイ[1帛、紙、水相、パルプ
その他全てのものを例示でき、特に制限はない。
Examples of materials related to the present invention include paper, aqueous phase, pulp, and all other materials, and there are no particular limitations.

本発明はν)、上の通りであり、不発明によると肯料中
の水分碑”を極めて迅速に測定することが0丁能となり
、71f11定時間の短縮に大きな寄与奮及はした8更
に湿度や温度を任意に一定状態に作り出すことか11丁
能であり、測定誤差もはとんどなく測定の精度向上に格
別なる効果を発揮した。
The present invention is ν), as described above, and according to the invention, it has become possible to extremely quickly measure the moisture content in samples, and has greatly contributed to shortening the 71f11 fixed time8. It has the ability to arbitrarily create a constant humidity and temperature, and it has been extremely effective in improving measurement accuracy, with almost no measurement errors.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本発明の一実施例を示す斜視図であり、ψ72
図はその作動状態を曲、明するための要部の斜視し[で
あり、様、3図は本発明の一実施例會示すfIJIl而
図であ面、第4図は他の実施例を説明するための要部の
斜視図であり、第5図、第6図は本発明により測定した
結果を表わすクラ7である。 tlL−−−−ボックス     f2+−一−−−−
−バーt3+ −−−一腎料吊下具    (41−−
−−−−アーム(5)−〜−−’u棒       (
61f91−−−−−スプリング(7+−−−−押え具
      ()l+−−−−−−一取り手引)−一−
−瞥料台(秤量台)  (121−−一−−−渦(1:
(l−−−−−ブレート      +141−−−−
−−針]Fa9 (151−−−−−−一資料吊下具の先端 1fiL−
−−−−−−ビン0η−−一−−−−七−ター    
  +1.a−−−−−−−のぞき窓にflii−−−
−−一断熱材      (21)−−−一秤l′器(
22)−−−一穴        (24)−−−−一
カキ部材特許出仙人 グンゼ株式公社
FIG. 1 is a perspective view showing an embodiment of the present invention, with ψ72
The figure is a perspective view of the main parts for illustrating the operating state, Figure 3 is a perspective view showing one embodiment of the present invention, and Figure 4 is a side view showing another embodiment. FIG. 5 and FIG. 6 are perspective views of the main parts for the measurement, and FIGS. tlL---Box f2+-1---
- Bar t3+ --- Single kidney drug hanging tool (41--
----- Arm (5) ---'u rod (
61f91-----Spring (7+-----Pressing tool ()l+--------1 handling manual) -1-
-Weighing table (121--1--Vortex (1:
(l---Brate +141------
--Needle] Fa9 (151------1 material tip of hanging tool 1fiL-
−−−−−−bin 0η−−1−−−−7−ter
+1. a------ flii in the peephole---
---1 insulation material (21) ---1 scale l' device (
22) --- One hole (24) --- One oyster component patented Sennin Gunze Co., Ltd.

Claims (1)

【特許請求の範囲】[Claims] 加湿及び乾燥自任なボックス内に回動、停止自在かつ、
降下自在なアームを設けると共に、前記アームに資料吊
下具を垂下せしめ、停止中のアームを降下せしめて前記
吊下具の垂下を解除せしめ、然る後、秤旬゛器で計匍・
シてなることを特徴とする資料の水分率泪11定方法。
It can be freely rotated and stopped in a humidifying and drying box.
An arm that can be lowered freely is provided, and a document hanging device is suspended from the arm, and the stopped arm is lowered to release the hanging device.
11 methods for determining the moisture content of materials, which are characterized by the following:
JP2662582A 1982-02-19 1982-02-19 Method for measuring moisture content of sample Pending JPS58143237A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2662582A JPS58143237A (en) 1982-02-19 1982-02-19 Method for measuring moisture content of sample

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2662582A JPS58143237A (en) 1982-02-19 1982-02-19 Method for measuring moisture content of sample

Publications (1)

Publication Number Publication Date
JPS58143237A true JPS58143237A (en) 1983-08-25

Family

ID=12198637

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2662582A Pending JPS58143237A (en) 1982-02-19 1982-02-19 Method for measuring moisture content of sample

Country Status (1)

Country Link
JP (1) JPS58143237A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3306300A4 (en) * 2015-05-28 2019-01-23 Kaken Test Center Humidity-dependent-mass measurement device and humidity-dependent-mass measurement method
CN111006456A (en) * 2019-11-20 2020-04-14 浙江省海洋水产研究所 Water sample suspended solid drying box

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3306300A4 (en) * 2015-05-28 2019-01-23 Kaken Test Center Humidity-dependent-mass measurement device and humidity-dependent-mass measurement method
CN111006456A (en) * 2019-11-20 2020-04-14 浙江省海洋水产研究所 Water sample suspended solid drying box

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