JPS5540603A - Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl)phenol)sulfide - Google Patents

Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl)phenol)sulfide

Info

Publication number
JPS5540603A
JPS5540603A JP11227078A JP11227078A JPS5540603A JP S5540603 A JPS5540603 A JP S5540603A JP 11227078 A JP11227078 A JP 11227078A JP 11227078 A JP11227078 A JP 11227078A JP S5540603 A JPS5540603 A JP S5540603A
Authority
JP
Japan
Prior art keywords
tetramethylbutyl
phenol
bis
sulfide
reacting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP11227078A
Other languages
Japanese (ja)
Other versions
JPS5842866B2 (en
Inventor
Teruhiro Yamaguchi
Tadashi Kobayashi
Keisaburo Yamaguchi
Naomichi Murakami
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Priority to JP53112270A priority Critical patent/JPS5842866B2/en
Priority to GB7931450A priority patent/GB2031422B/en
Priority to AU50788/79A priority patent/AU526442B2/en
Priority to IT25694/79A priority patent/IT1123138B/en
Priority to FR7922784A priority patent/FR2436137A1/en
Priority to NLAANVRAGE7906800,A priority patent/NL186632C/en
Priority to DE19792937294 priority patent/DE2937294A1/en
Publication of JPS5540603A publication Critical patent/JPS5540603A/en
Priority to US06/288,428 priority patent/US4380671A/en
Publication of JPS5842866B2 publication Critical patent/JPS5842866B2/en
Expired legal-status Critical Current

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To prepare 2, 2'-bis[4-(1, 1, 3, 3-tetramethylbutyl)phenol]sulfide, useful as a light stabilizer, an additive for lubricant oils, etc., easily without by-procucts, by reacting 4-(1, 1, 3, 3-tetramethylbutyl)phenol with sulfur dichloride in an aromatic hydrocarbon solvent at a specific temperature range.
CONSTITUTION: 2, 2'-Bis[4-(1, 1, 3, 3-tetramethylbutyl)phenol]sulfide expressed by the formula is prepared by reacting 4-(1, 1, 3, 3-tetramethylbutyl)phenol with sulfur dichloride. The reaction is carried out in an aromatic hydrocarbon solvent at a temperature range of -10W20°C in the absence of a catalyst or in the presence of a Lewis acid catalyst, thereby suppressing the by-products, increasing the yield of the monosulfide and giving easily the desired compound with the ordinary post- treatment in high yield. The solvent is, e.g. benzene, toluene, chlorobenzene, etc.
USE: Polyolefin improver and its intermediate.
COPYRIGHT: (C)1980,JPO&Japio
JP53112270A 1978-09-14 1978-09-14 Method for producing 2,2'↓-bis[4↓-(1,1,3,3↓-tetramethylbutyl)phenol] sulfide Expired JPS5842866B2 (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
JP53112270A JPS5842866B2 (en) 1978-09-14 1978-09-14 Method for producing 2,2'↓-bis[4↓-(1,1,3,3↓-tetramethylbutyl)phenol] sulfide
GB7931450A GB2031422B (en) 1978-09-14 1979-09-11 Preparation of 2,2'-bis(4-substituted-phenol sulfides
AU50788/79A AU526442B2 (en) 1978-09-14 1979-09-12 Preparation of 2,2: -bis (4-substituted phenol) sulphides
IT25694/79A IT1123138B (en) 1978-09-14 1979-09-12 PROCESS FOR THE PREPARATION OF 2,2'-BIS (FENOL 4-REPLACED) SULPHURS
FR7922784A FR2436137A1 (en) 1978-09-14 1979-09-12 PROCESS FOR THE PREPARATION OF SULPHIDES OF 2,2'-BIS (PHENOL SUBSTITUTED IN 4)
NLAANVRAGE7906800,A NL186632C (en) 1978-09-14 1979-09-12 Process for the preparation of 2,2'-bis (4-substituted phenol) sulfides, as well as a 2,2'-bis (4-substituted phenol) sulfide.
DE19792937294 DE2937294A1 (en) 1978-09-14 1979-09-14 METHOD FOR PRODUCING 2,2'-BIS (4-SUBSTITUTED PHENOL) SULFIDES
US06/288,428 US4380671A (en) 1978-09-14 1981-07-30 Process for the preparation of 2,2'-bis(4-substituted phenol)sulfides

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP53112270A JPS5842866B2 (en) 1978-09-14 1978-09-14 Method for producing 2,2'↓-bis[4↓-(1,1,3,3↓-tetramethylbutyl)phenol] sulfide

Publications (2)

Publication Number Publication Date
JPS5540603A true JPS5540603A (en) 1980-03-22
JPS5842866B2 JPS5842866B2 (en) 1983-09-22

Family

ID=14582493

Family Applications (1)

Application Number Title Priority Date Filing Date
JP53112270A Expired JPS5842866B2 (en) 1978-09-14 1978-09-14 Method for producing 2,2'↓-bis[4↓-(1,1,3,3↓-tetramethylbutyl)phenol] sulfide

Country Status (1)

Country Link
JP (1) JPS5842866B2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0537726U (en) * 1991-10-21 1993-05-21 中興化成工業株式会社 Conveyor belt
JP2013203742A (en) * 2012-03-27 2013-10-07 Taoka Chem Co Ltd p-tert-OCTYLPHENOL-SULFUR CHLORIDE CO-CONDENSED RESIN

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5536410A (en) * 1978-09-07 1980-03-14 Mitsui Toatsu Chem Inc Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl)phenol)sulfide

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5536410A (en) * 1978-09-07 1980-03-14 Mitsui Toatsu Chem Inc Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl)phenol)sulfide

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0537726U (en) * 1991-10-21 1993-05-21 中興化成工業株式会社 Conveyor belt
JP2013203742A (en) * 2012-03-27 2013-10-07 Taoka Chem Co Ltd p-tert-OCTYLPHENOL-SULFUR CHLORIDE CO-CONDENSED RESIN

Also Published As

Publication number Publication date
JPS5842866B2 (en) 1983-09-22

Similar Documents

Publication Publication Date Title
KR840004755A (en) Method for preparing pyrrolo [3,4-c] pyrrole
ES494769A0 (en) A PROCEDURE FOR THE PRE-PARATION OF PHENOXIALCOXIFENIL- DERIVATIVES.
SE8106125L (en) 4,5-POLYMETHYLEN-4-ISOTIAZOLIN-3-ONES, SET FOR PREPARING THEREOF AND USING IT AS A BACTERICID AND FUNGICIDA AGENTS
ES2068889T3 (en) PROCEDURE FOR THE PRODUCTION OF AN AROMATIC CARBONATE COMPOUND.
SE7712060L (en) PROCEDURE FOR THE PREPARATION OF FUROCUMARINES
ES511705A0 (en) PROCEDURE FOR PREPARING FLUORMETHYLPYRIDINES.
JPS5540603A (en) Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl)phenol)sulfide
MX172888B (en) COMPOSITION BASED ON METHYL AND BENZYL DERIVATIVES OF DIPHENYLMETHANE AND ITS APPLICATION AS A DIELECTRIC
ES517995A0 (en) A PROCEDURE FOR THE PREPARATION OF A HYDROXYBENCILAMINOBENZENE COMPOUND, PROVIDED WITH ANTI-INFLAMMATORY PROPERTIES.
GB1530767A (en) Process for the preparation of alkylthiomethylphenols
IL62023A0 (en) 2-nitro-5-(substituted-phenoxy)-benzoate esters of -hydroxyalkanoates, their preparation and their use as herbicides
JPS5622762A (en) Preparation of 2,2'-bis(4-substituted phenol)sulfide
Donleavy et al. The synthesis of some alkamine esters of alkylthiobenzoic acids
FR2395259A1 (en) ACETALS AND THIO-ACETALS FOR USE AS ADDITIVES FOR LUBRICANTS
MX6660E (en) IMPROVED PROCEDURE FOR PREPARING THIOPHENOL
JPS5622761A (en) Novel 2,2'-bis(4-cumylphenol)derivative
ES508473A0 (en) A PROCEDURE FOR THE PREPARATION OF RANITIDINE.
ES556126A0 (en) A PROCEDURE FOR THE PREPARATION OF LEUCOTRIENIAN ANTAGONISTS
ES456400A1 (en) Thienothiazine derivatives
JPS5780366A (en) Bromodifluoromethyl sulfide and its preparation
ATE23158T1 (en) HEXAHYDRODIOXOPYRIMIDINES, THEIR PREPARATION AND USE.
BR8401710A (en) PROCESS FOR THE PREPARATION OF N-SULFENILATED PHENETYLSULPHONAMIDES, PRAGUIDIC COMPOSITIONS AND PROCESSES FOR COMBATING THE PEST AND FOR THE PREPARATION OF COMPOSITIONS
EP1044965A4 (en) Process for the preparation of aromatic sulfur compounds
DE69107331T3 (en) Lubricating oil additives, their manufacture and their use.
ES520136A0 (en) A PROCEDURE FOR THE PREPARATION OF A DERIVATIVE OF FURILOXAZOLYL-CETICAL ACID