JPS5493021A - Production of dianthraquinone-n,n'-dihydroazine - Google Patents
Production of dianthraquinone-n,n'-dihydroazineInfo
- Publication number
- JPS5493021A JPS5493021A JP15568177A JP15568177A JPS5493021A JP S5493021 A JPS5493021 A JP S5493021A JP 15568177 A JP15568177 A JP 15568177A JP 15568177 A JP15568177 A JP 15568177A JP S5493021 A JPS5493021 A JP S5493021A
- Authority
- JP
- Japan
- Prior art keywords
- amount
- aminoanthraquinone
- dimethylsulfoxide
- conducted
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: The reaction of aminoanthraquinone with an alkaline condensation agent is conducted in the presence of a specific amount of dimethylsolfoxide to produce high-quality title compound in high yield.
CONSTITUTION: The reaction between 1-aminoanthraquinone and an alkaline condensation agent as potassium hydroxide is conducted in the presence of dimethylsulfoxide in an amount of 0.1W2.5 times the quantity of the aminoanthraquinone and an oxidizing agent, when necessary, an inert solvent at 80W140°C.
EFFECT: Troublesome recovery process can be eliminated since the amount of dimethylsulfoxide employed is little and further the amount of caustic alkali used can be largely reduced.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15568177A JPS5493021A (en) | 1977-12-26 | 1977-12-26 | Production of dianthraquinone-n,n'-dihydroazine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15568177A JPS5493021A (en) | 1977-12-26 | 1977-12-26 | Production of dianthraquinone-n,n'-dihydroazine |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5493021A true JPS5493021A (en) | 1979-07-23 |
JPS576474B2 JPS576474B2 (en) | 1982-02-04 |
Family
ID=15611234
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP15568177A Granted JPS5493021A (en) | 1977-12-26 | 1977-12-26 | Production of dianthraquinone-n,n'-dihydroazine |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5493021A (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58186082U (en) * | 1982-06-04 | 1983-12-10 | 株式会社ダイケン | sliding runner |
JPS5915780U (en) * | 1982-07-21 | 1984-01-31 | 木村新株式会社 | Folding door guide device |
-
1977
- 1977-12-26 JP JP15568177A patent/JPS5493021A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS576474B2 (en) | 1982-02-04 |
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