JPS5549396A - Preparation of 17alpha-methylsteroid - Google Patents
Preparation of 17alpha-methylsteroidInfo
- Publication number
- JPS5549396A JPS5549396A JP12179478A JP12179478A JPS5549396A JP S5549396 A JPS5549396 A JP S5549396A JP 12179478 A JP12179478 A JP 12179478A JP 12179478 A JP12179478 A JP 12179478A JP S5549396 A JPS5549396 A JP S5549396A
- Authority
- JP
- Japan
- Prior art keywords
- reacting
- steroid
- reaction
- methyl
- metal reagent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003153 chemical reaction reagent Substances 0.000 abstract 4
- 238000006243 chemical reaction Methods 0.000 abstract 3
- 239000002184 metal Substances 0.000 abstract 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 3
- 150000003431 steroids Chemical class 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- PAOWPNQOTVTCAF-OEUJLIAZSA-N (8r,9s,10r,13s,14s)-3-ethoxy-10,13-dimethyl-1,2,7,8,9,11,12,14,15,16-decahydrocyclopenta[a]phenanthren-17-one Chemical compound C1C[C@@H]2[C@](CCC(OCC)=C3)(C)C3=CC[C@H]2[C@@H]2CCC(=O)[C@]21C PAOWPNQOTVTCAF-OEUJLIAZSA-N 0.000 abstract 1
- QZLYKIGBANMMBK-UGCZWRCOSA-N 5α-Androstane Chemical compound C([C@@H]1CC2)CCC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CCC[C@@]2(C)CC1 QZLYKIGBANMMBK-UGCZWRCOSA-N 0.000 abstract 1
- 229930194542 Keto Natural products 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 1
- -1 keto compound Chemical class 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Landscapes
- Steroid Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12179478A JPS5549396A (en) | 1978-10-03 | 1978-10-03 | Preparation of 17alpha-methylsteroid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12179478A JPS5549396A (en) | 1978-10-03 | 1978-10-03 | Preparation of 17alpha-methylsteroid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5549396A true JPS5549396A (en) | 1980-04-09 |
| JPS629116B2 JPS629116B2 (enrdf_load_stackoverflow) | 1987-02-26 |
Family
ID=14820063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP12179478A Granted JPS5549396A (en) | 1978-10-03 | 1978-10-03 | Preparation of 17alpha-methylsteroid |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5549396A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57158984A (en) * | 1981-03-26 | 1982-09-30 | Nippon Dennetsu Kk | Method of producing sheathed heater |
| JPS57158986A (en) * | 1981-03-26 | 1982-09-30 | Nippon Dennetsu Kk | Method of producing sheathed heater |
| CN106397520A (zh) * | 2016-09-02 | 2017-02-15 | 湖南科瑞生物制药股份有限公司 | 甲基睾丸素的制备方法 |
| CN110003297A (zh) * | 2018-01-04 | 2019-07-12 | 上海安谱实验科技股份有限公司 | 一种稳定同位素标记的甲睾酮及其合成方法 |
-
1978
- 1978-10-03 JP JP12179478A patent/JPS5549396A/ja active Granted
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57158984A (en) * | 1981-03-26 | 1982-09-30 | Nippon Dennetsu Kk | Method of producing sheathed heater |
| JPS57158986A (en) * | 1981-03-26 | 1982-09-30 | Nippon Dennetsu Kk | Method of producing sheathed heater |
| CN106397520A (zh) * | 2016-09-02 | 2017-02-15 | 湖南科瑞生物制药股份有限公司 | 甲基睾丸素的制备方法 |
| CN110003297A (zh) * | 2018-01-04 | 2019-07-12 | 上海安谱实验科技股份有限公司 | 一种稳定同位素标记的甲睾酮及其合成方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS629116B2 (enrdf_load_stackoverflow) | 1987-02-26 |
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