JPH11258400A - Target for transition radiation x-ray generator - Google Patents

Target for transition radiation x-ray generator

Info

Publication number
JPH11258400A
JPH11258400A JP5656298A JP5656298A JPH11258400A JP H11258400 A JPH11258400 A JP H11258400A JP 5656298 A JP5656298 A JP 5656298A JP 5656298 A JP5656298 A JP 5656298A JP H11258400 A JPH11258400 A JP H11258400A
Authority
JP
Japan
Prior art keywords
target
thin films
rays
transition radiation
radiation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP5656298A
Other languages
Japanese (ja)
Inventor
Koji Yamada
浩治 山田
Teruo Hosokawa
照夫 細川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Telegraph and Telephone Corp
Original Assignee
Nippon Telegraph and Telephone Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Telegraph and Telephone Corp filed Critical Nippon Telegraph and Telephone Corp
Priority to JP5656298A priority Critical patent/JPH11258400A/en
Publication of JPH11258400A publication Critical patent/JPH11258400A/en
Pending legal-status Critical Current

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  • X-Ray Techniques (AREA)

Abstract

PROBLEM TO BE SOLVED: To realize a target for an X-ray generator that is easily fabricated and makes it possible to obtain X rays with intensity and good monochromatism. SOLUTION: A target has a structure where thin films 2, 4, 6, 8 and 10 made of substances that are highly efficient in transition radiation and those 3, 5, 7 and 9 made of substances that are high in the transmissivity of X rays are laminated alternately on a substrate 1. The thickness of the thin films 2, 4, 6, 8 and 10 made of the radioactive substances and the thin films 3, 5, 7 and 9 made of interstitial substances is set at the value where transitional radiation X rays with desired energy satisfy an interference condition. By filling with the space between the thin films made of the radioactive substances with the thin films made of interstitial substances, the former films are accurately arranged at equal intervals and interference is given to the transitional radiation X rays.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、電子ビーム照射に
よって遷移放射X線を発生させるX線発生装置用の標的
の構造に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a target structure for an X-ray generator that generates transition radiation X-rays by irradiating an electron beam.

【0002】[0002]

【従来の技術】従来より、電子ビーム照射によって遷移
放射X線を発生させるX線発生装置用の標的として、遷
移放射の発生効率が高い物質からなる薄膜が一定の間隔
で配設された多層薄膜標的が知られている。図4(a)
は従来の遷移放射型X線発生装置用標的の平面図、図4
(b)は図4(a)のA−A線断面図、図4(c)は後
述するスペーサーの平面図である。従来の遷移放射用標
的は、遷移放射の発生効率が高い物質(放射物質)から
なる薄膜12,14,16,18,20が等間隔に並べ
られた構造となっており、各薄膜間は真空あるいは大気
等の間隙となっていた。このような標的は、薄膜12,
14,16,18,20と上記間隙となるための穴が中
央部に配設された図4(c)のようなスペーサー13,
15,17,19とを交互に機械的に積層することによ
り製作される。
2. Description of the Related Art Conventionally, as a target for an X-ray generator for generating transition radiation X-rays by electron beam irradiation, a multilayer thin film in which thin films made of a substance having high transition radiation generation efficiency are arranged at regular intervals. Target is known. FIG. 4 (a)
FIG. 4 is a plan view of a conventional target for a transition radiation X-ray generator, and FIG.
4B is a sectional view taken along line AA of FIG. 4A, and FIG. 4C is a plan view of a spacer described later. A conventional transition radiation target has a structure in which thin films 12, 14, 16, 18, and 20 made of a substance (radiation material) having high transition radiation generation efficiency are arranged at equal intervals, and a vacuum is applied between the thin films. Or it was a gap such as the atmosphere. Such targets are thin films 12,
A spacer 13 as shown in FIG. 4 (c) in which holes for providing the above gaps with the spacers 14, 16, 18, 20 are arranged at the center.
It is manufactured by mechanically laminating 15, 17, and 19 alternately.

【0003】[0003]

【発明が解決しようとする課題】遷移放射標的に用いら
れる薄膜の厚さは通常0.1〜10μm程度であり、薄
膜の間隔、すなわちスペーサーの厚さも同程度である。
このように非常に薄い膜を狭い間隔で積層する標的に
は、製作が難しいという問題点があった。その理由は、
薄膜間隔が非常に狭いため、スペーサーが存在したとし
ても、製作過程で薄膜が変形して各薄膜が接触してしま
うことが多く、ひどい場合には薄膜自体が破損してしま
うからである。また、このような標的に電子ビームを照
射したときに得られるX線は、強度が弱く、単色性(波
長の単一性)に乏しいという問題点があった。その理由
は、薄膜間隔のばらつきが許容誤差である数%を大幅に
超えてしまうと、各薄膜から放射される遷移放射X線の
干渉性が失われるからである。また、一般にこれらの標
的は、電子ビームの散乱や発生したX線の減衰を防ぐた
め、真空中において電子ビームに照射されるのが好まし
いが、従来の構造では真空中で使用することができない
という問題点があった。その理由は、薄膜間隙に空気が
存在するため、真空中ではこの空気層と真空との間に大
きな圧力がかかり、薄膜が破損してしまうからである。
本発明は、上記課題を解決するためになされたもので、
製作が容易で、強力かつ単色性の良好な遷移放射X線を
得ることができる遷移放射型X線発生装置用標的を提供
することを目的とする。
The thickness of the thin film used for the transition radiation target is usually about 0.1 to 10 μm, and the distance between the thin films, that is, the thickness of the spacer is also about the same.
Such a target in which very thin films are stacked at a small interval has a problem that it is difficult to manufacture. The reason is,
This is because, since the distance between the thin films is very small, the thin films are often deformed during the manufacturing process and come into contact with each other even if a spacer is present, and in severe cases, the thin films themselves are damaged. Further, X-rays obtained when such a target is irradiated with an electron beam have low intensity and poor monochromaticity (uniformity of wavelength). The reason is that if the variation in the thin film interval greatly exceeds the allowable error of several percent, the coherence of transition radiation X-rays emitted from each thin film is lost. In general, it is preferable that these targets be irradiated with an electron beam in a vacuum in order to prevent scattering of the electron beam and attenuation of generated X-rays, but it cannot be used in a vacuum with a conventional structure. There was a problem. The reason is that since air exists in the gap between the thin films, a large pressure is applied between the air layer and the vacuum in a vacuum, and the thin film is damaged.
The present invention has been made to solve the above problems,
An object of the present invention is to provide a target for a transition radiation type X-ray generator that can be easily manufactured, and that can obtain strong and good monochromatic transition radiation X-rays.

【0004】[0004]

【課題を解決するための手段】本発明は、請求項1に記
載のように、電子ビーム照射によって遷移放射X線を発
生させるX線発生装置のための、遷移放射の発生効率が
高い物質からなる第1の薄膜が一定の間隔で配設された
多層薄膜標的であって、第1の薄膜間がX線透過率が高
い物質からなる第2の薄膜で満たされ、第1、第2の薄
膜の厚さは、所望のエネルギーの遷移放射X線が干渉条
件を満たすような値に設定されるものである。このよう
に、第1の薄膜間をX線透過率が高い物質からなる所定
膜厚の第2の薄膜で満たすことにより、遷移放射の発生
効率が高い物質からなる第1の薄膜を精度良く等間隔に
並べることができ、第1の薄膜から放射される遷移放射
X線に十分な干渉性を与えることができる。また、本発
明は、請求項2に記載のように、上記第1、第2の薄膜
がX線発生効率が低い物質からなる薄い基板上に形成さ
れたものである。
SUMMARY OF THE INVENTION According to the present invention, there is provided an X-ray generator for generating transition radiation X-rays by irradiating an electron beam. A first thin film formed of a substance having a high X-ray transmittance, wherein the first thin film is filled with a second thin film made of a substance having a high X-ray transmittance; The thickness of the thin film is set to a value such that transition radiation X-rays of desired energy satisfy the interference condition. As described above, by filling the gap between the first thin films with the second thin film having a predetermined thickness made of a substance having a high X-ray transmittance, the first thin film made of a substance having a high transition radiation generation efficiency can be precisely formed. The transition radiation X-rays emitted from the first thin film can be given sufficient coherence. In the present invention, the first and second thin films are formed on a thin substrate made of a material having low X-ray generation efficiency.

【0005】[0005]

【発明の実施の形態】[実施の形態の1]次に、本発明
の実施の形態について図面を参照して詳細に説明する。
図1は本発明の第1の実施の形態となる遷移放射型X線
発生装置用標的の断面図である。本実施の形態の標的
は、基板(メンブレン)1上に、遷移放射の発生効率が
高い物質(以下、放射物質と呼ぶ)からなる薄膜2,
4,6,8,10と、X線の透過率が高い物質(以下、
間隙物質と呼ぶ)からなる薄膜3,5,7,9とを交互
に積層した構造となっている。
DESCRIPTION OF THE PREFERRED EMBODIMENTS [First Embodiment] Next, an embodiment of the present invention will be described in detail with reference to the drawings.
FIG. 1 is a cross-sectional view of a target for a transition radiation X-ray generator according to a first embodiment of the present invention. The target of this embodiment is a thin film 2 made of a substance having a high transition radiation generation efficiency (hereinafter referred to as a radiation substance) on a substrate (membrane) 1.
4, 6, 8, 10 and substances having high X-ray transmittance (hereinafter, referred to as
This is a structure in which thin films 3, 5, 7, and 9 made of interstitial materials are alternately stacked.

【0006】電子ビームの照射時に基板1から発生する
X線は、薄膜2,4,6,8,10から発生する遷移放
射X線の干渉効果を乱すものである。しかしながら、基
板1として例えばSiN等のような電子密度が低い、す
なわち遷移放射や制動放射X線の発生効率が低い物質を
用いて、かつ発生X線の影響が小さくなるように基板1
を十分薄くすれば、その影響を殆ど無視することが可能
である。この基板1の使用により、薄膜2,4,6,
8,10から発生する遷移放射X線に影響を与えること
なく、標的の物理的強度を増大させることができる。
[0006] X-rays generated from the substrate 1 at the time of electron beam irradiation disturb the interference effect of transition radiation X-rays generated from the thin films 2, 4, 6, 8 and 10. However, the substrate 1 is made of a material having a low electron density such as SiN or the like, that is, a material having a low generation efficiency of transition radiation or bremsstrahlung X-rays, and the influence of the generated X-rays is reduced.
If is sufficiently thin, the effect can be almost ignored. By using this substrate 1, the thin films 2, 4, 6,
The physical intensity of the target can be increased without affecting the transition radiation X-rays generated from 8,10.

【0007】放射物質としては、遷移放射の発生効率が
高い、すなわち電子密度が高い固体の中重金属元素の単
体あるいはその化合物が好ましく、かつ発生するX線波
長周辺に吸収端を持たない材料が好ましい。このような
条件を満たす物質の例として、1〜10keVのX線領
域を対象とする場合にはニッケルが有望である。間隙物
質としては、X線透過率ができるだけ高い、すなわち電
子密度ができるだけ低い固体物質が好ましい。例えば、
ベリリウム、炭素、窒素などの軽元素の単体あるいはそ
れらの化合物が好ましい。
[0007] The radiating substance is preferably a simple substance or a compound of a medium heavy metal element having a high transition radiation generation efficiency, that is, a solid substance having a high electron density, and a material having no absorption edge around the generated X-ray wavelength. . As an example of a material that satisfies such conditions, nickel is promising in the case of targeting an X-ray region of 1 to 10 keV. As the interstitial material, a solid material having the highest possible X-ray transmittance, that is, the lowest possible electron density is preferable. For example,
Simple elements of light elements such as beryllium, carbon, and nitrogen or compounds thereof are preferable.

【0008】放射物質薄膜2,4,6,8,10及び間
隙物質薄膜3,5,7,9の厚さは、所望のエネルギー
の遷移放射X線が干渉条件を満たすような値に設定され
る。このとき、上記干渉条件は、放射物質薄膜2,4,
6,8,10の間隔、すなわち間隙物質薄膜3,5,
7,9の膜厚で決定され、遷移放射X線のエネルギー
は、放射物質薄膜2,4,6,8,10の膜厚とその間
隔で決定される。
The thicknesses of the radiating material thin films 2, 4, 6, 8, and 10 and the interstitial material thin films 3, 5, 7, and 9 are set to values such that transition radiation X-rays of desired energy satisfy interference conditions. You. At this time, the above-mentioned interference condition is set to the radiation substance thin films 2, 4,
6, 8, 10 intervals, ie, interstitial material thin films 3, 5,
The energy of the transition radiation X-ray is determined by the film thickness of the radiation material thin films 2, 4, 6, 8, and 10, and the interval between them.

【0009】以上のような構成は、適当な薄膜形成方法
によって基板1上に放射物質と間隙物質を交互に形成す
ることにより実現される。薄膜形成方法としては、半導
体プロセス等で従来から使用されている、蒸着法、CV
D法、スパッタ法、MBE法等を用いることが可能であ
る。なお、薄膜の層数については、任意に決定してよい
が、層数を増やし過ぎると、放射物質から発生した遷移
放射X線が吸収されるので注意が必要である。
The above configuration is realized by alternately forming a radiating substance and an interstitial substance on the substrate 1 by an appropriate thin film forming method. As a method for forming a thin film, a vapor deposition method, a CV
D method, sputtering method, MBE method and the like can be used. Note that the number of layers of the thin film may be arbitrarily determined, but care must be taken since excessively increasing the number of layers absorbs transition radiation X-rays generated from the radiating substance.

【0010】図2は本実施の形態の標的及び従来の標的
によって得られた遷移放射X線のエネルギースペクトル
を示す図である。図2においては、E1が本実施の形態
の標的による遷移放射X線のエネルギースペクトルであ
り、E2が従来の標的による遷移放射X線のエネルギー
スペクトルである。本実施の形態の標的としては、0.
188μm厚のニッケル薄膜と0.22μm厚の炭素薄
膜を交互に各10層堆積させたものを用い、従来の標的
としては、0.188μm厚のニッケル薄膜を不等間隔
で10層堆積させたもの(ニッケル薄膜間のスペーサー
の膜厚が不等なもの)を用いている。
FIG. 2 is a diagram showing energy spectra of transition radiation X-rays obtained by the target of the present embodiment and the conventional target. In FIG. 2, E1 is the energy spectrum of the transition radiation X-ray by the target of the present embodiment, and E2 is the energy spectrum of the transition radiation X-ray by the conventional target. As a target of the present embodiment, 0.
A 188 μm-thick nickel thin film and a 0.22 μm-thick carbon thin film were alternately deposited on each of 10 layers, and a conventional target was a 0.188 μm-thick nickel thin film deposited at 10 unequal intervals. (The thickness of the spacer between the nickel thin films is unequal).

【0011】図2は、これらの標的に対してエネルギー
15MeVの電子を照射し、このとき発生した遷移放射
X線を電子ビームの進行方向に対して34mrad角度
にて観測した場合のX線スペクトルを示している。従来
の標的では、放射物質薄膜の間隔のばらつきが大きいた
め、遷移放射X線の干渉性が失われる。したがって、図
2のE2で示すように、従来の標的に電子ビームを照射
したときに得られるX線は、強度が弱く、単色性に乏し
い。これに対し、本実施の形態の標的によれば、遷移放
射X線の干渉性が十分に得られるので、図2のE1で示
すように、強力かつ単色性の良好なX線が得られること
が分かる。
FIG. 2 shows an X-ray spectrum obtained by irradiating these targets with electrons having an energy of 15 MeV and observing transition emission X-rays generated at this time at an angle of 34 mrad with respect to the traveling direction of the electron beam. Is shown. In a conventional target, the coherence of transition radiation X-rays is lost due to a large variation in the distance between the radioactive substance thin films. Therefore, as shown by E2 in FIG. 2, the X-ray obtained when a conventional target is irradiated with an electron beam has low intensity and poor monochromaticity. On the other hand, according to the target of the present embodiment, since sufficient coherence of transition radiation X-rays can be obtained, X-rays having strong and good monochromaticity can be obtained as shown by E1 in FIG. I understand.

【0012】[実施の形態の2]図3は本発明の第2の
実施の形態となる遷移放射型X線発生装置用標的の断面
図であり、図1と同一の構成には同一の符号を付してあ
る。本実施の形態の標的は、実施の形態の1の標的と比
べて基板1がない構造となっている。このような構造
は、図1の標的の基板1を半導体プロセス等で従来から
使用されている各種エッチング法等によって除去するこ
とにより実現可能である。こうして、基板1の影響を完
全に除去することができる。
[Embodiment 2] FIG. 3 is a sectional view of a target for a transition radiation type X-ray generator according to a second embodiment of the present invention. Is attached. The target of the present embodiment has a structure without the substrate 1 as compared with the target of the first embodiment. Such a structure can be realized by removing the target substrate 1 of FIG. 1 by various etching methods conventionally used in a semiconductor process or the like. Thus, the influence of the substrate 1 can be completely removed.

【0013】[0013]

【発明の効果】本発明によれば、請求項1に記載のよう
に、第1の薄膜間を第2の薄膜で満たすことにより、遷
移放射の発生効率が高い物質からなる第1の薄膜を精度
良く等間隔に並べることができるので、第1の薄膜から
放射される遷移放射X線に十分な干渉性を与えることが
でき、強力かつ単色性の良好な遷移放射X線を得ること
ができる。また、第1、第2の薄膜の形成に周知の薄膜
形成法を利用することができるため、製作が容易とな
り、機械的製作箇所をなくすことができるため、製作工
程における薄膜の破損を防止することができる。さら
に、第1の薄膜間には空気層がないため、真空中でも使
用することが可能となる。
According to the present invention, as described in claim 1, by filling the space between the first thin films with the second thin film, the first thin film made of a substance having high transition radiation generation efficiency can be formed. Since they can be arranged at equal intervals with high accuracy, it is possible to give sufficient coherence to the transition radiation X-rays emitted from the first thin film, and to obtain transition radiation X-rays that are strong and have good monochromaticity. . In addition, since the well-known thin film forming method can be used for forming the first and second thin films, the manufacturing can be facilitated and the mechanical manufacturing portion can be eliminated, thereby preventing the thin film from being damaged in the manufacturing process. be able to. Furthermore, since there is no air layer between the first thin films, it can be used even in a vacuum.

【0014】また、請求項2に記載のように、第1、第
2の薄膜をX線発生効率が低い物質からなる薄い基板上
に形成することにより、標的の物理的強度を増大させる
ことができる。
Further, the physical strength of the target can be increased by forming the first and second thin films on a thin substrate made of a material having a low X-ray generation efficiency. it can.

【図面の簡単な説明】[Brief description of the drawings]

【図1】 本発明の第1の実施の形態となる遷移放射型
X線発生装置用標的の断面図である。
FIG. 1 is a cross-sectional view of a target for a transition radiation X-ray generator according to a first embodiment of the present invention.

【図2】 図1の標的及び従来の標的によって得られた
遷移放射X線のエネルギースペクトルを示す図である。
FIG. 2 is a diagram showing energy spectra of transition radiation X-rays obtained by the target of FIG. 1 and a conventional target.

【図3】 本発明の第2の実施の形態となる遷移放射型
X線発生装置用標的の断面図である。
FIG. 3 is a cross-sectional view of a target for a transition radiation X-ray generator according to a second embodiment of the present invention.

【図4】 従来の遷移放射型X線発生装置用標的の平面
図及び断面図とスペーサーの平面図である。
FIG. 4 is a plan view and a sectional view of a conventional target for a transition radiation X-ray generator, and a plan view of a spacer.

【符号の説明】[Explanation of symbols]

1…基板、2、4、6、8、10…放射物質薄膜、3、
5、7、9…間隙物質薄膜。
DESCRIPTION OF SYMBOLS 1 ... Substrate, 2, 4, 6, 8, 10 ... Radiation material thin film 3,
5, 7, 9 ... interstitial material thin film.

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 電子ビーム照射によって遷移放射X線を
発生させるX線発生装置のための、遷移放射の発生効率
が高い物質からなる第1の薄膜が一定の間隔で配設され
た多層薄膜標的であって、 前記第1の薄膜間がX線透過率が高い物質からなる第2
の薄膜で満たされ、 第1、第2の薄膜の厚さは、所望のエネルギーの遷移放
射X線が干渉条件を満たすような値に設定されることを
特徴とする遷移放射型X線発生装置用標的。
1. A multi-layer thin film target for a X-ray generator for generating transition radiation X-rays by electron beam irradiation, wherein first thin films made of a substance having high transition radiation generation efficiency are arranged at regular intervals. A second film made of a substance having a high X-ray transmittance between the first thin films.
Wherein the thickness of the first and second thin films is set to a value such that transition radiation X-rays of desired energy satisfy interference conditions. For target.
【請求項2】 請求項1記載の遷移放射型X線発生装置
用標的において、 前記第1、第2の薄膜がX線発生効率が低い物質からな
る薄い基板上に形成されていることを特徴とする遷移放
射型X線発生装置用標的。
2. The target for a transition radiation X-ray generator according to claim 1, wherein the first and second thin films are formed on a thin substrate made of a material having a low X-ray generation efficiency. A target for a transition radiation type X-ray generator.
JP5656298A 1998-03-09 1998-03-09 Target for transition radiation x-ray generator Pending JPH11258400A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP5656298A JPH11258400A (en) 1998-03-09 1998-03-09 Target for transition radiation x-ray generator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5656298A JPH11258400A (en) 1998-03-09 1998-03-09 Target for transition radiation x-ray generator

Publications (1)

Publication Number Publication Date
JPH11258400A true JPH11258400A (en) 1999-09-24

Family

ID=13030577

Family Applications (1)

Application Number Title Priority Date Filing Date
JP5656298A Pending JPH11258400A (en) 1998-03-09 1998-03-09 Target for transition radiation x-ray generator

Country Status (1)

Country Link
JP (1) JPH11258400A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004514120A (en) * 2000-11-09 2004-05-13 ステリス インコーポレイテッド X-ray target for products
WO2005098871A1 (en) * 2004-04-08 2005-10-20 Japan Science And Technology Agency X-ray-use target and device using it
US8208603B2 (en) 2009-07-28 2012-06-26 Canon Kabushiki Kaisha X-ray generating device
WO2016125289A1 (en) * 2015-02-05 2016-08-11 株式会社島津製作所 X-ray generator

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004514120A (en) * 2000-11-09 2004-05-13 ステリス インコーポレイテッド X-ray target for products
WO2005098871A1 (en) * 2004-04-08 2005-10-20 Japan Science And Technology Agency X-ray-use target and device using it
US7551722B2 (en) 2004-04-08 2009-06-23 Japan Science And Technology Agency X-ray target and apparatuses using the same
US8208603B2 (en) 2009-07-28 2012-06-26 Canon Kabushiki Kaisha X-ray generating device
WO2016125289A1 (en) * 2015-02-05 2016-08-11 株式会社島津製作所 X-ray generator
US10453579B2 (en) 2015-02-05 2019-10-22 Shimadzu Corporation X-ray generator

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