JPS57115419A - Reduction of oligomeric cyclic ether content in polymer - Google Patents

Reduction of oligomeric cyclic ether content in polymer

Info

Publication number
JPS57115419A
JPS57115419A JP56183930A JP18393081A JPS57115419A JP S57115419 A JPS57115419 A JP S57115419A JP 56183930 A JP56183930 A JP 56183930A JP 18393081 A JP18393081 A JP 18393081A JP S57115419 A JPS57115419 A JP S57115419A
Authority
JP
Japan
Prior art keywords
polymer
reduction
cyclic ether
ether content
oligomeric cyclic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP56183930A
Other languages
English (en)
Other versions
JPS5946972B2 (ja
Inventor
Bagubaado Koupurin Harii
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of JPS57115419A publication Critical patent/JPS57115419A/ja
Publication of JPS5946972B2 publication Critical patent/JPS5946972B2/ja
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0403—Solvent extraction of solutions which are liquid with a supercritical fluid
    • B01D11/0407—Solvent extraction of solutions which are liquid with a supercritical fluid the supercritical fluid acting as solvent for the solute
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4854—Polyethers containing oxyalkylene groups having four carbon atoms in the alkylene group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/16—Cyclic ethers having four or more ring atoms
    • C08G65/20—Tetrahydrofuran
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/32—Polymers modified by chemical after-treatment
    • C08G65/329—Polymers modified by chemical after-treatment with organic compounds
    • C08G65/337—Polymers modified by chemical after-treatment with organic compounds containing other elements
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP56183930A 1980-11-19 1981-11-18 重合体のオリゴマ−性環状エ−テル分減少方法 Expired JPS5946972B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US208422 1980-11-19
US06/208,422 US4306058A (en) 1980-11-19 1980-11-19 Method for reducing oligomeric cyclic ether content of a polymerizate

Publications (2)

Publication Number Publication Date
JPS57115419A true JPS57115419A (en) 1982-07-17
JPS5946972B2 JPS5946972B2 (ja) 1984-11-16

Family

ID=22774551

Family Applications (1)

Application Number Title Priority Date Filing Date
JP56183930A Expired JPS5946972B2 (ja) 1980-11-19 1981-11-18 重合体のオリゴマ−性環状エ−テル分減少方法

Country Status (6)

Country Link
US (1) US4306058A (ja)
EP (1) EP0052276A1 (ja)
JP (1) JPS5946972B2 (ja)
CA (1) CA1184344A (ja)
ES (1) ES507268A0 (ja)
PL (1) PL233898A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH024757A (ja) * 1988-03-22 1990-01-09 Rhone Poulenc Chim 液体若しくは過臨界ｃｏ↓２を用いた抽出によるイソシアネート縮合物の精製および単離方法

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4500705A (en) * 1984-01-09 1985-02-19 E. I. Du Pont De Nemours And Company Method for reducing oligomeric cyclic ether content of a polymerizate
DE3606479A1 (de) * 1986-02-28 1987-09-03 Basf Ag Verfahren zur herstellung von polyoxibutylenpolyoxialkylenglykolen mit enger molekulargewichtsverteilung und vermindertem gehalt an oligomeren cyclischen ethern
DE3725577A1 (de) * 1987-08-01 1989-02-09 Basf Ag Verfahren zur reinigung von polyoxybutylenpolyoxyalkylenglykolen
FR2628983B1 (fr) * 1988-03-28 1991-09-06 Commissariat Energie Atomique Procede de purification de composes emulsionnants en vue de reduire leur teneur en dioxanne
JPH07121321B2 (ja) * 1988-07-01 1995-12-25 東洋エンジニアリング株式会社 抽出方法
US5237048A (en) * 1988-09-22 1993-08-17 Toyo Engineering Corporation Method for purifying polymer
US5298670A (en) * 1993-04-02 1994-03-29 Industrial Technology Research Institute Method of controlling molecular weight distribution of polytetramethylene ether glycol
US5562808A (en) * 1993-09-21 1996-10-08 Pharm-Eco Laboratories, Inc. Method and apparatus for decontaminating a liquid surfactant of dioxane
US5684179A (en) * 1995-12-14 1997-11-04 E. I. Du Pont De Nemours And Company Method for recovering diacetate esters of polytetramethylene ethers
DE19616046C2 (de) 1996-04-23 1998-03-26 Joachim Brimmer Ingenieurbuero Verfahren zur Abtrennung von organischen Monomeren oder Hilfsstoffen
WO1998020051A1 (en) * 1996-11-07 1998-05-14 The Penn State Research Foundation Short-cycle removal of impurities from polymers
GB0216780D0 (en) * 2002-07-19 2002-08-28 Bradford Particle Design Ltd Methods of particle formation
US20100267905A1 (en) * 2009-04-15 2010-10-21 Invista North America S.A R.L. Copolyether glycol manufacturing process
US8609805B2 (en) 2009-04-15 2013-12-17 Invista North America S.A R.L. Copolyether glycol manufacturing process
MX2011010777A (es) * 2009-04-15 2012-01-20 Invista Tech Sarl Proceso mejorado para la produccion de copolieter glicoles.
DE102015215387A1 (de) 2015-08-12 2017-02-16 Evonik Degussa Gmbh Verfahren zur Herstellung von Polyalkenameren für Verpackungsanwendungen
EP3360904A1 (en) 2017-02-10 2018-08-15 Evonik Degussa GmbH Process for preparing polyalkenamers for packaging applications

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3202605A (en) * 1962-06-06 1965-08-24 Badger Co Propane deaspihalting process
DE1493190C3 (de) * 1963-04-16 1980-10-16 Studiengesellschaft Kohle Mbh, 4330 Muelheim Verfahren zur Trennung von Stoffgemischen
AT313039B (de) * 1971-05-07 1974-01-25 Studiengesellschaft Kohle Mbh Verfahren zur Gewinnung von Coffein aus Rohkaffee
DE2340566C2 (de) 1973-08-10 1985-11-07 Peter, Siegfried, Prof.Dr., 8520 Erlangen Verfahren zur Trennung von Komponenten von Stoffgemischen mit niedrigem Dampfdruck mit Hilfe eines komprimierten Gases unter überkritischen Bedingungen und einer weiteren, den Trenneffekt beeinflussenden Substanz
JPS5260899A (en) * 1975-11-14 1977-05-19 Nippon Oil & Fats Co Ltd Purification method of polyalkylene
JPS5381597A (en) * 1976-12-28 1978-07-19 Asahi Denka Kogyo Kk Purification of polyoxyalkylene polyol
US4202964A (en) * 1978-03-16 1980-05-13 E. I. Du Pont De Nemours And Company Method for reducing oligomeric cyclic ether content of a polymerizate
US4192943A (en) * 1978-06-13 1980-03-11 E. I. Du Pont De Nemours And Company Method for reducing oligomeric cyclic ether content of a polymerizate
FR2429234A1 (fr) * 1978-06-20 1980-01-18 Du Pont Procede perfectionne pour la preparation de copolyether-glycols

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH024757A (ja) * 1988-03-22 1990-01-09 Rhone Poulenc Chim 液体若しくは過臨界ｃｏ↓２を用いた抽出によるイソシアネート縮合物の精製および単離方法

Also Published As

Publication number Publication date
CA1184344A (en) 1985-03-19
EP0052276A1 (en) 1982-05-26
ES8304174A1 (es) 1983-02-16
ES507268A0 (es) 1983-02-16
US4306058A (en) 1981-12-15
JPS5946972B2 (ja) 1984-11-16
PL233898A1 (ja) 1982-05-24

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