JPS554350A - Preparation of o-alkylisourea - Google Patents

Preparation of o-alkylisourea

Info

Publication number
JPS554350A
JPS554350A JP7736578A JP7736578A JPS554350A JP S554350 A JPS554350 A JP S554350A JP 7736578 A JP7736578 A JP 7736578A JP 7736578 A JP7736578 A JP 7736578A JP S554350 A JPS554350 A JP S554350A
Authority
JP
Japan
Prior art keywords
solvent
urea
reaction
alkylisourea
dialkyl sulfate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP7736578A
Other languages
Japanese (ja)
Other versions
JPS6230983B2 (en
Inventor
Tomiro Iwai
Tomiyasu Tsunoda
Ichiro Yamamoto
Masao Kuronuma
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to JP7736578A priority Critical patent/JPS554350A/en
Publication of JPS554350A publication Critical patent/JPS554350A/en
Publication of JPS6230983B2 publication Critical patent/JPS6230983B2/ja
Granted legal-status Critical Current

Links

Abstract

PURPOSE: To obtain the title substance, a guanidyl group-forming agent, in high purity safely, by controlling the reaction of urea with a dialkyl sulfate in a specific solvent effectively under heating.
CONSTITUTION: One mole each of urea and a dialkyl sulfate are reacted in 7W30 ml of a solvent, e.g. a monocyclic aromatic hydrocarbon such as benzene or toluene, or a lower saturated cmonohydric alcohol such as methanol or ethanol, or a combination of two or more types at 80W100°C to give an O-alkylisourea.
EFFECT: Rapid increase of temperature can be controlled by absorbing the instantaneous heat generation in the reaction with the latent heat of vaporization of the solvent.
COPYRIGHT: (C)1980,JPO&Japio
JP7736578A 1978-06-28 1978-06-28 Preparation of o-alkylisourea Granted JPS554350A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP7736578A JPS554350A (en) 1978-06-28 1978-06-28 Preparation of o-alkylisourea

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7736578A JPS554350A (en) 1978-06-28 1978-06-28 Preparation of o-alkylisourea

Publications (2)

Publication Number Publication Date
JPS554350A true JPS554350A (en) 1980-01-12
JPS6230983B2 JPS6230983B2 (en) 1987-07-06

Family

ID=13631871

Family Applications (1)

Application Number Title Priority Date Filing Date
JP7736578A Granted JPS554350A (en) 1978-06-28 1978-06-28 Preparation of o-alkylisourea

Country Status (1)

Country Link
JP (1) JPS554350A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0915083A2 (en) * 1997-11-04 1999-05-12 Basf Aktiengesellschaft Process for the preparation of substituted guanidine derivatives
US5969182A (en) * 1997-11-04 1999-10-19 Basf Aktiengesellschaft Preparation of substituted guanidine derivatives
JP2008095634A (en) * 2006-10-13 2008-04-24 Denso Corp Scroll compressor
CN102432506A (en) * 2011-11-10 2012-05-02 江苏远洋药业股份有限公司 Synthetic method of O-methyl-isourea

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0915083A2 (en) * 1997-11-04 1999-05-12 Basf Aktiengesellschaft Process for the preparation of substituted guanidine derivatives
US5969182A (en) * 1997-11-04 1999-10-19 Basf Aktiengesellschaft Preparation of substituted guanidine derivatives
EP0915083A3 (en) * 1997-11-04 1999-12-08 Basf Aktiengesellschaft Process for the preparation of substituted guanidine derivatives
US6093848A (en) * 1997-11-04 2000-07-25 Basf Aktiengesellschaft Preparation of substituted guanidine derivatives
JP2008095634A (en) * 2006-10-13 2008-04-24 Denso Corp Scroll compressor
CN102432506A (en) * 2011-11-10 2012-05-02 江苏远洋药业股份有限公司 Synthetic method of O-methyl-isourea

Also Published As

Publication number Publication date
JPS6230983B2 (en) 1987-07-06

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