JPH1095992A - Production of powdery oil and fat - Google Patents
Production of powdery oil and fatInfo
- Publication number
- JPH1095992A JPH1095992A JP25463296A JP25463296A JPH1095992A JP H1095992 A JPH1095992 A JP H1095992A JP 25463296 A JP25463296 A JP 25463296A JP 25463296 A JP25463296 A JP 25463296A JP H1095992 A JPH1095992 A JP H1095992A
- Authority
- JP
- Japan
- Prior art keywords
- oils
- fats
- oil
- powdered
- particle size
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Bakery Products And Manufacturing Methods Therefor (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
【0001】[0001]
【発明の属する技術分野】本発明は、各種の飲食品、化
粧品、医薬品等に利用することができ、保存安定性、粉
体流動性に優れ、水に溶解した際に透明に溶解する新規
な粉末油脂の製造方法に関する。The present invention can be used for various foods and drinks, cosmetics, pharmaceuticals, etc., has excellent storage stability and powder fluidity, and is a novel compound which is transparently dissolved when dissolved in water. The present invention relates to a method for producing powdered fats and oils.
【0002】[0002]
【従来の技術】従来、各種の飲食品、化粧品、医薬品等
に利用される粉末油脂類の製法としては、例えば、油脂
類をゼラチンのような蛋白質溶液、デキストリンのよう
な加工澱粉溶液あるいはアラビアガムのような天然ガム
などの賦形剤で乳化し、熱風の流れる乾燥室中で圧力ま
たは遠心力を利用して液滴を噴霧することによって微粒
化し、短時間に水分を蒸発させ乾燥粉末化する噴霧乾燥
法などが用いられている。しかしながら噴霧乾燥法によ
って得られる粉末油脂類は、製造工程中に油脂類を比較
的高温で乾燥しているため、油脂類の着色、酸化、劣
化、変質等の恐れが多分にあり、得られる粉末の油脂類
含有量はかなり制約を受ける。また、製造工程中に乳化
処理を行っているため、得られた粉末油脂類を水に溶解
した場合に濁りを生じ、透明度を要求される飲食品等へ
の利用は制限されるなどの欠点があった。2. Description of the Related Art Conventionally, methods for producing powdered fats and oils used for various foods and drinks, cosmetics, pharmaceuticals, and the like include, for example, a method of preparing a fat or oil from a protein solution such as gelatin, a processed starch solution such as dextrin, or gum arabic. And emulsified with excipients such as natural gums, and atomized by spraying droplets using pressure or centrifugal force in a drying chamber where hot air flows, to evaporate water in a short time to form dry powder A spray drying method or the like is used. However, powdered fats and oils obtained by the spray-drying method, since the fats and oils are dried at a relatively high temperature during the manufacturing process, there is a possibility that the fats and oils may be colored, oxidized, deteriorated, deteriorated, etc. Of oils and fats is considerably restricted. In addition, since the emulsification treatment is performed during the manufacturing process, when the obtained powdered fats and oils are dissolved in water, turbidity is generated, and the use of the powdered fats and oils which is required to have transparency is limited. there were.
【0003】上記の欠点を解決するため、種々の提案が
なされている。例えば、DE18以下の澱粉加水分解物
の粘度0〜800cP(30℃)の水溶液を、内圧3〜
6kg/cm2 (温度140〜170℃)の条件下にド
ラムドライヤーで乾燥粉末化し、得られる粉末を粉末化
基剤として、油脂類と混合することを特徴とする粉状含
油組成物の製造方法(特公昭60−12399号公報参
照)、DE18以下の澱粉加水分解物および該澱粉加水
分解物の10−40重量%の香味油脂を混合して、得ら
れた香味油脂を吸着した澱粉加水分解物の0.5−5重
量%のプルランを水溶液として噴霧しながら、流動層造
粒することを特徴とする粉末香味料の製造法(特開平8
−47378号公報参照)などが提案されている。[0003] Various proposals have been made to solve the above-mentioned drawbacks. For example, an aqueous solution having a viscosity of 0 to 800 cP (30 ° C.) of a starch hydrolyzate having a DE of 18 or less is subjected to an internal pressure of 3 to
A method for producing a powdery oil-containing composition, comprising: drying and powdering with a drum dryer under conditions of 6 kg / cm 2 (temperature: 140 to 170 ° C.); and mixing the obtained powder with a fat or oil as a powdering base. (See Japanese Patent Publication No. 60-12399), a starch hydrolyzate having a DE of 18 or less and a flavor oil of 10 to 40% by weight of the starch hydrolyzate, and adsorbing the obtained flavor oil. Of 0.5 to 5% by weight of pullulan as an aqueous solution while granulating in a fluidized bed.
-47378) and the like.
【0004】しかしながら、上記、特公昭60−123
99号公報記載の製造法で得られる粉末油脂類は、水に
溶解した際に、完全に透明に溶解せず、また粉体の流動
性も、特に油脂類含有率が高い場合には基剤粒子表面が
べとついて流動性が悪くなるという欠点があった。ま
た、特開平8−47378号公報記載の製造法で得られ
る粉末油脂類は、粉体流動性の点で改善は見られるもの
の、油脂類と澱粉加水分解物を混合した後、流動層造粒
機にて顆粒化しているため、造粒機内の熱風により油脂
類の劣化が避けられず、必ずしも満足できるものではな
い。[0004] However, the above-mentioned Japanese Patent Publication No. Sho 60-123.
Powdered fats and oils obtained by the production method described in JP-A-99-99, when dissolved in water, do not completely dissolve transparently, and the fluidity of the powder, especially when the fats and oils content is high, the base There is a disadvantage that the surface of the particles becomes sticky and the fluidity deteriorates. Powdered fats and oils obtained by the production method described in JP-A-8-47378 are improved in terms of powder fluidity, but after mixing the fats and oils with a starch hydrolyzate, fluidized bed granulation is performed. Because of the granulation in the granulator, the deterioration of fats and oils due to the hot air in the granulator is inevitable and is not always satisfactory.
【0005】[0005]
【発明が解決しようとする課題】本発明の目的は、各種
の飲食品、化粧品、医薬品等に利用できる保存安定性、
粉体流動性に優れ、水溶液が透明である粉末油脂の製造
方法を提供するにある。SUMMARY OF THE INVENTION An object of the present invention is to provide a storage stability which can be used for various foods and drinks, cosmetics, pharmaceuticals, and the like.
An object of the present invention is to provide a method for producing a powdery fat or oil having excellent powder fluidity and a transparent aqueous solution.
【0006】[0006]
【課題を解決するための手段】本発明者らは上記欠点を
有する従来型の粉末油脂について、その欠点を解決すべ
く鋭意研究を行った結果、澱粉加水分解物を特定の範囲
内の粒径、粒度、ゆるめ嵩密度および圧縮度に顆粒化し
た後、これに油脂類を吸着させることにより前記課題が
解決されることを見いだし、本発明を完成するに至っ
た。Means for Solving the Problems The inventors of the present invention have conducted intensive studies on conventional powdered fats and oils having the above-mentioned drawbacks to solve the drawbacks. As a result, the starch hydrolyzate was found to have a particle size within a specific range. The present inventors have found that the above-mentioned problems can be solved by adsorbing fats and oils to the granules after granulation to a particle size, a loose bulk density and a degree of compression, thereby completing the present invention.
【0007】すなわち、本発明は、澱粉加水分解物を、
平均粒径200〜1000ミクロン、粒度100メッシ
ュパス30%以下、ゆるめ嵩密度0.1〜0.3g/c
m3、圧縮度5〜30%の範囲で顆粒化した後、油脂類
と混合することを特徴とする粉末油脂の製造方法であ
る。That is, the present invention provides a starch hydrolyzate
Average particle size 200-1000 microns, particle size 100 mesh pass 30% or less, loose bulk density 0.1-0.3 g / c
This is a method for producing a powdered oil or fat, which is characterized in that granulation is performed in the range of m 3 and a degree of compression of 5 to 30%, and then mixed with an oil or fat.
【0008】[0008]
【発明の実施の形態】以下、本発明について更に詳細に
述べる。本発明において使用しうる澱粉加水分解物は、
例えば、サツマイモ、ジャガイモ、トウモロコシ、キャ
ッサバ、コムギ、コメ等の各種の澱粉の加水分解により
得られるものである。加水分解方法は、例えば、適宜の
酸、酵素もしくは両者を併用して実施できる。本発明の
澱粉加水分解物は上記の方法で調製したものも使用でき
るが、市場で容易に入手でき、例えば、パインフロー
(松谷化学工業株式会社製)、オイルキュー(日澱化学
株式会社製)等を挙げることができる。BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, the present invention will be described in more detail. The starch hydrolyzate that can be used in the present invention includes:
For example, it is obtained by hydrolysis of various starches such as sweet potato, potato, corn, cassava, wheat, rice and the like. The hydrolysis method can be carried out, for example, by using an appropriate acid, enzyme or both. The starch hydrolyzate of the present invention may be one prepared by the above method, but it is easily available on the market. For example, Pine Flow (manufactured by Matsutani Chemical Industry Co., Ltd.) and Oil Cue (manufactured by Nichiten Chemical Co., Ltd.) And the like.
【0009】また、本発明では上記の澱粉加水分解物を
造粒して、特定の範囲内の粒径、粒度、ゆるめ嵩密度お
よび圧縮度に顆粒化した顆粒化澱粉加水分解物を、粉末
化基剤として用いるが、かかる造粒方法としては、例え
ば、上記の澱粉加水分解物に、結着剤水溶液を噴霧しな
がら流動層造粒する方法がある。結着剤としては、例え
ば、アラビアガム、キサンタンガム、グアガム、馬鈴薯
澱粉、コーンスターチ、ゼラチン、アルギン酸ソーダな
どを挙げることができ、その水溶液の粘度は、例えば、
100〜1000cP、好ましくは300〜500cP
の範囲が適当である。また、特定の範囲内の粒径、粒
度、ゆるめ嵩密度および圧縮度の粉末化基剤を得るため
には、例えば、流動層造粒機の条件として、吸気温度6
0〜90℃、結着剤噴霧空気圧1.0〜2.0Kg/c
m2 、結着液の分量20〜40%(基剤に対して)、結
着液の粘度500cPで造粒することにより、平均粒径
200〜1000ミクロン、粒度100メッシュパス3
0%以下、ゆるめ嵩密度0.1〜0.3g/cm3 、圧
縮度5〜30%の顆粒化物が得られる。In the present invention, the above-mentioned starch hydrolyzate is granulated, and the granulated starch hydrolyzate obtained by granulating into a specific range of particle size, particle size, loose bulk density and compressibility is powdered. The granulation method used as a base is, for example, a method of fluidized bed granulation while spraying an aqueous solution of a binder onto the starch hydrolyzate. Examples of the binder include gum arabic, xanthan gum, guar gum, potato starch, corn starch, gelatin, sodium alginate, and the like.
100-1000 cP, preferably 300-500 cP
Is appropriate. In order to obtain a powdered base having a particle size, particle size, loose bulk density and compressibility within a specific range, for example, as a condition of a fluidized bed granulator, an intake air temperature of 6
0-90 ° C, binder spray air pressure 1.0-2.0Kg / c
m 2 , by granulating with a binder liquid content of 20 to 40% (based on the base) and a binder liquid viscosity of 500 cP, an average particle diameter of 200 to 1000 μm and a particle diameter of 100 mesh pass 3
A granulated product having 0% or less, a loose bulk density of 0.1 to 0.3 g / cm 3 and a degree of compression of 5 to 30% is obtained.
【0010】本発明で粉末化基剤として使用する澱粉加
水分解物の顆粒化物は、平均粒径200〜1000ミク
ロン、粒度100メッシュパス30%以下、ゆるめ嵩密
度0.1〜0.3g/cm3 、圧縮度5〜30%の範
囲、好ましくは、平均粒径200〜600ミクロン、粒
度100メッシュパス25%以下、ゆるめ嵩密度0.1
5〜0.25g/cm3 、圧縮度10〜20%の範囲の
ものが利用できる。この範囲に入らないものを使用した
場合は、粉体流動性、吸油力、保存安定性が悪くなった
り、水に溶解した場合に濁りを生ずる。The granulated starch hydrolyzate used as a powdering base in the present invention has an average particle size of 200 to 1000 microns, a particle size of 100 mesh pass of 30% or less, and a loose bulk density of 0.1 to 0.3 g / cm. 3. The degree of compression is in the range of 5 to 30%, preferably, the average particle size is 200 to 600 microns, the particle size is 100 mesh pass 25% or less, and the loose bulk density is 0.1.
Those having a range of 5 to 0.25 g / cm 3 and a degree of compression of 10 to 20% can be used. If a material that does not fall within this range is used, the powder fluidity, oil absorbing power, and storage stability will deteriorate, and turbidity will occur when dissolved in water.
【0011】本発明によれば、澱粉加水分解物を特定の
範囲内の粒径、粒度、圧縮度、ゆるめ嵩密度で顆粒化し
た後、これを粉末化基剤として、油脂類と混合すること
により、所望の油脂類を吸着保持させてなる粉末油脂を
得る。このような粉末化基剤を油脂類と混合する場合
は、所望により通常用いられている粉末化基剤、例えば
微結晶セルロース粉末(アビセル(旭化成社製商品名)
など)、可溶性澱粉、加工澱粉、デキストリン、大豆多
糖類、乳糖、ブドウ糖、炭酸カルシウム、リン酸3カル
シウム、二酸化ケイ素等の1種または2種以上を配合す
ることもできる。According to the present invention, a starch hydrolyzate is granulated in a specific range of particle size, particle size, compressibility and loose bulk density, and then mixed with fats and oils as a powdering base. Thus, a powdered fat or oil obtained by adsorbing and holding a desired fat or oil is obtained. When such a powdered base is mixed with fats and oils, a powdered base usually used as required, for example, microcrystalline cellulose powder (Avicel (trade name, manufactured by Asahi Kasei Corporation))
), Soluble starch, processed starch, dextrin, soybean polysaccharide, lactose, glucose, calcium carbonate, tricalcium phosphate, silicon dioxide and the like.
【0012】また、本発明で混合され粉末化基剤に吸着
保持される油脂類は従来より食品、化粧品、医薬品等で
用いられている液体乃至固体状の油脂類が利用でき、具
体的には、例えば、大豆油、ゴマ油、ピーナッツ油、コ
ーン油、菜種油、ヤシ油、パーム油などの植物油脂類及
びそれらの硬化油;牛脂、豚脂、魚油などの動物油脂類
及びそれらの硬化油;バター、マーガリン、ショートニ
ングなどの加工油脂類;ビタミンE、DHA、EPA、
リノール酸、γ−リノレン酸、α−リノレン酸、月見草
油、ボラージ油、レシチン、オクタコサノール、γ−オ
リザノールなどの機能性油脂類;精油、香味油、オレオ
レジン、天然香料、合成香料およびそれらの2種以上の
調合物などの油溶性香料類などが挙げられる。これらを
1種または2種以上の混合物として使用することができ
る。The fats and oils mixed and adsorbed and held on the powdered base in the present invention may be liquid or solid fats and oils conventionally used in foods, cosmetics, pharmaceuticals and the like. For example, vegetable oils and fats such as soybean oil, sesame oil, peanut oil, corn oil, rapeseed oil, coconut oil, palm oil and their hardened oils; animal fats and oils such as tallow, lard, fish oil and the like, and butter; , Margarine, shortening and other processed oils and fats; Vitamin E, DHA, EPA,
Functional oils and fats such as linoleic acid, γ-linolenic acid, α-linolenic acid, evening primrose oil, borage oil, lecithin, octacosanol, γ-oryzanol; essential oils, flavor oils, oleoresins, natural flavors, synthetic flavors and their two. And oil-soluble flavors such as a mixture of more than one kind. These can be used alone or as a mixture of two or more.
【0013】上記の油脂類には、通常用いられている抗
酸化剤、例えば、ビタミンE、茶抽出物、生コーヒー豆
抽出物、クロロゲン酸、香辛料抽出物、カフェ酸、ロー
ズマリー抽出物、ビタミンCパルミテート、ルチン、ケ
ルセチン、ヤマモモ抽出物などを適宜配合することによ
り、これら油脂類の劣化を防止することができる。The above fats and oils include commonly used antioxidants such as vitamin E, tea extract, green coffee bean extract, chlorogenic acid, spice extract, caffeic acid, rosemary extract, vitamin By appropriately mixing C palmitate, rutin, quercetin, bayberry extract and the like, deterioration of these fats and oils can be prevented.
【0014】本発明の粉末化基剤と油脂類との配合割合
は、厳密に制限されるものではなく、用いる油脂類の種
類等に応じて広い範囲にわたり変えることができるが、
通常、粉末化基剤100重量部に対し油脂類を約10〜
約120重量部、好ましくは約20〜約100重量部の
範囲内が適当である。本発明によれば、油脂類と粉末化
基剤の配合割合が1:1となっても、従来品に比べ、保
存安定性、粉体流動性は顕著に改善される。The mixing ratio of the powdered base of the present invention and fats and oils is not strictly limited, and can be varied over a wide range depending on the kind of fats and oils to be used.
Normally, fats and oils are added in an amount of about 10 to 100 parts by weight of the powdered base.
A suitable range is about 120 parts by weight, preferably about 20 to about 100 parts by weight. According to the present invention, even when the mixing ratio of the fats and oils to the powdered base is 1: 1, the storage stability and powder fluidity are remarkably improved as compared with the conventional product.
【0015】前記油脂類を吸着保持する方法は単に、粉
末化基剤(顆粒化澱粉加水分解物)と油脂類とを混合す
るのみで足り、極めて容易に調製することができる。油
脂類が液体の場合はそのまま、また、固体状の場合はあ
らかじめ油脂類を加熱溶解後に粉末化基剤に添加し、ま
たは油脂類に粉末化基剤を添加して実施できる。混合機
としては公知の、例えば、リボンミキサー、ナウタミキ
サー、バーチカルグラニュレーター、ドラムミキサー、
高速攪拌混合機、パポーズミキサー、万能混合機、ケー
キミキサーなどが使用でき、混合温度は、約10〜約6
0℃、好ましくは約20〜約50℃で、約5分〜約2時
間、好ましくは約30分〜約1時間混合することにより
容易に目的とする粉末油脂が得られる。The method for adsorbing and holding the fats and oils is sufficient only by mixing a powdered base (hydrolyzate of granulated starch) and fats and oils, and can be prepared very easily. When the fats and oils are liquid, they can be used as they are, or when the fats and oils are solid, they can be added to a powdered base after heating and dissolving the fats or oils, or by adding a powdered base to the fats and oils. Known as a mixer, for example, a ribbon mixer, a Nauta mixer, a vertical granulator, a drum mixer,
A high-speed stirring mixer, a pausing mixer, a universal mixer, a cake mixer, etc. can be used, and the mixing temperature is about 10 to about 6
By mixing at 0 ° C., preferably about 20 ° C. to about 50 ° C., for about 5 minutes to about 2 hours, preferably for about 30 minutes to about 1 hour, the desired powdered fat or oil can be easily obtained.
【0016】本発明の粉末油脂の調製法の好ましい一実
施態様を示せば、例えば、澱粉加水分解物を流動層造粒
機にて造粒して得られる、平均粒径200〜1000ミ
クロン、粒度100メッシュパス30%以下、ゆるめ嵩
密度0.1〜0.3g/cm3 及び圧縮度5〜30%の
範囲の顆粒化物200gに、油脂類150gをケーキミ
キサーにて約30〜40℃で、約5〜30分混合して粉
末油脂を得る。このようにして得られる粉末油脂は、保
存安定性、粉体流動性に優れ、水に透明に溶解すること
ができる。上述のようにして得られる粉末油脂は、例え
ば、飲料、粉末飲料、デザート、チューインガム、錠
菓、スナック類、水産加工食品、畜肉加工食品、レトル
ト食品、スープ類などの飲食品さらには化粧品、医薬品
等にも利用することができる。In a preferred embodiment of the method for preparing a powdered fat or oil according to the present invention, for example, a starch hydrolyzate obtained by granulation with a fluidized bed granulator, having an average particle size of 200 to 1000 microns and a particle size of To 100 g of a granulated product having a 100 mesh pass of 30% or less, a loose bulk density of 0.1 to 0.3 g / cm 3 and a degree of compression of 5 to 30%, 150 g of fats and oils is added at about 30 to 40 ° C. using a cake mixer. Mix for about 5 to 30 minutes to obtain a powdered fat. The powdered fats and oils thus obtained are excellent in storage stability and powder fluidity, and can be transparently dissolved in water. Powdered fats and oils obtained as described above include, for example, beverages, powdered beverages, desserts, chewing gum, tablet confections, snacks, processed marine products, processed meat, retort foods, foods and drinks such as soups, and further cosmetics and pharmaceuticals. Etc. can also be used.
【0017】[0017]
【実施例】次に実施例を挙げて本発明をさらに具体的に
説明する。 (粉末化基剤の調製例)Glatt社製流動層造粒機を
用いて、パインフロー(松谷化学工業株式会社製澱粉加
水分解物)250gに0.5重量%のグアガム水溶液を
噴霧して、造粒条件を変化させ、表1に示す各種平均粒
径、粒度100メッシュパス、ゆるめ嵩密度、圧縮度の
粉末化基剤(顆粒化物)No.1〜4を得た。尚、造粒
条件は、吸気温度70℃、結着剤噴霧空気圧1.5kg
/cm2 とし、結着剤噴霧量を55g(No.1)、7
0g(No.2)、90g(No.3)、及び25g
(No.4)で行った。表1に、比較のためにパインフ
ロー、オイルキュー(日澱化学株式会社製澱粉加水分解
物)の各特性を併記する。Next, the present invention will be described more specifically with reference to examples. (Example of preparation of powdered base) Using a fluidized bed granulator manufactured by Glatt, a guagum aqueous solution of 0.5% by weight was sprayed on 250 g of pine flow (starch hydrolyzate manufactured by Matsutani Chemical Industry Co., Ltd.). The granulation conditions were changed, and the powdered base (granulated material) No. having various average particle sizes, a particle size of 100 mesh passes, a loose bulk density, and a degree of compression shown in Table 1 was used. 1-4 were obtained. The granulation conditions were as follows: intake temperature 70 ° C., binder spray air pressure 1.5 kg
/ Cm 2 and the binder spray amount is 55 g (No. 1), 7
0 g (No. 2), 90 g (No. 3), and 25 g
(No. 4). Table 1 also shows the characteristics of pine flow and oil cue (starch hydrolyzate manufactured by Nisseki Chemical Co., Ltd.) for comparison.
【0018】[0018]
【表1】 [Table 1]
【0019】(実施例1〜9及び比較例1〜9)上記の
調製例で得られたN0.1〜4の各粉末化基剤、パイン
フロー、オイルキュー各200gにラードを、含油率1
0、30、50重量%(粉末化基剤を100重量部とし
た場合、それぞれ11、43、100重量部)となるよ
うに、万能混合機内、時間30分、温度40℃で混合
し、粉末油脂を得た。得られた各粉末油脂の粉体流動性
および水に溶解したときの透明度を表2に示した。尚、
粉体流動性は圧縮度で示し、この圧縮度の値が小さいほ
ど流動性が良く、また、水に溶解したときの透明度は濁
度で示し、この濁度の値が小さいほど透明度が高いこと
を示す。圧縮度及び濁度の測定方法を以下に記す。(Examples 1 to 9 and Comparative Examples 1 to 9) Each of the powdered bases of N0.1 to N4, pine flow and oil cue obtained in the above preparation examples, lard was added to 200 g each, and the oil content was 1 unit.
The mixture was mixed in a universal mixer at a temperature of 40 ° C. for 30 minutes so as to be 0, 30, and 50% by weight (11, 43, and 100 parts by weight, respectively, when the powdered base was 100 parts by weight). An oil was obtained. Table 2 shows the powder fluidity of each of the obtained powdered fats and oils and the transparency when dissolved in water. still,
The powder fluidity is indicated by the degree of compression. The smaller the value of the degree of compression, the better the fluidity.The transparency when dissolved in water is indicated by the turbidity, and the smaller the value of the turbidity, the higher the transparency. Is shown. The method of measuring the degree of compression and turbidity is described below.
【0020】圧縮度 内径50mmφ、100ccの容器に、上方から10メ
ッシュのふるいを通して粉末油脂を疎充填し、重量を測
定してゆるめ嵩密度(A)を求める。次いで容器に同径
のわくをはめて粉末油脂を追加し、タッピング装置にか
けて18mmの落差で180回タッピングを行う。わく
をはずし、容器上縁で粉体をすり切って計量し、固め嵩
密度(B)を求める。圧縮度(C)は次式(1)で表さ
れる。 C[%]=(B−A)÷B×100‥‥(1) 濁度 粉末油脂1gに60℃の温水100gを加えて溶解した
後、5分後水層部を波長680nmで吸光度を測定す
る。Compressibility A 100-cc container having an inner diameter of 50 mmφ is loosely filled with powdered fat through a 10-mesh sieve from above, and the weight is measured to determine the loose bulk density (A). Then, a powdery fat is added to a container having the same diameter, and tapping is performed 180 times by a tapping device at a head of 18 mm. The frame is removed and the powder is ground at the upper edge of the container and weighed to obtain a consolidated bulk density (B). The compression degree (C) is represented by the following equation (1). C [%] = (B−A) {B × 100} (1) Turbidity 100 g of hot water at 60 ° C. was added to and dissolved in 1 g of powdered oil and fat, and after 5 minutes, the absorbance of the water layer was measured at a wavelength of 680 nm. I do.
【0021】[0021]
【表2】 [Table 2]
【0022】表2から明らかなように、比較例ではいず
れも含油量が低い場合は粉体流動性が若干良好である
が、含油量が高い場合は基剤粒子表面がべとついて流動
性が悪く、また水に溶解した場合には濁りを生じた。従
って、比較例1〜3(粉末化基剤No.4を使用)のよ
うに市販されている澱粉加水分解物を顆粒化して使用し
た粉末油脂でも、粉末化基剤を特定の範囲内の粒径、粒
度、ゆるめ嵩密度および圧縮度としなければ、所望の粉
末油脂は得られない。一方、実施例ではいずれも含油量
が高い場合も流動性が良好であり、水に透明に溶解し
た。As is clear from Table 2, in each of the comparative examples, when the oil content is low, the powder fluidity is slightly good, but when the oil content is high, the base particles have a sticky surface and the fluidity is low. Bad and turbid when dissolved in water. Therefore, even in the case of powdered fats and oils obtained by granulating a starch hydrolyzate which is commercially available as in Comparative Examples 1 to 3 (using powdered base No. 4), the powdered base is treated in a specific range. Unless the diameter, particle size, loose bulk density and degree of compression are set, the desired powdered fats and oils cannot be obtained. On the other hand, in each of the examples, even when the oil content was high, the fluidity was good, and the oil was transparently dissolved in water.
【0023】また、比較例および実施例の粉末油脂を室
温で1カ月保存したところ、比較例では油にじみが激し
くなり、油脂の劣化臭が生じたが、実施例ではいずれも
油脂の劣化は見られず、粉体流動性および香味の点でも
安定であった。When the powdered fats and oils of the comparative examples and examples were stored at room temperature for one month, oil bleeding became severe in the comparative examples and the odor of the fats and oils deteriorated. It was stable in terms of powder fluidity and flavor.
【0024】[0024]
【発明の効果】本発明によれば、澱粉加水分解物を顆粒
化した後に油脂を混合するため、造粒機内の熱風によっ
て油脂類が劣化せず、保存安定性、粉体流動性に優れ、
水に溶解した際に透明に溶解し、各種の飲食品、化粧
品、医薬品等に利用することができる粉末油脂の製造方
法を提供することができる。According to the present invention, fats and oils are mixed after granulation of a starch hydrolyzate, so that fats and oils are not deteriorated by hot air in a granulator, and have excellent storage stability and powder flowability.
It is possible to provide a method for producing powdered fats and oils that dissolves transparently when dissolved in water and can be used for various foods and drinks, cosmetics, pharmaceuticals, and the like.
───────────────────────────────────────────────────── フロントページの続き (72)発明者 伊東 昭 神奈川県川崎市中原区苅宿335 長谷川香 料株式会社技術研究所内 ──────────────────────────────────────────────────続 き Continued on the front page (72) Inventor Akira Ito 335 Kariyuku, Nakahara-ku, Kawasaki-shi, Kanagawa Pref.
Claims (1)
000ミクロン、粒度100メッシュパス30%以下、
ゆるめ嵩密度0.1〜0.3g/cm3 、圧縮度5〜3
0%の範囲で顆粒化した後、油脂類と混合することを特
徴とする粉末油脂の製造方法。1. A starch hydrolyzate having an average particle size of 200 to 1
000 microns, particle size 100 mesh pass 30% or less,
Loose bulk density 0.1-0.3 g / cm 3 , degree of compression 5-3
A method for producing powdered fats and oils, comprising granulating in the range of 0% and then mixing with fats and oils.
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JP25463296A JP3501595B2 (en) | 1996-09-26 | 1996-09-26 | Production method of powdered fats and oils |
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JP25463296A JP3501595B2 (en) | 1996-09-26 | 1996-09-26 | Production method of powdered fats and oils |
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JPH1095992A true JPH1095992A (en) | 1998-04-14 |
JP3501595B2 JP3501595B2 (en) | 2004-03-02 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004033142A (en) * | 2002-07-05 | 2004-02-05 | Showa Sangyo Co Ltd | Granular tempura flour |
JP2008521396A (en) * | 2004-11-29 | 2008-06-26 | エルサム・エンジニアリング・アクティーゼルスカブ | Enzymatic hydrolysis of biomass with high dry matter (DM) content |
JP2009011269A (en) * | 2007-07-06 | 2009-01-22 | Japan Tobacco Inc | Oil and fat-containing granule and method for producing the same |
WO2023120319A1 (en) * | 2021-12-24 | 2023-06-29 | 株式会社J-オイルミルズ | Cosmetic composition |
-
1996
- 1996-09-26 JP JP25463296A patent/JP3501595B2/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004033142A (en) * | 2002-07-05 | 2004-02-05 | Showa Sangyo Co Ltd | Granular tempura flour |
JP2008521396A (en) * | 2004-11-29 | 2008-06-26 | エルサム・エンジニアリング・アクティーゼルスカブ | Enzymatic hydrolysis of biomass with high dry matter (DM) content |
JP2009011269A (en) * | 2007-07-06 | 2009-01-22 | Japan Tobacco Inc | Oil and fat-containing granule and method for producing the same |
WO2023120319A1 (en) * | 2021-12-24 | 2023-06-29 | 株式会社J-オイルミルズ | Cosmetic composition |
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